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Development of Karl Fischer Reagents

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I-1. Questions & Answers about <strong>Karl</strong> <strong>Fischer</strong> <strong>Reagents</strong><br />

Characteristics <strong>of</strong> the Aquamicron Series<br />

When using the Aquamicron Series <strong>of</strong> electrolytes it is important to<br />

understand the following characteristics <strong>of</strong> the products.<br />

a) Very small quantities <strong>of</strong> water (about 10ug) can be measured<br />

accurately.<br />

b) Titration procedures are very simple.<br />

c) Measurements can be carried out quickly (1-10 minutes).<br />

d) It is not necessary to assess the titer <strong>of</strong> the reagent.<br />

e) The reagent can be used repeatedly.<br />

f) The composition <strong>of</strong> the solvents has been enhanced to make them<br />

suitable for immediate use with various samples. This eliminates the<br />

troublesome task <strong>of</strong> adding other solvents.<br />

1. General-Purpose Electrolytes<br />

The general-purpose Aquamicron Series <strong>of</strong> products are ideally constituted<br />

to facilitate <strong>Karl</strong> <strong>Fischer</strong> reactions with solvents, including methanol and<br />

propylene carbonate. Sample solubility is excellent, and even trace amounts<br />

<strong>of</strong> moisture can be extracted and titrated coulometrically with ease. These<br />

products also <strong>of</strong>fer superior reagent stability, which is the most important<br />

requirement when measuring minute amounts <strong>of</strong> water. This means that<br />

measurements can be taken with good reproducibility.<br />

The Aquamicron Series is suitable for a wide range <strong>of</strong> products including<br />

aromatics and other organic solvents, petroleum products, inorganic<br />

products and gas products.<br />

They are also the ideal reagents for the water vaporization method. A<br />

particularly convenient feature is the fact that they can be used immediately<br />

without the need to add other solvents. Aquamicron products have an<br />

excellent reputation for use in day-to-day moisture measurement for plastics<br />

and other solid samples.<br />

Product<br />

Pyridine-free, chlor<strong>of</strong>orm-free<br />

Type<br />

Packaging<br />

Aquamicron AX Anolyte<br />

500ml glass bottles<br />

Aquamicron CXU<br />

Pyridine-free<br />

Catholyle<br />

5ml ampoules (10 per case)<br />

Aquamicron AS Anolyte<br />

500ml glass bottles<br />

Aquamicron CXU Catholyle<br />

5ml ampoules (10 per case)<br />

34

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