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Development of Karl Fischer Reagents

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[Examples <strong>of</strong> Measurement]<br />

(1) Volumetric titration<br />

<strong>Reagents</strong> used:<strong>Karl</strong> <strong>Fischer</strong> Reagent SS-Z (or SS)<br />

Dehydrated Solvent GEX (or MS) 25-50ml<br />

Substance<br />

Soil<br />

Dried soil<br />

Powdered quartz<br />

Substance<br />

Dehydrated<br />

solvents<br />

General-use<br />

"<br />

"<br />

Heating Temperature<br />

( � C)<br />

Sample Quantity<br />

(g)<br />

0.0508<br />

0.0858<br />

1.6711<br />

Sample Quantity<br />

(g)<br />

Chapter III: Applications - 2<br />

Measurement Value<br />

(mg)<br />

23.63<br />

04.21<br />

00.94<br />

Measurement Value<br />

(mg)<br />

Moisture Content<br />

(%)<br />

46.500<br />

04.910<br />

00.056<br />

(2) Moisture vaporization - Volumetric titration<br />

<strong>Reagents</strong> used: <strong>Karl</strong> <strong>Fischer</strong> Reagent SS-Z (or SS)<br />

Dehydrated Solvent GEX (or MS) + PG (3:1) 50-100ml<br />

Rocks<br />

Clay<br />

"<br />

Soil<br />

Iron ore<br />

Limestone<br />

Cement<br />

Ferrite<br />

Coal<br />

Amphibole<br />

Black mica<br />

Kaolin<br />

Talc<br />

Bentonite<br />

Manganese ore<br />

900<br />

110<br />

700<br />

200<br />

750<br />

700<br />

800<br />

200<br />

180<br />

1000<br />

1000<br />

800<br />

1000<br />

800<br />

750<br />

0.0798<br />

0.8837<br />

0.1033<br />

0.0483<br />

0.5638<br />

0.2462<br />

1.5555<br />

0.8967<br />

1.0022<br />

1.0283<br />

1.1005<br />

0.1414<br />

0.2003<br />

0.1135<br />

0.2313<br />

13.11<br />

34.46<br />

14.99<br />

22.88<br />

13.58<br />

0.84<br />

11.20<br />

9.20<br />

33.47<br />

16.04<br />

25.75<br />

19.94<br />

14.40<br />

18.61<br />

24.29<br />

Moisture Content<br />

(%)<br />

16.4<br />

03.90<br />

14.5<br />

47.2<br />

02.41<br />

00.34<br />

00.720<br />

01.03<br />

03.34<br />

01.56<br />

02.34<br />

14.1<br />

07.19<br />

16.4<br />

10.5<br />

187

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