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ECOPROBE 5 - rs dynamics

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11.2 PID SINGLE POINT CALIBRATION PROCEDURE (Figs. 17.1 to 17.5)<br />

� In case you calibrate the PID analyzer for the fi<strong>rs</strong>t time, you<br />

have to unscrew the sealing cap from the cylinder and fit the<br />

calibration valve.<br />

� The concentration of the calibration gas in the cylinder may<br />

not be exactly 100 ppm as it may vary +/-10%. The actual<br />

value is written on the cylinder certificate.In our case the<br />

concentration was 104 ppm. About 1 liter of gas is enough to<br />

complete the calibration.<br />

� Prepare a short length of plastic tubing to connect the<br />

calibration bag to the instrument.<br />

� Create a new locality for calibration (for instance CALIB.lc)<br />

using the LOCALITY MANAGEMENT item in the Main Menu<br />

(Window W2). Make sure that the configuration file of the<br />

CALIB.lc locality is set up properly. If you need to calibrate<br />

Standard mode, PID must be set on Standard, calibration gas<br />

on Isobutene, units on ppm. Other paramete<strong>rs</strong> such as pump<br />

speed, etc. should be set to the same values as you will use<br />

for measuring in the field.<br />

� Return to the Main Menu and select LOCALITY 1 (or 2)<br />

CALIB to open its measuring mode. Let the instrument<br />

measure several points to allow it to stabilize. The next point<br />

will be used for the calibration measurement.<br />

� Fill the calibration bag from the gas cylinder and immediately close<br />

the valves on the cylinder and on the bag. For easier operation, the<br />

bag’s plastic tube can be sealed with your thumb.<br />

� Start the measuring cycle: After the resetting period, use the short<br />

plastic tube to connect the bag to <strong>ECOPROBE</strong> 5 with minimum<br />

delay, and open the valve on the bag. Press the right arrow on the<br />

instrument handle to confirm the option “Press” on the screen to start<br />

the measuring.<br />

Fig.17.1–<br />

Calibration valve<br />

on gas cylinder.<br />

Fig.17.2 –<br />

Calibration bag.<br />

Fig.17.4 – Calibration bag connected.<br />

CALIBRATION<br />

Fig.17.5 – Calibrating.<br />

� Keep the bag connected until the instrument<br />

stops measuring.<br />

50<br />

Fig.17.3 –<br />

Calibration bag.

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