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İ. TEĞİN ve S. AKDENİZ./ ISEM2016 Alanya – Turkey iyonı için pH 9,0’da geri kazanma verimine elüent türü, derişimin etkisinin incelenmesi için yapılan çalışmanın sonuçlarına göre, düşük hacim ve düşük konsantrasyonda, maksimum geri kazanma veriminin sağlandığı asit çözeltisi Cd için 5 mL 1,5M HNO3 olarak belirlenmiştir. Sonuçlar Tablo 4’te ve Şekil 10-11’de verilmiştir. Elüasyon Çözelti Türü HCl HNO3 Tablo 4. Elüent Tipi ve Miktarının Geri Kazanıma Etkisi Elüasyon Çözelti Elüasyon Çözelti Hacmi Cd(II) Derişimi (mol/L) (mL) Geri Kazanım Verimi (%) 0,5 5 92,30 1,0 5 95,07 1,5 5 94,56 2,0 5 93,37 0.5 5 92,27 1.0 5 93,68 1.5 5 98,35 2,0 5 98,31 Geri kazanım, % 105 100 95 90 85 80 75 70 0 1 2 3 HNO 3 Derişimi, mol/L %Cd Geri kazanım, % 100 95 90 85 80 75 70 0 1 2 3 HCL Derişimi, mol/L %Cd Şekil 10. HNO 3 konsantrasyonun Etkisi Şekil 11. HCI konsantrasyonun Etkisi Tablo 4 ve Şekil 10-11 incelendiğinde en uygun elüentin Cd için 1,5 M HNO3 olduğu görülmektedir. 3.7. Yabancı İyonların Etkisi Gerçek örneklerde eser metallerin tayin edilmesi yabancı iyonların matriks etkisi yapmasından dolayı zorlaşmaktadır. Matriks etkisini incelemek için su örneklerinde yer alan Na + ,Cl - , Mn 2+ , Mg 2+ , Ca 2+ , F - iyonlarının Cd (II) analit iyonlarının geri kazanım değerlerine etkisi incelendi. Farklı 726
İ. TEĞİN ve S. AKDENİZ./ ISEM2016 Alanya – Turkey derişimlerde bu iyonların yer aldığı model çözeltilere geliştirilen yöntem uygulanıp geri kazanım değerleri incelendi. Elde edilen sonuçlar Tablo 5’te verilmiştir. Tablo 5. Yabancı İyonların Geri Kazanıma Etkisi İyon Eklenen Tuzu Derişim (mg/L) Cd(II) için Geri Kazanım, (%) Na+ NaCI 10000 98,84 ± 1,26 Cl- BaCl2.H2O 20 85,82 ± 1,96 Mn2+ MnS04.H2O 50 82,89 ± 1,78 Mg2+ Mg(NO3)3.6 H2O 5000 85,69 ± 1,87 Ca2+ CaCl2.2H2O 3000 83,50 ± 1,98 F- KF 1000 98,38 ± 1,65 3.8. Kolonun Tekrarlanabilirliği Zenginleştirme çalışmalarında absorbanın tekrar kullanılabilirliği oldukça önemli bir faktördür. Bu amaçla 2ppm Cd çözeltisi hazırlandı. Hazırlanan bu çözelti daha önce belirlenen optimum koşullarda Badem kabuğu immobolize edilmiş Amberlit XAD-4 kolon dolgu maddesi için belirlenen optimum koşullarda Cd çözeltisi 10 defa geçirildi. Elde dilen sonuçlar Şekil 12’de verilmiştir. 110 90 Geri kazanım, % 70 50 30 10 0 2 4 6 8 10 12 Kolonun Tekrarlanabilirliği Cd Şekil 12. Kolonun Tekrarlanabilirliği 727
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