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Development of Karl Fischer Reagents

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5. Japan LPG Association Standards<br />

Chapter I: Basic Knowledge<br />

Moisture Content Test Method in LPG: <strong>Karl</strong> <strong>Fischer</strong> Method<br />

JLPGA-S-02-99<br />

6. Japan Agricultural Standards (JAS)<br />

Vegetable Oils (<strong>Karl</strong> <strong>Fischer</strong> Method, moisture content 0.2% or lower) (1969)<br />

Q15<br />

Please provide some examples <strong>of</strong> the international standards (ISO) and foreign<br />

standards that have been adopted for the <strong>Karl</strong> <strong>Fischer</strong> titration method.<br />

Listed below are some examples <strong>of</strong> standards established by the<br />

International Organization for Standardization (ISO) and the American<br />

Society For Testing and Materials. The BS (U.K.) and DIN (Germany)<br />

systems are also based on these standards.<br />

1. General Testing Methods<br />

(1) Volumetric titration<br />

ISO 760-1978<br />

Determination <strong>of</strong> water - <strong>Karl</strong> <strong>Fischer</strong> method (General method)<br />

ASTM E203-01<br />

Water using <strong>Karl</strong> <strong>Fischer</strong> reagent<br />

(2) Coulometric titration<br />

ASTM E1064-92<br />

Water in organic liquids by coulometric <strong>Karl</strong> <strong>Fischer</strong> titration<br />

2. Individual Standards<br />

ASTM D1364-95<br />

Water in volatile solvents (<strong>Fischer</strong> reagent titration method)<br />

ASTM D1533-96<br />

Water in insulating liquids (<strong>Karl</strong> <strong>Fischer</strong> reaction method)<br />

ASTM D1631-94<br />

Water in phenol and related materials by the iodine reagent method<br />

ASTM D1744-92<br />

Water in liquid petroleum products by <strong>Karl</strong> <strong>Fischer</strong> reagent<br />

ASTM D3277-95<br />

Moisture content <strong>of</strong> oil-impregnated cellulosic insulation<br />

ASTM D3466-85<br />

Water content <strong>of</strong> trichlorotrifluoroethane<br />

63

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