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L 225/220 21.8.2001 Journal officiel des Communautés européennes FR (76) Kördel W., Stutte J., Kotthoff G. (1993), ‘HPLC — screening method for the determination of the adsorption coefficient on soil — comparison of different stationary phases’. Chemosphere 27 (12), pp. 2341-2352. (77) Hance, R. J., (1967), ‘The Speed of Attainment of Sorption Equilibria in Some Systems Involving Herbicides’. Weed Research, Vol. 7, pp. 29-36. (78) Koskinen W. C., and Harper S. S., (1990), ‘The retention processes: mechanisms’ in Pesticides in the Soil Environment: Processes, Impacts and Modelling (ed. H.H. Cheng). Soil Sci. Soc. Am. Book Series, No. 2, Madison, Wisconsin. (79) Cohen S. Z., Creeger S. M., Carsel R. F., and Enfield C. G. (1984), ‘Potential pesticide contamination of groundwater from agricultural uses’, in Treatment and Disposal of Pesticide Wastes, pp.297-325, ACS Symp. Ser. 259, American Chemical Society, Washington, DC. (80) Giles C. H., (1970), ‘Interpretation and use of sorption isotherms’ in Sorption and Transport Processes in Soils. S.C.I. Monograph No. 37, pp. 14-32. (81) Giles, C. H.; McEwan J. H.; Nakhwa, S.N. and Smith, D, (1960), ‘Studies in adsorption: XI. A system of classification of solution adsorption isotherms and its use in the diagnosis of adsorption mechanisms and in measurements of pesticides surface areas of soils’. J. Chem. Soc., pp. 3973-93. (82) Calvet R., Tercé M., and Arvien J. C., (1980), ‘Adsorption des pesticides par les sols et leurs constituants: 3. Caractéristiques générales de l'adsorption’. Ann. Agron. 31: pp. 239-251. (83) Bedbur E., (1996), ‘Anomalies in the Freundlich equation’, Proc. COST 66 Workshop, Pesticides in soil and the environment, 13-15 May 1996, Stratford-upon-Avon, UK. (84) Guth, J. A., (1985), ‘Adsorption/desorption’, in Joint International Symposium, Physicochemical Properties and their Role in Environmental Hazard Assessment, July 1-3, Canterbury, UK. (85) Soil Texture Classification (US and FAO systems): Weed Science, 33, Suppl. 1 (1985) and Soil Sci. Soc. Amer. Proc. 26:305 (1962).
21.8.2001 L 225/221 Journal officiel des Communautés européennes FR Phase 3 Phase 2 Phase 1 Conditions préalables Sélection de rapports sol/ solution optimaux APPENDICE 1 ORGANIGRAMME D'ESSAI Élaboration d’une méthode analytique adéquate Méthode disponible? Oui Étude préliminaire 2 sols Détermination du temps d’équilibre Plateau d’équilibre atteint? Oui Cinétique d’adsorption 5 sols Non Fin des essais Vérification de l’adsorption sur les parois du récipient si: Kd* (m sol/V 0) > 0,3 (méthode indirecte: mesure de la déplétion de la solution) Kd* (m sol/V 0) > 0,1 (méthode directe: mesure des deux phases) Isothermes d’adsorption Cinétique de désorption Vérification de la stabilité au moyen du bilan matière Si le bilan matière est < 90 % la substance à tester n’est pas stable durant l’échelle de temps de l’essai. On peut compléter l’essai par l’analyse des deux phases (sol et solution aqueuse) selon le cas Isothermes de désorption
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