2009 MAGNET DEVELOPMENT AND INSTRUMENTATIONPulsed high-field coilsThe production of user coilsAlso in 2009 the copper-zylon coils remain the workhorseof the laboratory. The production of these coils has nowbecome standard; parts are parameterized and can be producedin 2 weeks on the computerized milling machine,the actual winding takes less than a week and testing a fewdays. Since most of the time parts are in stock and at least4 members of the team have the experi<strong>en</strong>ce to wind a coil,a standard coil can be produced in 10 days. Moreover, thepolicy is to have at least one standard coil in stock, in orderto avoid as far as possible any delay for users after a(finally unavoidable) coil failure. A first glidcop zylon coilwas tested up to 72 T and is now available for users duringthe time the 1 MJ transportable g<strong>en</strong>erator is available.Giv<strong>en</strong> the success of this small-volume, short-pulse prototype,we have constructed a longer pulse (t max = 33 ms,t total = 200 ms ) 72 T coil which can be <strong>en</strong>ergized by the14 MJ g<strong>en</strong>erator. This magnet has be<strong>en</strong> successfully testedand is now available to users on a perman<strong>en</strong>t basis.Figure 168:XXL coilSpecial coilsIn 2009 a special coil for optical experim<strong>en</strong>ts (BMV) wasdeveloped and successfully tested in house and to the highestfield at our colleagues in Dresd<strong>en</strong>. This coil (nicknamedXXL - see figure 168) is an up-scaled version of the X-coil. This coil produced 300 T 2 .m and is an improvem<strong>en</strong>tof 1100% compared to the former X-coils. The split coil,specially <strong>des</strong>igned for synchrotron X-ray experim<strong>en</strong>ts, wasfinally tested inside its cryostat after some problems due tothe complicated integration of the coil-body with the liquidnitrog<strong>en</strong> cryostat. Last, but not least, a mini-coil madefrom Cu-stainless wire was produced by Jérome Béard andhe was able to break with this coil (used as an insert in astandard 60 T coil) the record field of the Toulouse laboratorythat now stands at 81 T. This test was partly made tovalidate our multi-coil <strong>des</strong>ign code that was used to <strong>des</strong>igna large two-coil magnet (ARMS4).Technical developm<strong>en</strong>tsMost of the time in coil winding is sp<strong>en</strong>t on applying thezylon reinforcem<strong>en</strong>t, therefore we decided to improve thezylon spinhead by making it more reliable (new frictionbrakes) and easier to maintain (the spinhead modules canbe exchanged in 2 minutes, to be cleaned and maintained).Since the main progress in coil performance has to comefrom progress in materials it is of utmost importance tostudy the materials used in coil construction under realisticconditions (cryog<strong>en</strong>ic temperature and high mechanicalloads). To test the effici<strong>en</strong>cy of the fibre reinforcem<strong>en</strong>t wedecided to continue the explo-vessel studies (as first developedin at the Universiteit van Amsterdam). Unfortunatelyonce the setup was running (using the high-pressure rig atthe Clar<strong>en</strong>don Laboratory in Oxford) and 30 pressure vesselshad be<strong>en</strong> produced, it turned out that this installationwas not longer available to us due to changing priorities inOxford. Another high-pressure rig was id<strong>en</strong>tified in Franceand we expect to restart the explo-vessel tests before the<strong>en</strong>d of the year. These tests will be used to determine forthe first time the properties of zylon reinforcem<strong>en</strong>t underrealistic conditions, study the influ<strong>en</strong>ce of various impregnatesand impregnation methods, and last but not least toinvestigate other high-str<strong>en</strong>gth fibres that could be used as afall back solution in case zylon would not be available anymore.Apart from the mechanical str<strong>en</strong>gth of the conductorand the fibre reinforcem<strong>en</strong>t the quality of the isolation underhigh mechanical load at cryog<strong>en</strong>ic temperature is of greatimportance to have coils with a long lifetime. In order totest various types of insulations we developed an isolationtest on wires applying realistic loads to the isolation. Thisinstallation has started to work and the first results will beavailable before the <strong>en</strong>d of the year.OutlookThe success of pulsed fields combined with large-scale neutronand X-ray sources has created a demand for more timeat high magnetic fields per 24 hour period. This will be realizedby improving the duty cycle of the coils by increasingthe pulse duration (to prolong lifetime) combined with a reductionof the cool down time. Some test with liquid nitrog<strong>en</strong>based on techniques used up to now in dc fields lookedvery promising (cool down times of only a few minutes). Itis likely that by implem<strong>en</strong>ting these techniques in our coilswe can gain at least a factor of t<strong>en</strong> in the duty cycle.J. Béard, J. Billette, P. Frings, F. Giquel , J.-M. Lagarrigue, J. Mauchain119
MAGNET DEVELOPMENT AND INSTRUMENTATION 2009High str<strong>en</strong>gth conductors for pulsed magnetsR&D of high str<strong>en</strong>gth composite conductors- for B > 80 T in the coilin/coilex system: the developm<strong>en</strong>tof Cu/SS wires, for the coilin, with 60% of stainless steel(UTS(77 K)>1550 MPa) and a cross section of 2.00×1.25mm 2 allowed us to reach 81 Tesla (the LNCMI record) inspring 2009.- Cu alloys for magnets with optimized curr<strong>en</strong>t distribution:conductors made of copper alloys like GlidCop(CuAl 2 O 3 ) or CuAg (with low silver cont<strong>en</strong>t 0.08%) havebe<strong>en</strong> processed by industrial companies to be combinedwith Zylon fibers in the user’s magnet with optimized reinforcem<strong>en</strong>tdistribution.Ultra-high str<strong>en</strong>gth nanocomposite Cu/Nb conductorsThe developm<strong>en</strong>t of reinforced conductors, with high electricalconductivity and high str<strong>en</strong>gth, is ess<strong>en</strong>tial to provid<strong>en</strong>on-<strong>des</strong>tructive high pulsed magnetic fields over 80 Tesla:the best compromise is obtained with copper-based continuousnanofilam<strong>en</strong>tary wires (UTS = 2 GPa and ρ =0.6 µΩcm at 77 K). The fabrication process of thes<strong>en</strong>anocomposite wires is based on severe plastic deformation(SPD) applied by accumulative drawing and bundling,leading to a multi-scale copper matrix containing up toN = 85 4 (∼ 50×10 6 ) continuous and parallel niobium nanotubes[Vidal et al., Scripta Mat., 60, 171 (2009)].In 2007, the extrusion of the nanocomposite conductorshas be<strong>en</strong> stopped at the “C<strong>en</strong>tre de Recherche” of TRE-FIMETAUX because of its closure. We decided to pursueour developm<strong>en</strong>t in collaboration with the CEA/LTMEX inSaclay where a 575 tons extrusion press is available.Developm<strong>en</strong>t of a new co-axial CuNbCuNb nanocompositewiresA new nanocomposite structure has be<strong>en</strong> <strong>des</strong>igned with asuperposition of Nb and Cu nanotubes (figure 169). Weadded nanometric phases remembering that the extraordinarystr<strong>en</strong>gth<strong>en</strong>ing of the co-cylindrical structure is relatedto: (i) an increase of Cu-Nb interfaces surface acting asdislocations barriers; (ii) a rapid and controlled access tonanometre scale where size effect operates on the plasticitymechanisms; (iii) the contribution of an additional reinforcingphase: the Cu-f nanofibers embedded in the Nbnanotubes behave as whiskers with strong size dep<strong>en</strong>d<strong>en</strong>ce.A conductor containing 85 3 Nb nanowhiskers, Cu nanotubesand Nb nanotubes, embedded in a copper matrixhas be<strong>en</strong> obtained. This Cu/Nb/Cu/Nb system is thereforemore effici<strong>en</strong>t than Cu/Nb filam<strong>en</strong>tary and Cu/Nb/Cu cocylindricalsystems for high-str<strong>en</strong>gth applications in magnets(figure 170): it exhibits a controlled microstructureand an effici<strong>en</strong>t str<strong>en</strong>gth<strong>en</strong>ing in the nanocomposite zones,where size and also geometry play major roles.Figure 169: Co-axial conductors: (a) N = 85; (b) N = 85 3 .Figure 170: Ultimate t<strong>en</strong>sile str<strong>en</strong>gth of co-axial CuNbCuNb andco-cylindrical CuNbCu nanocomposite wires versus diameter.The improvem<strong>en</strong>t of the drawing conditions led us to applythe same procedure for the optimization of the extrusionconditions. In the framework of the NANOFILMAGproject, funded by the ANR and involving the PHYMAT,two CEA laboratories (DAPNIA, LTMEX), and an industrialpartner (Alstom/MSA), a program has be<strong>en</strong> defined tooptimize the extrusion conditions. The aim is the prev<strong>en</strong>tionof fractures during the extrusion step of the ADB processand the scale-up of the size of the nanocomposite billets.A Ph.D stud<strong>en</strong>t, J.B Dubois, is involved in the projectand shares his activity betwe<strong>en</strong> LNCMI and PHYMAT.In addition, in-situ neutron diffraction (POLDI-PSI) and exsitulaboratory x-ray diffraction experim<strong>en</strong>ts (PHYMAT-Poitiers, ESRF) have be<strong>en</strong> performed for differ<strong>en</strong>t heattreatm<strong>en</strong>ts to study the formation of the texture. Textureand microstructure in the copper after heat treatm<strong>en</strong>tspres<strong>en</strong>t radical differ<strong>en</strong>ces dep<strong>en</strong>ding on the size of the consideredcopper channels [to be published].F. Lecouturier, N. Ferreira, L. B<strong>en</strong>dichou, J.M. Lagarrigue, J.B. DuboisL. Thilly, P.O R<strong>en</strong>ault (PHYMAT, Poitiers, France), H. van Swyg<strong>en</strong>hov<strong>en</strong>, S. van Petegem (POLDI-Paul ScherrerInstitut, Switzerland), P. Olier (CEA-DEN-LTMEX, Saclay, France), C. Berriaud (CEA-IRFU-SACM, Saclay)120
- Page 1 and 2:
LABORATOIRE NATIONAL DES CHAMPS MAG
- Page 4 and 5:
TABLE OF CONTENTSPreface 1Carbon Al
- Page 6 and 7:
Coexistence of closed orbit and qua
- Page 8:
2009PrefaceDear Reader,You have bef
- Page 12 and 13:
2009 CARBON ALLOTROPESInvestigation
- Page 14 and 15:
2009 CARBON ALLOTROPESPropagative L
- Page 16 and 17:
2009 CARBON ALLOTROPESEdge fingerpr
- Page 18 and 19:
2009 CARBON ALLOTROPESObservation o
- Page 20 and 21:
2009 CARBON ALLOTROPESImproving gra
- Page 22 and 23:
2009 CARBON ALLOTROPESHow perfect c
- Page 24 and 25:
2009 CARBON ALLOTROPESTuning the el
- Page 26 and 27:
2009 CARBON ALLOTROPESElectric fiel
- Page 28 and 29:
2009 CARBON ALLOTROPESMagnetotransp
- Page 30 and 31:
2009 CARBON ALLOTROPESGraphite from
- Page 32:
2009Two-Dimensional Electron Gas25
- Page 35 and 36:
TWO-DIMENSIONAL ELECTRON GAS 2009Di
- Page 37 and 38:
TWO-DIMENSIONAL ELECTRON GAS 2009Sp
- Page 39 and 40:
TWO-DIMENSIONAL ELECTRON GAS 2009Cr
- Page 41 and 42:
TWO-DIMENSIONAL ELECTRON GAS 2009Re
- Page 43 and 44:
TWO-DIMENSIONAL ELECTRON GAS 2009In
- Page 45 and 46:
TWO-DIMENSIONAL ELECTRON GAS 2009Ho
- Page 47 and 48:
TWO-DIMENSIONAL ELECTRON GAS 2009Te
- Page 50 and 51:
2009 SEMICONDUCTORS AND NANOSTRUCTU
- Page 52 and 53:
2009 SEMICONDUCTORS AND NANOSTRUCTU
- Page 54 and 55:
2009 SEMICONDUCTORS AND NANOSTRUCTU
- Page 56 and 57:
2009 SEMICONDUCTORS AND NANOSTRUCTU
- Page 58 and 59:
2009 SEMICONDUCTORS AND NANOSTRUCTU
- Page 60:
2009Metals, Superconductors and Str
- Page 63 and 64:
METALS, SUPERCONDUCTORS... 2009Anom
- Page 65 and 66:
METALS, SUPERCONDUCTORS... 2009Magn
- Page 67 and 68:
METALS, SUPERCONDUCTORS ... 2009Coe
- Page 69 and 70:
METALS, SUPERCONDUCTORS ... 2009Fie
- Page 71 and 72:
METALS, SUPERCONDUCTORS... 2009High
- Page 73 and 74:
METALS, SUPERCONDUCTORS... 2009Angu
- Page 75 and 76: METALS, SUPERCONDUCTORS... 2009Magn
- Page 77 and 78: METALS, SUPERCONDUCTORS... 2009Meta
- Page 79 and 80: METALS, SUPERCONDUCTORS... 2009Temp
- Page 81 and 82: METALS, SUPERCONDUCTORS... 200974
- Page 84 and 85: 2009 MAGNETIC SYSTEMSY b 3+ → Er
- Page 86 and 87: 2009 MAGNETIC SYSTEMSMagnetotranspo
- Page 88 and 89: 2009 MAGNETIC SYSTEMSHigh field tor
- Page 90 and 91: 2009 MAGNETIC SYSTEMSNuclear magnet
- Page 92 and 93: 2009 MAGNETIC SYSTEMSStructural ana
- Page 94 and 95: 2009 MAGNETIC SYSTEMSEnhancement ma
- Page 96 and 97: 2009 MAGNETIC SYSTEMSInvestigation
- Page 98 and 99: 2009 MAGNETIC SYSTEMSField-induced
- Page 100 and 101: 2009 MAGNETIC SYSTEMSMagnetic prope
- Page 102: 2009Biology, Chemistry and Soft Mat
- Page 105 and 106: BIOLOGY, CHEMISTRY AND SOFT MATTER
- Page 108 and 109: 2009 APPLIED SUPERCONDUCTIVITYMagne
- Page 110 and 111: 2009 APPLIED SUPERCONDUCTIVITYPhtha
- Page 112: 2009Magneto-Science105
- Page 115 and 116: MAGNETO-SCIENCE 2009Study of the in
- Page 117 and 118: MAGNETO-SCIENCE 2009Magnetohydrodyn
- Page 119 and 120: MAGNETO-SCIENCE 2009112
- Page 122 and 123: 2009 MAGNET DEVELOPMENT AND INSTRUM
- Page 124 and 125: 2009 MAGNET DEVELOPMENT AND INSTRUM
- Page 128 and 129: 2009 MAGNET DEVELOPMENT AND INSTRUM
- Page 130 and 131: 2009 MAGNET DEVELOPMENT AND INSTRUM
- Page 132 and 133: 2009 MAGNET DEVELOPMENT AND INSTRUM
- Page 134 and 135: 2009 MAGNET DEVELOPMENT AND INSTRUM
- Page 136 and 137: 2009 PROPOSALSProposals for Magnet
- Page 138 and 139: 2009 PROPOSALSSpin-Jahn-Teller effe
- Page 140 and 141: 2009 PROPOSALSQuantum Oscillations
- Page 142 and 143: 2009 PROPOSALSThermoelectric tensor
- Page 144 and 145: 2009 PROPOSALSDr. EscoffierCyclotro
- Page 146 and 147: 2009 PROPOSALSHigh field magnetotra
- Page 148 and 149: 2009 THESESPhD Theses 20091. Nanot
- Page 150 and 151: 2009 PUBLICATIONS[21] O. Drachenko,
- Page 152 and 153: 2009 PUBLICATIONS[75] S. Nowak, T.
- Page 154 and 155: Contributors of the LNCMI to the Pr
- Page 156 and 157: Institut Jean Lamour, Nancy : 68Ins
- Page 158 and 159: Lawrence Berkeley National Laborato