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S.BEYHAN et al./ ISEM2016 Alanya – Turkey doğal puzolanlar, çimentonun toplam özgül yüzeyini artırdıkları için su ihtiyacını da artırabilmektedirler. Portland çimentosunun ve doğal puzolanın bir karışım halinde uygulandığı harçlarda ve betonlarda katılaşma sürelerinin, puzolanın katılım oranına, inceliğine ve reaktivitesine bağlı olarak gelişme gösterdiği ifade edilmektedir [18]. CaO, MgO ve SO3 gibi bazı zararlı maddelerin çimentoda hacim genleşmesini tetikledikleri için bu maddelerin çimentoda belli sınırların altında olması gerekmektedir. CaO miktarı kütlece %3, MgO miktarı ise kütlece %4,5’ten fazla olmamalıdır. Doğal puzolanlar, inceliklerine bağlı olarak bu zararlı maddelerle tepkimeye girmekte ve bunların çimento içerisindeki oranlarını düşürmektedir [18]. 3. Malzeme ve Yöntem Deneylerde kullanılan CEM I 42,5 R çimentosunun, uçucu külün ve volkanik tüfün kimyasal özellikleri Tablo 1’de, standart kumun granülometrik bileşimi ise Tablo 2’de verilmiştir. Tablo1. Uçucu kül, CEM I 42,5 R çimentonun ve tüfün kimyasal analiz değerleri Numune No SiO 2 Al 2O 3 Fe 2O 3 MgO CaO Na 2O K 2O SO 3 TiO 2 KK Toplam Uçucu Kül (UK) 50.97 19.30 12.89 4.21 4.31 0.57 2.31 1.77 0.82 2.26 99.41 Tüf (T) 65.22 16.03 1.75 2.70 1.80 1.97 3.40 - 0.22 6.43 99,52 CEM I 42.5R 18.90 5.15 3.36 1.57 63.59 0.40 0.77 2.65 - 3.59 99.98 Tablo 1’den görüldüğü üzere uçucu kül SiO2 + Al2O3 + Fe2O3 değeri %70’den büyük ve CaO değeri de
S.BEYHAN et al./ ISEM2016 Alanya – Turkey ve çimentoya ikame numunelerin miktar ve oranları Tablo 3’de verilmiştir. Çimento harçları, 40×40×160mm boyutlu çelik kalıplara yerleştirilmiştir (Şekil 1). Harç numuneleri, 20±2 ºC sıcaklık ve %90’dan fazla bağıl neme sahip kür dolabında 24 saat bekletilmiş ve daha sonra 2, 7 ve 28 gün 20 ± 2 ºC sıcaklığa sahip su havuzunda küre tabi tutulmuştur (Şekil 2). Kür havuzundan alınan numunelerin önce ağırlıkları belirlenmiş ve daha sonra sırasıyla TS EN 196-1’ e uygun hazırlanan harç numuneleri üzerinde ultrases geçiş süresi, eğilmede çekme ve basınç deneyleri yapılmıştır. Tablo 3. Harç malzemesi oranları ve karışım miktarları Karışım oranları Karşım miktarları Çimento (gr) UK (gr) T (gr) Kum (gr) Su (gr) Toplam (gr) Şahit numune 450 - - 1350 225 2025 %10 (%5 UK+%5 T) 405 22.5 22.5 1350 225 2025 %20 (%10 UK+%10 T) 360 45.0 45.0 1350 225 2025 %30 (%15 UK+%15 T) 315 67.5 67.5 1350 225 2025 %40 (%20 UK+%20 T) 270 90.0 90.0 1350 225 2025 UK: Uçucu kül, T: Tüf Şekil 1. Kalıplara dökülmüş harç numuneleri Şekil 2. Numunelerin kür havuzunda bekleme durumları 4. Deneysel Çalışmalar 4.1. Eğilme dayanımı deneyi Harç numunelerin eğilme deneyi, numunenin ortasına gelecek şekilde tek noktadan yükleme yapılarak uygulanmıştır. Yükleme hızı saniyede 0,4 kN/sn olacak şekilde ayarlanmış ve eğilme dayanımı (Rf ), Eşitlik 1 yardımıyla hesaplanmıştır [20]. Burada; = , (1) Rf : Eğilme dayanımı (N/mm 2 ) b : Prizmanın kare kesitinin kenar uzunluğu (mm) 157
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ISBN 9786054735846

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