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Development of Karl Fischer Reagents

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I-1. Questions & Answers about <strong>Karl</strong> <strong>Fischer</strong> <strong>Reagents</strong><br />

2. <strong>Karl</strong> <strong>Fischer</strong> Reagent Products<br />

Q6<br />

22<br />

What volumetric titration reagents are available? Please explain<br />

the types <strong>of</strong> reagents and their uses, and the methods employed.<br />

Mitsubishi Chemical Corporation has a range <strong>of</strong> products to suit every<br />

purpose. Its products can be broadly divided into the following four<br />

categories.<br />

�Mitsubishi <strong>Karl</strong> <strong>Fischer</strong> <strong>Reagents</strong><br />

Titrant<br />

Can be used in various titer according to anticipated<br />

moisture content<br />

�Mitsubishi Dehydrated Solvents<br />

They are suitable as titration solvents for the <strong>Karl</strong> <strong>Fischer</strong><br />

reaction, to dissolve or disperse a sample in order to extract<br />

water.<br />

�Mitsubishi Standard Water Methanol<br />

This is used to determine the titer <strong>of</strong> a <strong>Karl</strong> <strong>Fischer</strong> reagent.<br />

The type used depends on the titer. Water methanol can also<br />

be used a titration agent for back titration.<br />

�Mitsubishi Standard Liquid<br />

This is used to determine the titer <strong>of</strong> a <strong>Karl</strong> <strong>Fischer</strong> reagent.<br />

<strong>Karl</strong> <strong>Fischer</strong> reagents and dehydrated solvents have traditionally been<br />

available in both pyridine types and pyridine-free types, which do not have<br />

the pyridine odor. There is no significant difference in performance between<br />

the two types, and they can be used interchangeably.

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