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2009 APPLIED SUPERCONDUCTIVITYMagnetic field behaviour of ex-situ processed MgB 2 multifilam<strong>en</strong>tary wiresIn order to make MgB 2 useful not only for dc but also for acapplications further conductor developm<strong>en</strong>t and optimizationare still needed, in particular to reduce the ac lossescaused by magnetic hysteresis in the MgB 2 core, filam<strong>en</strong>tcoupling and eddy curr<strong>en</strong>ts flowing through the metallicmatrix. In this context research work should be focused onmultifilam<strong>en</strong>tary strands with a large number of very finefilam<strong>en</strong>ts, twisted filam<strong>en</strong>ts and non-magnetic and high resistivitysheath.We have focused our work on obtaining multifilam<strong>en</strong>taryconductors with a large number of very fine filam<strong>en</strong>ts. Inthis context, the powder’s granulometry can play a crucialrole. In this experim<strong>en</strong>t we have prepared two MgB 2 startingpowders which are either not milled (NM) or milled(M) with differ<strong>en</strong>t granulometries (NM= 1.5 µm and M=450 nm) and by the ex-situ powder in tube (PIT) methodwe have realized multifilam<strong>en</strong>tary wires with 19, 91 and361 filam<strong>en</strong>ts and an average size of each filam<strong>en</strong>t of 279,110 and 30 µm respectively. In figure 143 the cross sectionsof the three wire types are shown.We have studied the relationship betwe<strong>en</strong> grain and filam<strong>en</strong>tsize in terms of transport properties. The measuredcritical curr<strong>en</strong>t d<strong>en</strong>sities (J C ) for the samples with NM powderand M powder are reported in figure 144. The criticalcurr<strong>en</strong>t d<strong>en</strong>sity improves with milling for all samples asreported in our previous work [A. Malagoli et al J. Appl.Phys. 104, 103908 (2008)]. Focusing on the behaviour ofthe not milled samples, passing from 19 to 91 filam<strong>en</strong>ts aremarkable critical curr<strong>en</strong>t d<strong>en</strong>sity degradation is evid<strong>en</strong>t,that is partially recovered going to 361 filam<strong>en</strong>ts. On thecontrary for the milled samples 19M and 91M have almostid<strong>en</strong>tical critical curr<strong>en</strong>t d<strong>en</strong>sity - a slightly better behaviourin field being observed in 91M. Wh<strong>en</strong> the number of filam<strong>en</strong>tsincreases up to 361, critical curr<strong>en</strong>t d<strong>en</strong>sity decreasesstaying though above the 361NM.Such a behaviour of the critical curr<strong>en</strong>t d<strong>en</strong>sity in field cannotbe explained or well understood simply considering theeffects of milling. In these complex conductors several factorshave to be tak<strong>en</strong> into account which have an effect onthe transport properties: the starting granulometry of theMgB 2 powders, the cold deformation force and the final filam<strong>en</strong>tsize. Therefore, in the final analysis, the capabilityof these conductors to transport high critical curr<strong>en</strong>ts cruciallydep<strong>en</strong>ds on a proper balance of these parameters. Inthis work we have obtained the best ratio filam<strong>en</strong>t size/grainsize on a 91 filam<strong>en</strong>ts wire with an average filam<strong>en</strong>t size ofabout 110 µm and a powder starting average grain diameterof about 450 nm. A finer MgB 2 granulometry seems to b<strong>en</strong>eeded to realize very thin filam<strong>en</strong>ts (10−30 µm) with highcritical curr<strong>en</strong>t d<strong>en</strong>sity.Figure 143: Images of differ<strong>en</strong>t cross sections through the wireswith 19, 91 and 361 filam<strong>en</strong>ts respectively.Figure 144: Transport critical curr<strong>en</strong>t d<strong>en</strong>sity (J C ) for differ<strong>en</strong>tmilled (M) and not milled (NM) samples measured up to magneticfields of 13 T using a wide bore resistive magnet and a Heliumbath cryostat (T = 4.2 K).E. MossangA. Malagoli, G. Romano, M. Vignolo, C. Ferdeghini, M. Putti (CNR-INFM LAMIA, G<strong>en</strong>ova, Italy), S. Brisigotti, G.Grasso, A. Tumino (Columbus Superconductors S.p.A., G<strong>en</strong>ova, Italy)101

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