universidade de são paulo - Faculdade de Odontologia - Unesp
universidade de são paulo - Faculdade de Odontologia - Unesp
universidade de são paulo - Faculdade de Odontologia - Unesp
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93<br />
minutes. The <strong>de</strong>nture base acrylic resin was processed in a 500 W domestic<br />
microwave oven (Brastemp – Brastemp Amazonia SA, Manaus, AM, Brazil) for<br />
20 minutes at 20% power, followed by 5 minutes at 90% power. The flasks were<br />
allowed to bench cool at room temperature, the specimens were <strong>de</strong>flasked, and<br />
excess flash was aseptically removed with a sterile bur (Maxi-Cut; Lesfils <strong>de</strong><br />
August Malleifer SA, Ballaigues, Switzerland).<br />
Surface roughness measurements<br />
The surface roughness of all specimens was measured with a profilometer<br />
(Mitutoyo SJ 400 – Mitutoyo Corporation – Tokyo, Japan). Four measurements<br />
were ma<strong>de</strong> for each specimen and the average reading was <strong>de</strong>signated as the Ra<br />
(μm) value of that specimen. Resolution was 0.01 μm, interval (cutoff length) was<br />
0.8 mm, transverse length was 2.4 mm, the stylus speed was 0.5 mm/s, and the<br />
diamond stylus tip radius was 5 μm. All measurements were recor<strong>de</strong>d by one<br />
operator.<br />
Plasma treatments<br />
After roughness measurements, the specimens were cleaned in ultrasonic<br />
water and <strong>de</strong>tergent bath for 15 minutes, then sonicated in distilled water for 15<br />
minutes and dried in air. The specimens were then divi<strong>de</strong>d into three groups, each<br />
one including 18 specimens. In the control group, the specimens were left<br />
untreated. For the two experimental groups, both specimen surfaces were exposed<br />
to generated plasmas using the following conditions: argon atmosphere at 50 W<br />
(group Ar/50 W); atmospheric air at 130 W (AAt/130 W). The plasma exposure