Development of Karl Fischer Reagents
Development of Karl Fischer Reagents
Development of Karl Fischer Reagents
Create successful ePaper yourself
Turn your PDF publications into a flip-book with our unique Google optimized e-Paper software.
I-1. Questions & Answers about <strong>Karl</strong> <strong>Fischer</strong> <strong>Reagents</strong><br />
3. Notes to Official Food Additive List (7th ed., 1999)<br />
62<br />
Sorbitan sesquioleate 0.5% (1g)<br />
Propylene glycol 0.5% (2g)<br />
Polysorbate 80 3.0% (1g, back titration)<br />
Sodium lauryl sulfate 5.0% (0.5g)<br />
Polyvinyl pyrrolidone K25 5.0% (1.0g)<br />
Polyvinyl pyrrolidone K30 5.0% (1.0g)<br />
Polyvinyl pyrrolidone K90 5.0% (1.0g)<br />
Macrogol 400 1.0% (2g)<br />
Macrogol 1500 1.0% (2g)<br />
Macrogol 4000 1.0% (2g)<br />
Macrogol 6000 1.0% (2g)<br />
Berberine tannate 6.0% (0.7g)<br />
General Test Method 17: Moisture Content Test (<strong>Karl</strong> <strong>Fischer</strong> Method)<br />
The <strong>Karl</strong> <strong>Fischer</strong> method is stipulated for the following food additives.<br />
Item Tolerance<br />
5'-Inosinic acid sodium salt 29.0% or lower (0.15g, back titration)<br />
5'-Uridine acid sodium salt 26.0% or lower (0.15g, back titration)<br />
Citric acid (anhydrous) 0.5% or lower (2g)<br />
Disodium glycyrrhizate 13.0% or lower (0.2g, back titration)<br />
5'-Cytidine acid sodium salt 26.0% or lower (0.15g, back titration)<br />
Sucrose fatty acid ester 4.0% or lower (back titration)<br />
Sodium dehyroacetate 8.3-10.0% or lower (0.3g, back titration)<br />
Folic acid 8.5% or lower (0.2g, back titration)<br />
5'-Calcium ribonucleotide 23.0% or lower (0.15g, back titration)<br />
5'-Sodium ribonucleotide 27.0% or lower (0.15g, back titration)<br />
4. Japan Petroleum Institute Standards<br />
Test for water in liquid petroleum products (<strong>Karl</strong> <strong>Fischer</strong> Method)<br />
JPI-5S-14-76