OP-II-3

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ORAL PRESENTATIONSSECTION IIIChemical Reactors and Technologiesfor Emerging ApplicationsSection III-AProcessing of Biomass and Renewable Feedstocks
OP-III-A-1A NEW SIMPLE MICROCHANNEL DEVICE FOR INTENSIFYINGBIODIESEL PRODUCTIONSantacesaria E. 1 , Di Serio M., Tesser R., Russo V., Turco R., Tortorelli M.University of Naples “Federico II” – Department of Chemistry,Complesso Universitario Monte S. Angelo, Via Cintia 4, I-80126 Naples (Italy)1 E-mail address: elio.santacesaria@unina.it - Fax: +39 081674026In the present work a new laboratory device, recently patented 1 , specificallydeveloped to obtain microchannels, in order to test the process intensification effecton different reactions will be described. This device represents a useful connectionbetween a traditional tubular packed bed reactor and the microreactors that are veryefficient, as it is well known, in mass and energy transfer operations. The apparatusdeveloped in this work is constituted by a tubular reactor which packing is composedby metallic spheres with different diameters and/or of filling material of differentshape and size. The filling material size is chosen in a way that the cavities betweenthe particles promote a very active local micromixing. In the obtained packing of thetubular reactor, microchannels are present with variable sizes in a range between200-2000 µm, values that are comparable with those of the commercially availablemicroreactors. Moreover, with microchannels of these sizes, an intensive mixing isrealized also at relatively low flow rates, enhancing the mass transfer effect, inparticular in the case of immiscible liquid phases, while, the metal thermalconductivity allows a fast heat exchange.The transesterification reaction of vegetable oil with methanol, promoted bypotassium or sodium hydroxide or related alkoxides, is characterized by theimmiscibility of the reagents. Therefore, the reaction is strongly enhanced by anefficient stirring and is, therefore, particularly suitable to be conducted in amicroreactor in which micromixing is very active. Moreover, this aspect can be betterprofited by increasing the temperature above the boiling point of methanol (65°C),obviously operating at higher pressure. In this case the reaction rate increases moreand more but, due to micromixing, the reaction is not limited by the mass transfer.This behavior has recently been demonstrate by using, for producing biodiesel, aCorrugated Plates Heat Exchanger (CP-HEX reactor) as reactor 2,3 . As this reaction isathermic the operation is safe and the isothermicity can easily be achieved. We willdemonstrate in this work that by using a tubular reactor filled with spheres or filling153
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Boreskov Institute of Catalysisof t
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INTERNATIONAL SCIENTIFIC COMMITTEEV
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SILVER SPONSORThe organizers expres
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PL-1HOW TO DESIGN OPTIMAL CATALYTIC
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MULTIFUNCTIONAL DEVICES FOR INTENSI
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PL-3DESIGN OF CATALYTIC PROCESSES F
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PL-3Indeed preparation and testing
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PL-4The second part of the lecture
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PL-5Reactor designs with intensifie
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PL-6MEMBRANE REACTORS: STATE OF THE
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KEY-NOTE PRESENTATIONS
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KN-1description, that can be charac
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KN-2selective catalytic reduction o
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KN-3Fig. 1. Experimental burner of
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KN-4~200°C. This is based on the H
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KN-5for addressing the quality of t
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KN-6reaction with ethanol and the b
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KN-7at temperature lower than 873K,
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REACTION KINETICS AND REACTION ENHA
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OP-I-2RELATION BETWEEN THE ACTIVATI
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COMPARISON OF CHEMICAL AND ENZYMATI
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OP-I-4NONLINEAR PHENOMENA DURING ME
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OP-I-5SPECIFICITY OF THE OSCILLATIO
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OP-I-6TRENDS IN BISTABILITY DOMAINS
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OP-I-7NON-STEADY-STATE CATALYST CHA
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OP-I-8TRANSIENT KINETIC STUDIES OF
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OP-I-9A REDOX KINETICS FOR THE PART
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OP-I-9500Flow of Air = 0.3 m 3 (STP
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OP-I-11ELUCIDATION OF THE REACTIVIT
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KINETIC MODELLING OF THE JOINT TRAN
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OP-I-13n-HEXANE SKELETAL ISOMERIZAT
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OP-I-14the slow branch of kinetic c
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OP-I-15The hydride palladium comple
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Energy Conservation (field j)∂∂
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OP-I-17Selectivity (mol. %)10099989
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OP-I-18According to GLC the main pr
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OP-I-19and slug dimensions, formati
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OP-I-20A RANS volume of fluids [1]
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OP-I-21the physical-chemical charac
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OP-I-22calculated values of pressur
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OP-I-23where L c - capillary length
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OP-I-24and diffuse transmission thr
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OP-I-25effect of bubble break-up wo
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OP-I-26strong influence on the soli
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OP-I-27wHCOOH=1+K2K1(1 + K3⋅ P⋅
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OP-I-28dimensional profiles detecte
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OP-I-29results. The results of the
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OP-I-30Fig. 1. Hydrodynamics and co
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OP-I-31Convection and diffusion wit
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TEMPERATURE RISE DURING REGENERATIO
Page 101 and 102: OP-II-2[4]. Similar temperature pro
Page 103 and 104: OP-II-3(Fig, 1 a, b) upon testing i
Page 105 and 106: OP-II-4In the second step optimizat
Page 107 and 108: OP-II-5membrane contactors were stu
Page 109 and 110: OP-II-6reaction over Cu/CeO 2-x cat
Page 111 and 112: OP-II-7is modelled by means of a tw
Page 113 and 114: OP-II-8the reactor [6]. However, th
Page 115 and 116: OP-II-9Figure 1. Computed volume fr
Page 117 and 118: OP-II-10assumes variables’ distri
Page 119 and 120: OP-II-11oxide support, it comes tha
Page 121 and 122: OP-II-12was connected to G.C. via s
Page 123 and 124: OP-II-13catalyst bed was 6 mm. Thre
Page 125 and 126: OP-II-14as coolant is an important
Page 127 and 128: OP-II-15Flow (L/h)7654321Bottoms ra
Page 129 and 130: OP-II-16(4) The gas recirculation r
Page 131 and 132: OP-II-17Catalytic reactions were ca
Page 133 and 134: OP-II-18At steady surface coverage
Page 135 and 136: OP-II-19gaimpulsegeneratorwateFig.
Page 137 and 138: OP-II-20examined (see Figure 1). Th
Page 139 and 140: OP-II-21References[1]. M.P. Dudukov
Page 141 and 142: OP-II-22of the hydrogen oxidation a
Page 143 and 144: OP-II-23TemperaturesensorsThe efflu
Page 145 and 146: OP-II-24of reactant conversions. Pa
Page 147 and 148: OP-II-25(surface) ‘wall-reaction
Page 149 and 150: OP-II-26It was found that the 10 wt
Page 151: OP-II-27non-flow type. During the M
Page 155 and 156: BUBBLING FLUIDISED BED PYROLYSIS OF
Page 157 and 158: PINEWOOD PYROLYSIS UNDER VACUUM CON
Page 159 and 160: OP-III-A-5PYROLYSIS OF HDPE IN A CO
Page 161 and 162: OP-III-A-6REACTORS FOR THE GREEN TR
Page 163 and 164: DEHYDRATION OF GLYCEROL TO ACROLEIN
Page 165 and 166: OP-III-A-8LACTIC ACID BASED ON BIO
Page 167 and 168: RECOVERY OF ACETIC ACID FROM PYROLY
Page 169 and 170: OP-III-A-10LIPASE-CATALYZED REACTIO
Page 171 and 172: OP-III-A-11INVESTIGATION ON THERMOC
Page 173 and 174: OP-III-A-12SELECTIVE CATALYTIC DEOX
Page 175 and 176: ETHANOL STEAM REFORMING OVER COBALT
Page 177 and 178: OP-III-A-14HYDROTREATMENT CATALYSTS
Page 179 and 180: ORAL PRESENTATIONSSECTION IIIChemic
Page 181 and 182: OP-III-B-1Reactor parameters:Intern
Page 183 and 184: OP-III-B-2JOINT STEAM REFORMING OF
Page 185 and 186: OP-III-B-3LANDFILL BIOGAS PURIFICAT
Page 187 and 188: OP-III-B-4MODELING AND SIMULATION O
Page 189 and 190: OP-III-B-5DemonstratorThe medium-te
Page 191 and 192: OP-III-B-630/19.6 Nl/min (space vel
Page 193 and 194: OP-III-B-7mixed in the ratios: 94,8
Page 195 and 196: OP-III-B-8Table 1.Material balance
Page 197 and 198: OP-III-B-9Based on the results of t
Page 199 and 200: OP-III-B-10On this basis it can be
Page 201 and 202: OP-III-B-11Similar trends caused by
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OP-III-B-12(mol/s g cat)x108r4,6-DM
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OP-III-B-13carbon in Wyoming coal i
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OP-III-B-14MODELING PRODUCT DISTRIB
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OP-III-B-15COMBINED TECHNOLOGY OF U
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MATEMATICAL MODEL FOR DOWNDRAFT BIO
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OP-III-B-17CATALYTIC DEHYDRATION OF
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OP-III-B-18SYNGAS AND HYDROGEN PROD
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POSTER PRESENTATIONSSECTION I
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PP-I-1influence of the direction of
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PP-I-2At the agitation of the liqui
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PP-I-3NOLINEAR PHENOMENA IN CATALYT
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PP-I-4A NEW APPROACH TO KINETIC STU
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PP-I-5KINETICS OF PROX REACTION OVE
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PP-I-6PHENOMENA OF SUPERADIABATIC T
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ELECTROMAGNETIC REACTOR OF WATER TR
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PP-I-8DIRECT SYNTHESIS OF HYDROGEN
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PP-I-9DYNAMICS OF FIRST-ORDER PHASE
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PP-I-10ELECTROCHEMICAL OXIDATION OF
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PP-I-11CHEMPAK SOFTWARE PACKAGE: OP
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PP-I-12COMPUTER SIMULATION OF ENDOT
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PP-I-13MODELLING KINETICS OF PROCES
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PP-I-14THE INVESTIGATION OF REACTIO
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PP-I-15The qualitative picture of s
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Thus, knowing the composition of ra
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PP-I-17current density. Preliminary
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PP-I-18Hydrogenation kinetics was d
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PP-I-19the active mixing, amplitude
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PP-I-20where r, h indicate the radi
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PP-I-21model is very anisotropic be
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PP-I-22- Reduction of the number of
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PP-I-23oscillations of intermediate
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PP-I-25SYNTHESIS OF ETHYLENE OXIDE
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PP-I-26OPTIMUM KINETICS FOR POLYSTY
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PP-I-27TableSpecific surface area (
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PP-I-28γ-preirradiated sample), th
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PP-I-29commercial CFD solver FLUENT
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PP-I-30modulus, a considerable decr
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PP-I-31The destruction ways of CF 3
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PP-I-32[7]. Karoor S, Sirkar K. Gas
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PP-I-33above 750°. The catalytic p
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PP-I-35REVERSE FLOW REACTOR WITH FO
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FLOW-RECIRCULATION METHOD FOR INVES
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TO A PROBLEM OF OPTIMIZATION OF FUN
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PP-I-38THE INFLUENCE OF REACTION MI
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PP-I-39METHANOL OXIDATIVE STEAM REF
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PP-I-41CORRECT INVESTIGATION OF THE
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PP-I-42NEW APPROACH OF DEFINITION O
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PP-I-43STREAM HEAT EXCHANGE OF AERO
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PP-I-44HIGH TEMPERATURE OXYGEN TRAN
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PP-I-45KINETICS OF TRANSESTERIFICAT
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MATHEMATICAL MODELING AND OPTIMIZAT
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PP-I-47The basic side reaction is r
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PP-I-49EXPERIMENTAL STUDY OF THE HA
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PP-I-51ON THE KINETICS AND REGULARI
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PP-I-52DIFFERENTIAL THERMAL ANALYSI
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PP-I-53oxidation reaction demonstra
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PP-I-54of reaction. It is establish
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PP-I-55effects, are energetically c
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PP-I-56The experiments and simulati
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PP-I-57In the studied range of temp
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PP-I-58HeadingsAdvances in Chemical
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PP-I-59calculated. During the aroma
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PP-I-60with honeycomb catalyst) act
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Т - temperature, K, D eff - effect
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PP-I-62stirring rate were adopted u
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PP-I-63m 2 = (k 1 y 0 1 +k -1 +k 1
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POSTER PRESENTATIONSSECTION II
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PP-II-1values of operating paramete
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⎡⎛⎢⎜bF⎣⎝=2ab ⎞ 6+ ⎟
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PP-II-4HONEYCOMB MONOLITHIC CATALYS
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MATHEMATICAL MODELING OF THE ALUMIN
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PP-II-6MODELING OF VINYL ACETATE SY
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PP-II-7СENTRIFUGAL DISK REACTORAvv
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PP-II-83) An opportunity of operati
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PP-II-10UV-ACTIVATION OF METHANE CO
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PP-II-11COMBINED APPROACH (FMEA- HA
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PP-II-12Testing the pilot variant o
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PP-II-14NOVEL MICROREACTOR FOR THE
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PP-II-15of 1-2.5 lead to a decreasi
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PP-II-16stages. Kinetic parameters
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PP-II-17whiskers, which assure an a
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PP-II-18с m , с cat - density of
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PP-II-19decrease. So, the potential
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PP-II-20products became a mixture o
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PP-II-21A numerical algorithm and s
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PP-II-22motions at any external con
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PP-II-23One of the main technologic
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PP-II-24100 m x 250 μm x 0.5 μm,
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PP-II-25A model was developed to ca
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PP-II-26The results of calculations
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PP-II-27modes of reaction and two d
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PP-II-29OZONE-DESTRUCTION REACTOR B
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PP-II-30Fig. 1. Axial profile of me
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PP-II-31isobutylene in butene fract
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PP-II-322.5x10 -3 ( i )2.5x10 -3 (
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PP-II-33No olefinreadsorptionWith o
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PP-II-34using titania or Ag-doped t
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PP-II-35accidents, is condition dep
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PP-II-36be seen that at temperature
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PP-II-37the solid phase solute conc
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PP-II-38As shown in Table 1, the ca
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PP-II-39better to the obtained in t
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PP-II-40Hydrodynamic regime in the
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PP-II-41activity, relative unit1,21
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PP-II-42One of the major indicators
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PP-II-43These conditions are confor
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PP-II-44For the hepten, alpha-methy
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PP-II-46PARTIAL OXIDATION OF METHAN
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PP-II-47DEVELOPMENT OF VORTEX APPAR
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MODELING OF CFTALYTIC α-OLEFINS OL
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PP-II-49Hinselwood kinetic equation
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3) iterate concentrations at a cut
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PP-II-51data such flow sheet provid
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PP-II-53ON THE TECNOLOGY OF TECHNIC
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PP-II-54PROPYLENE POLYMERIZATION AN
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REACTOR FOR LIQUID-PHASE PROCESSES
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PP-II-56MODELING OF CATALYTIC MICRO
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PP-II-57MATHEMATICAL MODELING OF BE
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PP-II-58HONEYCOMB CATALYSTS WITH PO
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POSTER PRESENTATIONSSECTION IIISECT
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ReferencesPP-III-1[1]. A.N. Pestrya
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PP-III-2Table1. Percentages of diff
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PP-III-3conversion for the reaction
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PP-III-4900Reformer temperature (K)
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PP-III-5Catalytic performance of th
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PP-III-6optimization permit better
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PP-III-8DE-NO X SYSTEM BASED ON H 2
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PP-III-9SEPARATION BETWEEN CHLORIDE
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CONVERSION OF WASTE COTTON TO BIOET
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PP-III-12THE METHOD OF GLYCERIC ACI
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NOx conversion vs. temperature is p
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PP-III-14intermetallic diffusion at
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PP-III-15The conversion of O 2 was
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PP-III-16H 2consumpition (a.u)(a)39
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PP-III-17the characteristic structu
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PP-III-18Figure 1. Influence of tem
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PP-III-19(a)(b)CH 4conversion, %100
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PP-III-20take into account own size
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PP-III-2110080CS-18CS-34CHZ30CHZ801
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EXPERIMENTALPP-III-22We synthesized
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PP-III-23Base composition component
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PP-III-25CO REMOVAL AT THE MICROSCA
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HYDROGEN PRODUCTION FROM METHANOL U
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PP-III-27NON CATALITIC PRODUCTION O
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PP-III-28Different reaction conditi
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PP-III-29followed by WGS reaction.
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PP-III-30As a solvent-coreactants w
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PP-III-31It was concluded that on t
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PP-III-32Hydrogenolysis of glycerol
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PP-III-331,6W 0, μmol Н 2/min1,20
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PP-III-34preparation (glass fiber f
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PP-III-35In the modification proces
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PP-III-36The kinetics of acid hydro
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PP-III-37reaction: i) C=O double bo
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PP-III-38methane and carbon monoxid
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PP-III-39from 25 to 60, which was d
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PP-III-401% w/w for Pd with respect
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PP-III-41material. Besides, the mol
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PP-III-43METHANOL AND DIMETHYL ETHE
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PP-III-44goal is attained by using
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OLIGOMERISATION OF TERTIARY AMINE L
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PP-III-47meter (Shimazu Co.; TOC-50
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PP-III-48the range of 29-87 kJ/mol
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PP-III-49determine the optimal type
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PP-III-50NEW CONCEPT FOR A SELF CLE
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PP-III-51HYDROGEN PRODUCTION BY MET
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PP-III-52CATALYTIC UPGRADING OF PRO
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PP-III-53CATALYTIC CONVERSION OF FI
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PROCESS FOR THE PRODUCTION OF BUTYL
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PP-III-55been previously fixed and
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PP-III-56The influence of reaction
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PP-III-57sample does not contain so
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PP-III-58The re-activation of the e
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PP-III-59The aim of this work is th
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PP-III-61BIODIESEL FROM MICROALGAE
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DEVELOPING MICROFLUIDIC DEVICE WITH
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THREE-PHASE DIRECT OILS HYDROGENATI
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Co-BASED CATALYSTS FOR THE HYDROLYS
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PP-III-65KINETIC STUDY OF THE CATAL
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PP-III-66PRODUCTION OF HYDROGEN AND
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PP-III-67ENHANCED GASIFICATION OF P
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PP-III-68INFLUENCE OF SPILLOVER ON
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PP-III-69AEROBIC OXIDATIVE COUPLING
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PP-III-70MECHANISMS FOR CHEMICAL RE
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PP-III-70SBS molecules and increase
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PP-III-71and as a resut, could enha
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PP-III-72conversion). Al 2 O 3 /PSS
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PP-III-73SBA50TiSBA% Transmittance5
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PP-III-74stove heating. Another par
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PP-III-75TG [%]0-10-20-30380°C400
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PP-III-76The elementary version of
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PP-III-77thermodynamically enhanced
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PP-III-78GFC textileStructuringmeta
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PP-III-79All the prepared spinel-ox
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PP-III-80Our new process is polluti
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PP-III-81Fig. 1. Scheme of the biog
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PP-III-82Pic. 1 Pic. 2Pic. 1. Schem
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ARKHIPOV Vladimir AfanasievichResea
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CENTENO Felipe OrlandoNúcleo de Ex
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FLID Mark RafailovichScientific Res
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HOSEN Mohammad AnwarUniversity of M
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KOZLOVA EkaterinaBoreskov Institute
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MAKARSHIN Lev LvovichBoreskov Insti
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ONSAN Zeynep IlsenDepartment of Che
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REBOLLAR MoisesInstituto De Investi
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SHEIKH Munir AhmedTraining and Staf
Page 615 and 616:
SULMAN Esfir MikhailovnaTver Techni
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ZHAPBASBYEV Uzak KairbekovichKazakh
Page 619 and 620:
OP-I-3 Pécar D., Gorsek A.COMPARIS
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OP-II-3Kucherov A.V., Finashina E.D
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OP-III-A-9 Rasrendra C.B., Girisuta
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PP-I-9Bykov V., Tsybenova S.B.DYNAM
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PP-I-43 Pechenegov Y.Y., Kuzmina R.
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PP-II-10 Basov N.L., Oreshkin I., T
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PP-II-45 Stepanek J., Koci P., Kubi
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PP-III-19 Fedorova Z.A., Danilova M
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PP-III-53 Pölczmann G., Valyon J.,
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XIX International Conference on Che
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