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N. SOZBIR et al./ ISEM2016 Alanya – Turkey Şekil 3. Alüminyum Cürufun XRD Analizi 5. Sonuç Örnek tesiste yıkama işlemine tabi tutulacak olan tuzlu kara alüminyum cürufunun analizi, yıkama işlemine yönelik laboratuar bazında yapılan test sonuçları ve bazı literatür çalışmaları dikkate alındığında; işletmede hammadde olarak kullanılacak olan ve içerisindeki tuzun ayrıştırılmasına yönelik olarak yıkama işlemine tabi tutulacak olan tuzlu kara alüminyum cürufunda, metal bileşiklerinden alüminyum fosfür, alüminyum sülfürün ve Al4C3 bulunmadığı görülmüştür. Örnek tesiste yıkama sonucu sadece amonyak (NH3) gazı çıkışı olduğu anlaşılmıştır. Yıkama işleminin 25 o C ve 60 o C sıcaklığındaki su ile yapılması sonucu cüruftan ayrılan tuz miktarının yaklaşık aynı olduğu, dolayısıyla suyun ısıtılması için harcanacak enerjiden tasarruf edilmesi gerektiği ve oda sıcaklığında uygulanacak işlem sonucunda meydana gelecek gaz emisyon miktarının da daha az olacağı, tesisin saatlik cüruf yıkama kapasitesinin yaklaşık 8,44 ton/h olduğu ve buna bağlı olarak da çıkacak toplam gaz miktarının yaklaşık 3.89 m 3 /h ve dolayısıyla toplam gaz emisyonun saatlik kütlesel debisinin de 2.6 kg/h olacaktır. Bu durumda yıkama sonucunda çıkacak gazın emisyon değeri Tablo 1’de belirtilen değerlerin altında olduğu görülmektedir. Alüminyum cürufundan çelik endüstrisi için flaks yapılırken içerisindeki tuzların oda sıcaklığındaki (25 o C) su ile yıkanması ekonomik olarak avantajlı olduğu daha sıcak su ile yıkama yapmanın avantajlı olmadığı görülmüştür. 862
N. SOZBIR et al./ ISEM2016 Alanya – Turkey Tablo 1. Sanayi Kaynaklı Hava Kirliliğinin Kontrolü Yönetmeliği Ek-2 Tablo 2.1 Kütlesel Debiler [5]. Normal işletme şartlarında ve haftalık iş günlerindeki işletme Emisyonlar saatleri için kütlesel debiler (kg/saat) Bacadan Toz 10 1 Baca Dışındaki Yerlerden Kurşun 0.5 0.05 Kadmiyum 0.01 0.001 Talyum 0.01 0.001 Klor 20 2 Hidrojen klorür ve Gaz Halde İnorganik 20 2 Klorür Bileşikleri Hidrojen florür ve Gaz Halde İnorganik 2 0.2 Florür Bileşikleri Hidrojen Sülfür 4 0.4 Karbon Monoksit 500 50 Kükürt Dioksit 60 6 Azot Dioksit [NO x (NO 2 cinsinden)] 40 4 Toplam Organik Bileşikler 30 3 Not: Tablodaki emisyonlar İşletmenin tamamından (bacaların toplamı) yayılan saatlik kütlesel debilerdir. 6. Kaynaklar [1] Nedim Sözbir, Mustafa Akçil, ve Hasan Okuyucu “Alüminyum Cürufundan Alüminyum Metali ve Flaks Eldesi”, ISEM2014 Adıyaman – TÜRKİYE, 1108-113, 2014. [2] Onuralp Yücel ve Erman Car “Alüminyum Cüruflarının Değerlendirilmesi ve Kalsiyum Alüminat Sentetik Cüruf Yapıcı Üretimi”, Türk Mühendis ve Mimar Odaları Birliği Metalurji ve Malzeme Mühendisleri Odası, Metalurji Sayı: 175, Ağustos 2015. [3] H.Z. Wang, D.Y.C. Leung, M.K.H. Leung and M. Ni “A Review on Hydrogen Production Using Aluminium and Aluminium Alloys”, Renewable and Sustainable Energy Reviews, 13 (2009) 845–853. [4] A. Binnaz Yoruç ve Mustafa Çiğdem “Tuzlu Alüminyum Cüruflarının Değerlendirilmesi”, Yıldız Teknik Üniversitesi, Kimya-Metalurji Fakültesi, Metalurji ve Malzeme Mühendisliği Bölümü, 2001. [5] Sanayi Kaynaklı Hava Kirliliğinin Kontrolü Yönetmeliği, Resmi Gazete, Sayı:29211, 20 Aralık 2014. 863
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ISBN 9786054735846

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