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2009 MAGNETO-SCIENCEChanges in the microstructure resulting from a high cooling rate in Fe-xC-Mnalloys in strong magnetic fieldThe impact of magnetic field on the microstructures obtainedafter rapid cooling is observed in Fe-xC-1.5wt%Mnsteels with x = 0.2 and 0.3 wt%C. The experim<strong>en</strong>ts aredone in a furnace in which alloys are water cooled in magneticfield from the aust<strong>en</strong>ite state [T.Garcin et al., Pat<strong>en</strong>t955380, 2009]. After holding at 1173K for 5min, the poweris switched off and the sample is qu<strong>en</strong>ched. More than200 K/s is obtained by water qu<strong>en</strong>ching betwe<strong>en</strong> 1173 Kand 373 K. The Figure show the SEM micrographs afterqu<strong>en</strong>ching under 0T and 16T.These modifications in the resulting microstructure by theapplication of a static magnetic field may be interestingwh<strong>en</strong> a mixture of ferrite, bainite and mart<strong>en</strong>site is <strong>des</strong>ired.Figure 1(a) shows the 0.2wt%C steel gra<strong>des</strong> cooled under0T and 16T. In the 0T sample, the microstructure is composedof a mixture of bainite (α B ) and mart<strong>en</strong>site(α’). Bainiteis a two-phase structure that contains ferrite-cem<strong>en</strong>titeregions formed from the eutectoid decomposition of aust<strong>en</strong>ite(γ). Mart<strong>en</strong>site is a product of diffusionless transformationand can occur in the form of thin, l<strong>en</strong>ticular plateswhich oft<strong>en</strong> ext<strong>en</strong>d right across the par<strong>en</strong>t gamma grains, oras packets of approximately parallel, fine laths whose sizeis g<strong>en</strong>erally smaller than that of the γ grains. Only severalislands of allotriomorphic ferrite are observed in the structure.The allotriomorphic ferrite (α) grows rapidly alongthe aust<strong>en</strong>ite grain boundary (which is an easy diffusionpath) but thick<strong>en</strong>s more slowly. Application of 16T leads toa considerable increase in the allotriomorphic ferrite fractionalong the prior aust<strong>en</strong>ite grains boundaries. In addition,a large amount of Widmansttt<strong>en</strong> ferrite (α W ) is detected bythe pres<strong>en</strong>ce of thin-wedge plates which have grown fromthe prior aust<strong>en</strong>ite grain boundaries.Figure 1(b) shows the 0.3wt%C steel gra<strong>des</strong> cooled under0T and 16T. In the 0T sample the microstructure iscomposed of a mixture of bainite and mart<strong>en</strong>site. No allotriomorphicferrite is observed probably due to the relativelyhigh carbon cont<strong>en</strong>t in alloy. Wh<strong>en</strong> the transformationoccurs under 16T, the microstructure is predominantlymart<strong>en</strong>site but also has allotriomorphic ferrite, Widmansttt<strong>en</strong>ferrite, bainite and ev<strong>en</strong> pearlite. The mart<strong>en</strong>site structurecan be here referred to as lath mart<strong>en</strong>site which consistsof mart<strong>en</strong>site needles with differ<strong>en</strong>t but well-definedori<strong>en</strong>tations. Notice that the spherical shape of pearlitecolonies is obvious in this sample because of the lack ofimpingem<strong>en</strong>t with other pearlite colonies. Vickers hardnessmeasurem<strong>en</strong>ts have be<strong>en</strong> performed for the differ<strong>en</strong>t alloyscomposition after thermomagnetic treatm<strong>en</strong>t. The applicationof a strong magnetic field results in a g<strong>en</strong>eral decreasein the hardness values. This reduction of hardness is relatedto the <strong>en</strong>hancem<strong>en</strong>t of the ferrite precipitation in the alloystreated under static magnetic field.Figure 151: SEM micrographs showing the structure after waterqu<strong>en</strong>ching under 0 and 16 T for the Fe-0.2C-1.5Mn (a) and forFe-0.3C-1.5Mn (b)(wt%). Original magnification 4000x, 4% nitaletching sample.F. DebrayT. Garcin, S. Rivoirard, R. Morgunov, E. Beaugnon, (CRETA, CNRS, Gr<strong>en</strong>oble, France)107

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