Introduction to Soil Chemistry

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x contents 7.5. Extract Cleanup 139 7.6. Extract Analysis 142 7.7. Conclusions 142 Problems 143 Bibliography 143 References 144 CHAPTER 8 SPECTROSCOPY 147 8.1. Spectral Overlap 148 8.2. Noise 149 8.3. X-ray Diffraction 149 8.4. X-ray Fluorescence 150 8.5. Atomic Spectroscopy 152 8.6. Ultraviolet and Visible Spectroscopy 156 8.7. The Visible Region 158 8.8. Color Measurement: The Spectrophotometer 159 8.9. Regression Analysis 161 8.10. Relationship to Original Sample 163 8.11. Infrared Spectroscopy 163 8.12. Nuclear Magnetic Resonance 167 8.13. Mass Spectroscopy 169 8.14. Conclusion 170 Problems 170 Bibliography 171 References 171 CHAPTER 9 CHROMATOGRAPHY 175 9.1. Fundamentals of Chromatography 175 9.2. Gas Chromatography 176 9.3. High-Performance Liquid Chromatography 184 9.4. Thin-Layer Chromatography 186 9.5. Electrophoresis 9.6. Identification of Compounds Separated by Chromatographic 188 Procedures 189 9.7. Quantification 191 9.8. Conclusion 191 Problems 192 Bibliography 192 References 193
contents xi CHAPTER 10 SPECIATION 195 10.1. Cations 198 10.2. Anions 202 10.3. Nitrogen 204 10.4. Phosphorus 205 10.5. Sampling, Sample Storage, and Speciation 206 10.6. Conclusions 207 Problems 208 Bibliography 208 References 209 INDEX 211
Page 1: Introduction to Soil Chemistry Anal
Page 4 and 5: CHEMICAL ANALYSIS A SERIES OF MONOG
Page 6 and 7: Copyright © 2005 by John Wiley & S
Page 9 and 10: CONTENTS PREFACE xiii CHAPTER 1 SOI
Page 11: contents ix 4.14. Conclusion 89 Pro
Page 16 and 17: xiv preface Moisture levels can cha
Page 19 and 20: CHAPTER 1 SOIL BASICS I MACROSCALE
Page 21 and 22: soil basics i 3 Mollisol Ap 0 - 17.
Page 23 and 24: soil basic i 5 Spodosol Oi 0 - 2.5
Page 25 and 26: horizonation 7 or basic.Thus, the t
Page 27 and 28: horizonation 9 Table 1.2. Major-Min
Page 29 and 30: peds 11 As would be expected, only
Page 31 and 32: peds 13 Figure 1.7. Peds isolated f
Page 33 and 34: P soil color 15 B P = pores B = bri
Page 35 and 36: soil naming 17 Under most condition
Page 37 and 38: soil chemistry, analysis, and instr
Page 39 and 40: ibliography 21 thus increased oxida
Page 41 and 42: CHAPTER 2 SOIL BASICS II MICROSCOPI
Page 43 and 44: O O Si O O d - d H H + d + O soil s
Page 45 and 46: d - Si O O O Al O O H d+ O O HO OH
Page 47 and 48: O HO O O O HO O O Si O Al O Si O O
Page 49 and 50: soil solids 31 the name taken from
Page 51 and 52: onding considerations 33 The two op
Page 53 and 54: surface features 35 Because differe
Page 55 and 56: energy considerations 37 side-by-si
Page 57 and 58: In Figure 2.5 the path to the right
Page 59 and 60: H O H H O C Na +- O O H H O H H O H
Page 61 and 62: eferences 43 2.7. Explain how the r
Page 63 and 64:
CHAPTER 3 SOIL BASICS III THE BIOLO
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animals 47 C Figure 3.2. An ant col
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plants 49 Grasses and other similar
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plants 51 Rhizosphere Figure 3.4. I
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microorganisms 53 Table 3.1. Design
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microorganisms 55 microaerophilic,
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ioorganic 57 activity may be increa
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organic compounds 59 and may contai
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organic compounds 61 Table 3.3. Fun
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R 2C R organic compounds 63 O C - O
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analysis 65 3.7.1. Analysis for Ani
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problems 67 oxide by components in
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eferences 69 6. Bais HP, Park S-W,
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CHAPTER 4 SOIL BASICS IV THE SOIL A
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water 73 The soil atmosphere also c
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D C water 75 B Figure 4.3. A wide-d
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compounds in solution 77 tion is li
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+ NH4 + NH4 H H O + NH4 H H H + NH
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organic ions in solution 81 consequ
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distribution between soil solids an
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oxidative and reductive reactions i
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measuring soil water 87 soil is rep
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problems 89 blocks, and thermocoupl
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eferences 91 8. Bohn HL, McNeal BL,
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94 electrical measurements Figure 5
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96 electrical measurements 1200 100
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98 electrical measurements Referenc
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100 electrical measurements Standar
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102 Table 5.1. Ion-Selective Electr
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104 electrical measurements In addi
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106 electrical measurements along w
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108 electrical measurements cools w
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110 electrical measurements Science
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112 titrimetric measurement pH 13 1
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114 titrimetric measurement Table 6
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116 titrimetric measurement H 3 O +
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118 titrimetric measurement Because
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120 titrimetric measurement Soil Sa
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122 titrimetric measurement 6.6. NI
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124 titrimetric measurement - + X +
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126 titrimetric measurement REFEREN
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128 extraction Organic compounds, i
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130 extraction 3. What is the distr
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132 extraction All nonaqueous solve
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134 extraction Table 7.2. Character
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136 extraction Figure 7.3. Solution
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138 extraction Figure 7.5. A microw
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140 extraction serious interference
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142 extraction taining one to sever
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144 extraction Cohen DR, Shen XC, D
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146 extraction ultrasound; Applicat
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148 spectroscopy although technical
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150 spectroscopy Incident X-rays q
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152 spectroscopy with cellulose or
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154 spectroscopy extract components
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156 spectroscopy 8.6. ULTRAVIOLET A
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158 spectroscopy placed in the samp
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160 spectroscopy to scratch them. W
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162 spectroscopy Data Concentration
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164 spectroscopy these make analysi
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166 spectroscopy Table 8.1. Importa
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168 spectroscopy nance (NMR) spectr
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170 spectroscopy nitrogen containin
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172 spectroscopy 7. Bernick MB, Get
Page 193 and 194:
CHAPTER 9 CHROMATOGRAPHY Chromatogr
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Mobile phase in abaybayby abaybayby
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gas chromatography 179 Figure 9.3.
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gas chromatography 181 Table 9.3. C
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gas chromatography 183 Gas tight sy
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high-performance liquid chromatogra
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thin-layer chromatography 187 They
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alization of components on a thin-l
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conclusion 191 then a pure sample o
Page 211:
eferences 193 U.S. Environmental Pr
Page 214 and 215:
196 speciation - Al H 2 O K H2O H2O
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198 speciation to consider all poss
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200 speciation many more species th
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202 speciation atomic absorption is
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204 speciation Table 10.2. Common O
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206 speciation reflecting the titra
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208 speciation Some oxyanions are s
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210 speciation 13. Wang J, Ashley K
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212 index Bioreactor, 124 Bioremedi
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214 index Gas chromatograph-mass sp
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216 index Path length, 159 Ped(s),
Page 236 and 237:
218 index TMS, see Tetramethylsilan
Page 238 and 239:
Vol. 34. Neutron Activation Analysi
Page 240 and 241:
Vol. 117 Applications of Fluorescen
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Introduction to Soil Chemistry

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