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F.AYĞAN/ ISEM2016 Alanya – Turkey Kaynakça Ardoğan Recep, “İslam’da Çevre Teolojisinin Pratiğe Yansıması: Çevre Ahlakı”, Birey ve Toplum, 2/3 (2012), s. 115-143. Câhız Ebû Osman Amr b. Bahr, Kitâbü’l-hayevân, thk. Abdusselam Muhammed Hârûn, y.y, 1965. Cüveynî, Ebu’l-Meâlî Abdülmelik b. Abdullah, el-İrşad ila kavâtıi'l-edilleti fî usûli'l-i'tikad, thk. Muhammed Yusuf Musa, Kahire: Mektebetü’l-Hanci, 1950. Esed Muhammed, Kur’an Mesajı, İstanbul: İşaret Yayınları, 1999. Evkuran Mehmet, “Çevre Bilincinin Teolojik Temelleri Üzerine”, Uluslararası Çevre ve Din Sempozyumu Bildirileri, İstanbul 2008, II, 35-48. Gazzâlî, el-Hikme fî mahlûkâtillah, thk. Muhammed Reşid Kabbânî, Beyrut: Dâru İhyâi’lulum, 1978. Güler İlhami, “Global Isınma, Ekolojik Dengenin Bozulması ve İklim Değişikliğinin Teolojisi”, Direniş Teolojisi, Ankara: Ankara Okulu Yayınları 2010, s. 21-23. Keleş Ruşen (ed), Çevre, İnsan, Toplum, Ankara 1992. Özdemir İbrahim, “Çevre Sorunlarının Antroposentrik Karakteri”, Felsefe Dünyası, Ankara: Türk Felsefe Dünyası Derneği Yay. 27 (1998). --------,“Çevre Bilincinin Gelişiminde Çevre Ahlâkının Önemi”, Ankara Üniversitesi İlahiyat Fakültesi Dergisi, Ankara 39/2 (1999). 9 872
ISEM2016, 3 rd International Symposium on Environment and Morality, 4-6 November 2016, Alanya – Turkey Demir Yüklenmiş Hibrid Silika Kullanılarak Sudan Arseniğin Seçimli Giderimi 1* Ayten ATEŞ and 2 Medhat Mohamed El-Molselhy *1 Cumhuriyet University, Engineering Faculty, Department of Chemical Engineering, 58140 Sivas, Turkey 2 Chemistry department, Faculty of Science, Al-Azhar University, Cairo, Egypt. Özet Demir katyonlarıyla hibrid malzemeler kullanılarak arsenik giderimi sağlandığını gösteren birçok çalışma gerçekleşmiştir. Bu çalışmalarda, yüksek demir içerikli malzemeler ile arsenik giderimi büyük başarı ile sonuçlanmıştır. Arsenik giderimi, arsenik ile demir oksitlerin elektrostatik ilişkisine bağlıdır. Bu çalışmada, farklı parçacık boyutuna sahip silikatlar, çok basit ve ucuz bir yol olan demir katyonları ile modifiye edilmiştir. Demir modifiye edilmiş örneklerde, demir oksihidroksit ve oksit fazlarını oluşturmak için 100 o C’de kurutma sonrası 150- 300 o C aralığında kalsine edilmiştir. Tüm örneklerin yapı ve bileşimi XRD, SEM/TEM ve N 2 adsorpsiyonu-desorpsiyonu yöntemleri kullanılarak karakterize edilmiştir. Modifiye edilmiş malzemeler ile sulu çözeltilerden ve içme sularından arsenik anyonlarının ayrımında kesikli deney sistemi kullanılmıştır. En yüksek arsenik ayrımı %2.2 (wt.) Fe içeren silikada 40.0 mg/g olarak bulunmuştur. Adsorbentin rejenerasyonu sonrası yaklaşık aynı adsorpsiyon kapasitesine sahip olduğu gözlenmiştir. Anahtar Kelimeler: Arsenik, adsorpsiyon, demir oksit, silika, demir modifikasyonu Abstract There are many studies containing arsenic removal via hybrid silicates containing iron cations. In these studies, arsenic removal using materials with high iron content succeed where arsenic removal depends on electrostatic relationship between arsenic and iron oxides. Therefore, in this study silicates with different particle size were modified with iron cations, which is simple and cheap method. Samples modified with iron was dried at 100 o C and calcined in a temperature range from 150 to 300 o C in order to formation of hydrated iron oxide species. Structure and composition of all samples were characterized using XRD, SEM/TEM and N 2 adsorptiondesorption. A batch experimental setup was used for removal of arsenic ions from aqueous solutions and drinking water using modified materials. Maximum arsenic removal was found as 40.0 mg/ g on silica gel containing 2.2 (wt.) % Fe. After regeneration of adsorbents, their adsorption capacity remains stable. Key words: Arsenic, adsorption, iron oxide, silica- gel, iron modification 1. Giriş Arsenik dünya yüzeyinde en yüksek risk oluşturan, çevrede geniş ölçüde yayılan riskli metallerden biridir. Uzun dönemde arsenik akciğer, karaciğer, böbrek, mesane, kanser hastalıklarına yol açmaktadir[1-4]. Yoğun ölçüde suda bulunan arsenik öldürücü etkiye de sahiptir. İçme sularında arsenik kirliliği şimdiye dek 70 ülkede görülmüş, tahmini 150 milyon insanda sağlık riski oluşturmaktadır [5,6]. WHO ve EPA'a göre içme suyunda arseniğin eşik değeri 50- 10 mg/L olmalıdır [7]. *Corresponding author: Address: Faculty of Engineering, Department of Chemical Engineering Cumhuriyet University, 58140, SivasTURKEY. E-mail address: aytates@gmail.com, Phone: +903462191010-2248 873
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ISBN 9786054735846

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