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M. ERAT et al./ ISEM2016 Alanya – Turkey UV katalitik reaksiyonlar için 1 x 20 W (UV lambası, P.R.C.) tipli UV lambası kullanılmıştır. Çalışmada RB5 azo boyası 50 mg/L konsantrasyon olacak şekilde hazırlanmıştır. İstenilen pH aralığına 0.1 M HCl ve 0.1 M NaOH kullanılarak ayarlamanmıştır. İstenilen konsantrasyonda hazırlanan boyar madde çözeltisi, uygun pH ayarı yapıldıktan sonra kesikli reaksiyon uygulanmış ve batch ortaminda UV ile muamele edilmiştir. Belirlenen deney süresi sırasında belli aralıklarla numune alınarak 0.45 mm membran filtreden geçirilerek spektrofotometre (Epoch Nanodrop UV-VIS spektrometre) olarak renk analizleri yapılmıştır. Boya gideriminde optimum pH, optimum sıcaklık ve zaman parametreleri tespit edilmiştir [14,15]. 3. Sonuçlar 3.1. AR37’nin UV katalitik giderimi Başlangıçta RB5 azo boyası için kalibrasyon grafiği oluşturuldu. Bu amaçla maksimum absorbans verdiği belirlenen 597 nm’de ölçümler yapıldı (Çizelge 1). Çizelge 1. Reaktif black 5 (RB5)’in genel özellikleri Parametreler Boya sınıfı Di azo boyar madde Color İndeks Adı Reactive black 5 Moleküler formülü C26H21N5Na4O19S6 Adsorpsiyon gösterdiği 597 nm dalga boyu (λmax) Molekül ağırlığı (g/mol) 991.82 Kalibrasyon grafiğinin oluşturulması amacıyla farklı konsantrasyonlarda hazırlanan RB5 boyasının absorbansı 597 mn’de ölçüldü ve grafik oluşturuldu (Şekil 2). 1,6 Absorbans (597 nm) 1,2 0,8 0,4 y = 0,0257x + 0,0015 R² = 0,9999 0 0 10 20 30 40 50 60 ppm Şekil 2. Reactif black 5 (RB5) kalibrasyon grafiği RB5 azo boyasının UV katalitik olarak giderilmesinde optimum zamanının belirlenmesi amacıyla, kurulan reaksiyon ortamından belirli aralıklarla alınan numunelerin absorbansı spektrofotometrik olarak ölçülmüş ve optimum 5 dakikada %90.62 oranında boya gideriminin olduğu 20 dakikada ise boyanın tamamına yakınının giderildiği ve dengeye ulaşıldığı belirlenmiştir. 3 959
M. ERAT et al./ ISEM2016 Alanya – Turkey 120 100 Boya giderimi (%) 80 60 40 20 0 0 20 40 60 80 Zaman (dak) Şekil 3. Reaktif black 5 (RB5) azo boyasının UV katalitik olarak gideriminin zamana bağlı değişimi Reaktif black 5 (RB5) azo boyasının gideriminde pH’nın etkisini araştırmak amacıyla farklı pH ortamlarında hazırlanan boya çözeltisiyle TiO2 nanopartiküller varlığında UV katalitik giderim yapılmış ve sonuçlar Şekil 4’de verilmiştir. 120 100 Boya giderimi (%) 80 60 40 20 Şekil 4. Reaktif black 5 (RB5) azo boyasının TiO 2 nanopartikül varlığında UV katalitik olarak gideriminin pH’a bağlı değişimi Elde edilen bulgulardan pH 4.0 ve 10.0’da sırasıyla %97.23 ve %91.4 oranlarında Reaktif black 5 (RB5) azo boyasının TiO 2 nanopartiküllerinin varlığında UV katalitik olarak giderildiği belirlendi. Bu metotla boyanın asidik ve bazik pH’larda giderilebileceği çevre açısından olumlu bir sonuç olarak görüldü. 3. Tartışma 0 3 5 7 9 11 TiO2 nanopartikülleri UV ışığı yöntemiyle Reaktif black 5 (RB5) azo boyasının giderimi, UV ışığı varlığında ve yarı iletken TiO2 nanopartiüküllerin katalizörlüğünde sağlanmaktadır. TiO2’in UV ışını ile uyarılması sonucu iletim band elektronları (e) ve değerlik band boşluklarının (h) oluşumu gerçekleşir. Bu elektron (e) – (h) boşluk çiftlerinden bazıları birleşirken bazıları TiO 2 katalizör yüzeyine hareket ederek burada daha önceden absorbanmış olan H 2O, OH - , O 2 ile redoks tepkimesine girerek OH radikalinin oluşumuna sebep olur. Bu tepkimeler aşağıdaki tepkimelerle verilmiştir: pH 4 960
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ISBN 9786054735846

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