Development of Karl Fischer Reagents
Development of Karl Fischer Reagents
Development of Karl Fischer Reagents
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I-1. Questions & Answers about <strong>Karl</strong> <strong>Fischer</strong> <strong>Reagents</strong><br />
Characteristics <strong>of</strong> the Aquamicron Series<br />
When using the Aquamicron Series <strong>of</strong> electrolytes it is important to<br />
understand the following characteristics <strong>of</strong> the products.<br />
a) Very small quantities <strong>of</strong> water (about 10ug) can be measured<br />
accurately.<br />
b) Titration procedures are very simple.<br />
c) Measurements can be carried out quickly (1-10 minutes).<br />
d) It is not necessary to assess the titer <strong>of</strong> the reagent.<br />
e) The reagent can be used repeatedly.<br />
f) The composition <strong>of</strong> the solvents has been enhanced to make them<br />
suitable for immediate use with various samples. This eliminates the<br />
troublesome task <strong>of</strong> adding other solvents.<br />
1. General-Purpose Electrolytes<br />
The general-purpose Aquamicron Series <strong>of</strong> products are ideally constituted<br />
to facilitate <strong>Karl</strong> <strong>Fischer</strong> reactions with solvents, including methanol and<br />
propylene carbonate. Sample solubility is excellent, and even trace amounts<br />
<strong>of</strong> moisture can be extracted and titrated coulometrically with ease. These<br />
products also <strong>of</strong>fer superior reagent stability, which is the most important<br />
requirement when measuring minute amounts <strong>of</strong> water. This means that<br />
measurements can be taken with good reproducibility.<br />
The Aquamicron Series is suitable for a wide range <strong>of</strong> products including<br />
aromatics and other organic solvents, petroleum products, inorganic<br />
products and gas products.<br />
They are also the ideal reagents for the water vaporization method. A<br />
particularly convenient feature is the fact that they can be used immediately<br />
without the need to add other solvents. Aquamicron products have an<br />
excellent reputation for use in day-to-day moisture measurement for plastics<br />
and other solid samples.<br />
Product<br />
Pyridine-free, chlor<strong>of</strong>orm-free<br />
Type<br />
Packaging<br />
Aquamicron AX Anolyte<br />
500ml glass bottles<br />
Aquamicron CXU<br />
Pyridine-free<br />
Catholyle<br />
5ml ampoules (10 per case)<br />
Aquamicron AS Anolyte<br />
500ml glass bottles<br />
Aquamicron CXU Catholyle<br />
5ml ampoules (10 per case)<br />
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