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A. ATES et al./ ISEM2016 Alanya – Turkey Adsorpsiyon izotermleri Şekil 4d’de dengede arsenik adsorpsiyonu (qe) ile dengede arsenik derişimi (Ce) arasındaki ilişkiyi ifade eden adsorpsiyon izotermi gösterilmiştir. Artan As(V) derşimi ile de arsenik giderimi artı HFO yüklü silikat etkinliği ile kirlenmiş sudan arsenik seçici olarak giderimi artmıştır. Maksimum arsenik adsorpsiyon kapasitesi (qmak)(300 mg As/g HFO-Si5,pH=8) bulunmuş ve adsorpsiyon izoterminin de Langmuir'in izotermine uyduğu gözlenmiştir. Bu değerler literatürde rapor edilenler ile karşılaştırıldığında, literatürden 5 kat yüksek As(V) ayrımı başarılmıştır[13, 14]. Dolgulu yatak çalışmaları Dolgulu yatak kolon deneyleri HFO-Si5 ile As (V) giderim kapasitesini değerlendirmek için çalışılmıştır. Çalışma bulguları Şekil 5’de gösterilmiştir. Şekilden görüldüğü gibi As(V) ayırma verimi yaklaşık 24000 yatak hacminde gerçekleşmektedir. Bu da, sürekli sistemlerde HFO-Si adsorbentinin etkinliğini göstermektedir. Adsorpsiyon kinetiği Partikül içi difüzyon mekanizması Şekil 6’da deneysel sonuçlardan açıkça görülmektedir ki, qt ve t 0,5 arasındaki ilişki, adsorbsiyon sürecinin üç adımda gerçekleştiğini göstermektedir. Öncelikle,''sharper portion (keskin bölüm) '' adsorbsiyonun dış yüzeyine tutunan çözeltiye veya sınır yüzeydeki çözünmüş molekülleri ifade etmektedir. İkinci olarak, “intra particle (partikül içi)” hız sınırlayıcı olduğu yerde aşamalı adsorbsiyon evresi gerçekleşmektedir. Üçüncüde, ''partion'' soldaki ultra düşük yüzeye tutunan çözeltiye rağmen yavaşlamaya başlayan partikül içi difüzyona sahip denge evresine eklenir. Ayrıca, uzaklaştırma oranı yüzeye tutunan molekül tarafından sınırlandırılmış olabilir. Şekil 6a’da görüldüğü gibi doğru tüm zaman boyunca doğrusal değildir. Bu durum adsorpsiyonda birden fazla taşınım olayının etkin olduğunu göstermektedir. Doğrusal kısmın eğiminin, yavaş adsorpsiyon prosesine eğimini oranı bize yavaş adsorpsiyon prosesini belirtir. Bu da gözeneklerdeki arsenik iyonlarının difüzyonun, HFO-Si5 için kısıtlayıcı basamak olduğunu göstermektedir. Deneysel verilere pseude first order ve pseudo-second order modelleri uygulanmış olup, pseude first order modelinin regresyon katsayısı düşük olduğundan, burada gösterilmemiştir. Sonuçlar göre de, Pseude second order burada deneysel sonuçlar ile iyi uyum sağlamaktadır. 878
A. ATES et al./ ISEM2016 Alanya – Turkey (a) (b) (c) (d) Şekil 4. As(V) ayrımına pH (a) ve demir içeriğinin etkisi(b, c), d) HFO-Si5 ile As(V) ayrımı üzerine başlangıç As(V) derişiminin etkisi. 879
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