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A. ATES et al./ ISEM2016 Alanya – Turkey 1800 1600 Şiddet [a.u] 1400 1200 1000 800 600 400 200 HFO-Si5 HFO-Si3 HFO-Si2 HFO-Si1 Silika- jel 0 5 10 15 20 25 30 35 40 45 50 55 60 65 2 [ o ] Şekil 1. Silika jel ve demir yüklenmiş silika jelin XRD görünümleri Yüzey alanı ve gözenek boyut dağılımı Şekil 2. HFO-Si5’in SEM, EDX ve TEM görünümleri Silika jel ve demir yüklenmiş silika jel örneklerinin N2-adsorpsiyon- desorpsiyon izotermleri Şekil 3’de gösterilmiştir. Silika jel, HFO-Si1, HFO-Si2 ve HFO-Si3 örnekleri izoterm gruplarından Tip-II’e uymakta olup, adsorpsiyon ve desorpsiyon eğrilerinin birbirine yakınlığı mikro gözenek yapının varlığını göstermektedir. HFO-Si4 ve HFO-Si 5 örnekleri ise, Tip IV izotermi göstermektedir. Adsorpsiyon- desorpsiyon izotermlerinden hesaplanmış yüzey alanı ve gözenek boyut dağımı sonuçları Tablo 1’de gösterilmiştir. Silika jelin yüzey alanı 190.3 m 2 g -1 iken, demir yüklemesiyle bu değer, demir yüklemesine bağlı olarak azalmıştır. Bu demir oksitlerin gözeneklerde birikiminin bir sonucu olabilmektedir. Ancak, demir miktarının artışı ile HFO-Si4 (426.6 m 2 /g) ve HFO-Si5 (781.8 m 2 .g -1 ) örneklerin yüzey alanı çok artmış olup, bu demir türlerinin nano boyutta yüzeyde dağılımın bir sonucu olmaktadır. Gözenek hacmi ve ortalama gözenek çapı incelendiğinde, yüksek demir yüklemelerinde mikro gözeneklerin sayısı artırdığı söylenebilmektedir. 876
A. ATES et al./ ISEM2016 Alanya – Turkey Adsorplanmış hacim [cm 3 g -1 ] 450 400 350 300 250 200 150 100 Silika jel HFO-Si1 HFO-Si2 HFO-Si3 HFO-Si4 HFO-Si5 50 0 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 P/P o [-] Şekil 3. Silika jel ve demir yüklenmiş silika jelin N 2 adsorpsiyon- desorpsiyon izotermleri Tablo 1. Demir yüklemesiyle yüzey alanı ve gözenek özelliklerinde değişimi Örnek S BET a (m 2·g -1 ) V Toplam b (cm 3·g -1 ) V mikro c (cm 3·g -1 ) Dp (Å) Silika-jel 190.3 0.53 0.077 55.8 HFO-Si1 81.9 0.54 0.030 130.9 HFO-Si2 91.9 0.44 0.042 97.8 HFO-Si3 111.8 0.36 0.008 65.2 HFO-Si4 426.6 0.51 0.028 24.1 HFO-Si4 781.8 0.61 0.021 15.7 a Çok noktalı BET ; b p/p 0 = 0.99’da adsorplanmış hacim.; c DR yöntemi ile hesaplanmış mikro gözenek hacmi As(V) giderimi üzerine pH ve demir içeriğinin etkisi Adsorpsiyon ile arsenik gideriminde pH anahtar parametredir. pH değerlerindeki değişim (2-12 aralığı) incelenmiş ve Şekil 4a’de gösterilmiştir. pH=8.0’e kadar As(V) ayrımı artmış ve sonra tekrar azalmıştır. Bu sonuçlar daha önce rapor edilen sonuçlarla uyumludur [13-20]. Bunun nedeni, hidratlanmış demir oksidin yüzeyi negatif olarak yükleniyor ve negatif yüklü yüzey ve HAsO4 2 – arasında elektrostatik itmeye neden olmaktadır [14, 15,20]. Demir içeriğinin As(V) ayrımı üzerine etkisi Şekil 4b ve c’de gösterilmiştir. Demir içeriğinin artışı ile As(V) ayrımı artmaktadır. Maksimum As(V) ayrımı ise HFO-Si5 örneklerinde 300 mg As(V)/g olarak bulunmuştur. Bu da, As(V)’in özellikle HFO formu üzerinde adsorplanmasının bir sonucudur [13]. 877
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ISBN 9786054735846

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