Inhaltsverzeichnis - Anorganische Chemie
Inhaltsverzeichnis - Anorganische Chemie
Inhaltsverzeichnis - Anorganische Chemie
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81<br />
Table 38: Crystal data and data collection<br />
Empirical formula Cl 6 Hg 2 N 6 S 4<br />
Formula weight 826.20<br />
Crystal size<br />
Crystal color and habit<br />
Crystal system<br />
Space group<br />
0.20 x 0.04 x 0.035 mm<br />
light yellow rod<br />
triclinic<br />
P1<br />
Unit cell dimensions a = 6.00860(10) Å α = 105.0320(11)°<br />
b = 8.2445(2) Å β = 99.2003(11) °<br />
c = 9.2830(2) Å γ = 106.4211(14)°<br />
Volume 412.289(15) Å 3<br />
Z 1<br />
Density (calculated) 3.328 Mg/m 3<br />
Absorption coefficient 20.062 mm -1<br />
F(000) 368<br />
Diffractometer used<br />
Nonius Kappa CCD<br />
Radiation and wavelength MoK with λ=0.71073 Å<br />
Scan type<br />
Temperature<br />
Hemisphere<br />
200(2) K<br />
2 θ range for data collection 2.55 to 27.49°<br />
Index ranges -7 h 7 -10 k 10 -12 l 12<br />
Reflections collected 7569<br />
Independent reflections 1881 (R int = 0.0581 )<br />
Observed reflections<br />
Absorption correction<br />
177 (F>4σ(F))<br />
SADABS<br />
Max. and min. transmission 0.1329 and 0.5646<br />
Experimental details :<br />
1200 frames measured in phi (0-360) with chi=0 and omega=2theta=25<br />
65 frames measured in omega (15-35) with chi=280, 2theta=29 and phi=0<br />
Crystal mounted in perfluorpolyetheroil
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