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M. Celebi et al./ ISEM2016 Alanya - Turkey 3 / 8 çalışmaya rastlanmamıştır. Bu çalışmada rejenere edilebilen anyonik polimer kullanılarak literatürdeki bu eksiklik giderilmiştir. Çizelge 1. Bazik boyaların giderilmesinde literatürde kullanılan yöntemler Boyarmadde Bazik Blue 41 Bazik Blue 41 Bazik Blue 41 Bazik Red 46 Bazik Yellow 28 Bazik boyar madde tekstil atık suyu Bazik Red 46 Kristal Violet Methylene Blue Methylene Blue Kristal Violet, Bismarck Brown Y Methylene Blue Methylene Blue Bazik Violet 3 Bazik Red 9 Kristal Violet, Bazik Fuchsin, Brillant Green, Malachite Green Metil Violet Yöntem Adsorpsiyon (Nikel Demir Nanopartiküller) Adsorpsiyon (Magnetik demir nanopartikül–alginat) Enzimatik (Kloroperoksidaz enzimi) Elektrokoagülasyon Elektrokoagülasyon Elektrokoagülasyon Fotokatalitik (immobilize TiO 2 nanopartiküller) Adsorpsiyon (aktif karbon) Biyosorpsiyon (Trichoderma viride fungus) Süper absorbent hidrojel Adsorpsiyon (modifiye kitosan) Lignin Peroksidaz enzimi Adsorpsiyon (Hidrojeller) P. Ostreatus, S. Commune, S. Rolfsii, N. Crassa, Polyporus sp., T. Villosa and M. Thermohila Aeromonas hydrophila strain DN322 Adsorpsiyon (perlit) Bu çalışmada, 3 adet katyonik boyar madde (Basic Blue 41, Basic Yellow 28, Basic Red 46) ve sentetik atık su ticari perflorokarbon esaslı polimer ile farklı koşullarda (pH, sıcaklık, başlangıç boyar madde konsantrasyonu) başarılı bir şekilde giderilmiştir. 2. Malzeme ve Yöntem Çalışmada kullanılan boyar maddeler akrilik elyaf fabrikasından temin edildi. Bazik karakterde akrilik elyaf boyahane atık suyu sentetik olarak 3 adet bazik boyar madde kullanılarak hazırlandı [15]. Kullanılan boyar maddelerin özellikleri Çizelge 2’de gösterilmiştir. 60 mg ticari anyonik polimer sentetik boyar madde çözeltilerine ilave edilip 250 rpm’de bir saat karıştırıldı. Boyar maddelerin başlangıç boya konsantrasyonu 60 mg/L’dır. Boyar maddelerin yüzde giderimi, maksimum dalga boylarındaki azalmaya göre belirlendi. 570
M. Celebi et al./ ISEM2016 Alanya - Turkey 4 / 8 Çizelge 2. Çalışmada kullanılan katyonik boyarmaddelerin özellikleri Boyar madde Molekül ağırlığı (g/mol) Maksimum absorbans dalgaboyu (λ max) Basic Yellow 28 (BY 28) 433,52 438 Basic Blue 41 (BB41) 482,57 609 Basic Red 46 (BR 46) 403,32 530 Şekil 1. Basic Blue 41 Boyar maddesi Şekil 2. Basic Red 46 Boyar maddesi Şekil 3. Basic Yellow 28 Boyar maddesi 3. Sonuçlar ve Tartışma Bazik boyar maddelerin (BB41: Basic Blue 41; BY28: Basic Yellow 28; BR46: Basic Red 46) farklı sıcaklık değerlerinde perflorokarbon esaslı polimer ile giderilmiştir. 571
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