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M. Celebi et al./ ISEM2016 Alanya - Turkey 7 / 8 Boya Giderme (%) BB41 BY28 BR46 Süre (dakika) Şekil 7. pH:7,0, 45 ˚C ve 60 mg/L başlangıç boya konsantrasyonlarında farklı bekleme sürelerinde elde edilen % boya giderme değerleri Bu çalışmada, akrilik elyaf boyanmasında kullanılan bazik boyar maddelerin kumaşa boyanma sonrası tutunmadan kalan boyar maddelerden oluşan rengin giderilerek çevreye zararsız hale getirilmesi amaçlandı. Bu amaca ulaşmak için ticari perflorkarbon esaslı polimer pozitif yüklü boyar maddelerin giderilmesinde kullanıldı. Kısacası, bazik boyar maddelerin atık sudan giderilmesi amacıyla ticari perflorokarbon esaslı polimer kullanılmıştır. Boyar maddelerin giderilmesi farklı sıcaklık ve pH’larda yüksek boya giderme yüzdesi ile gerçekleşmiştir. Sıcaklık arttıkça boyar maddelerin boya giderme yüzdeleri artmıştır. BR46 boyar maddesi molekül yapısı ve molekülün diğer boyar maddelere göre daha küçük olması nedeniyle daha kısa sürede yüzde yüz boya giderme değerine ulaşmıştır. Bu çalışmada kullanılan polimerin maliyeti yüksektir. Buna karşın perflokarbon esaslı anyonik polimer rejenere edilerek defalarca (en az 10 kez) kullanabilmektedir. Rejenere olabilen daha ucuz maliyetle üretilebilecek polimerlerin elde edilmesi bazik boyar maddelerin daha ekonomik bir şekilde atık sulardan giderilmesine fayda sağlayacaktır. Teşekkür: Bu çalışma Yalova Üniversitesi (Proje No: 2014/BAP/083) tarafından desteklenmiştir. Referanslar [1] Celebi M. Tekstil Atık Sularında Boyaların Biyobozunma ile Giderilmesi, İstanbul Sanayi Odası Yayınları, İstanbul; 2013. [2] Baser İ, Yusuf İ, Boyar Madde Kimyası, Marmara Üniversitesi, Nadir Kitap; 1990. [3] Celebi M, Altikatoglu M, Akdeste Z. M, Yildirim H. Determination of decolorization properties of Reactive Blue 19 dye using Horseradish Peroxidase enzyme, Turkish J. Biochem. 2013; 38: 200–206. 574
M. Celebi et al./ ISEM2016 Alanya - Turkey 8 / 8 [4] Celebi M., Arif M, Altikatoglu M, Yildirim H. Removal of Cationic Dye from Textile Industry Wastewater with Using Enzyme , Fungus and Polymer, The Online J. Sci. and Technol. 2013; 3(2): 39–45. [5] Fee D, Morgan F, Yazdani M, Bahrami H, Arami M, Jaikumar V. Simultaneous ultrasoundassisted removal of sunset yellow and erythrosine by ZnS:Ni nanoparticles loaded on activated carbon: Optimization by central composite design. Desalination and Water Treatment. 2014; 52(2): 193–202. [6] Fazli M. M, Mesdaghinia A. R, Naddafi K, Nasseri S, Yunesian M, Assadi M. M., Rezaie S, Hamzehei H. Optimization of reactive blue 19 decolorization by ganoderma sp. using response surface methodology, Iranian J. Environ. Health Sci. Eng. 2010; 7(1): 35-42. [7] Song S, Yao J, He Z, Qiu J, Chen J. Effect of operational parameters on the decolorization of C.I. Reactive Blue 19 in aqueous solution by ozone-enhanced electrocoagulation. J. Hazardous Materials, 2008; 152(1): 204–210. [8] Lin S. H, Wang C. S. Treatment of high-strength phenolic wastewater by a new two-step method. J. Hazardous Materials, 2002; 90(2): 205–216. [9] Al-Aseeri M, Bu-Ali Q, Haji S, Al-Bastaki N. Removal of Acid Red and sodium chloride mixtures from aqueous solutions using nanofiltration. Desalination, 2007; 206(1-3): 407–413. [10] Harrelkas F, Paulo A, Alves M. M, El Khadir L, Zahraa O, Pons M. N, van der Zee, F. P. Photocatalytic and combined anaerobic-photocatalytic treatment of textile dyes. Chemosphere, 2008; 72(11): 1816–1822. [11] Basha C. A, Selvakumar K. V, Prabhu H. J, Sivashanmugam P, Lee C. W. Degradation studies for textile reactive dye by combined electrochemical, microbial and photocatalytic methods. Sep. and Purif. Technol. 2011; 79(3): 303–309. [12] Forgacs E, Cserhati, T, Oros G. Removal of synthetic dyes from wastewaters: A review. Environ. Int. 2004; 30(7): 953-971. [13] Parvathi C, Shoba U. S., Prakash C. Study of the removal of direct dye from aqueous solution by using solid agricultural waste. Int. J. Current Res. 2013; 5(1), 4, 218–221. [14] Onat T. A., Gümüşdere H.T, Güvenç A, Dönmez G, Mehmetoğlu Ü. Decolourization of Textile Azo Dyes by Ultrasonication and Microbial Removal. Desalination, 2010; 255:154-158. [15] Aspland, J. R. Chapter 12: The Application of Basic Dye Cations to Anionic Fibers: Dyeing Acrylic and Other Fibers with Basic Dyes - Tags: DYES & dyeing -- Textile fibers anions. Textile Chemist Colorist, 1993; 25(6), 21. 575
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