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universidade de são paulo - Faculdade de Odontologia - Unesp

universidade de são paulo - Faculdade de Odontologia - Unesp

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34<br />

respectively. The flasks were separated, the silicone patterns were removed, and<br />

the stone surfaces were painted with a separating medium (Vipi Film - VIPI<br />

Indústria e Comércio Exportação e Importação <strong>de</strong> Produtos Odontológicos Ltda<br />

Pirassununga, SP, Brazil). For each specimen, 1 g of pow<strong>de</strong>r and 0.47 mL of<br />

monomer liquid were mixed and processed according to the manufacturer’s<br />

instructions. The mixture was packed into the molds, a trial pack was completed,<br />

and excess material was removed. A final pack was performed and held for 15<br />

minutes. The <strong>de</strong>nture base acrylic resin was processed in a 500 W domestic<br />

microwave oven (Brastemp – Brastemp da Amazonia SA, Manaus, AM, Brazil)<br />

for 20 minutes at 20% power, followed by 5 minutes at 90% power. The flasks<br />

were allowed to bench cool at room temperature, the specimens were <strong>de</strong>flasked,<br />

and excess flash was aseptically removed with a sterile bur (Maxi-Cut; Lesfils <strong>de</strong><br />

August Malleifer SA, Ballaigues, Switzerland).<br />

Surface Roughness Measurements<br />

The surface roughness of all specimens was measured with a profilometer<br />

(Mitutoyo SJ 400 – Mitutoyo Corporation - Japan). Three measurements were<br />

ma<strong>de</strong> for each specimen and the average reading was <strong>de</strong>signated as the Ra (μm)<br />

value of that specimen. Resolution was 0.01 μm, interval (cutoff length) was 0.8<br />

mm, transverse length was 2.4 mm, the stylus speed was 0.5 mm/s, and the<br />

diamond stylus tip radius was 5 μm. All measurements were recor<strong>de</strong>d by one<br />

operator.

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