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N. SOZBIR et al./ ISEM2016 Alanya – Turkey Mezur Şekil 1. Test Düzeneği 4. Çıkan Gazın Yönetmeliğe Göre Durumu Örnek tesiste yaklaşık 40.000 ton/yıl (135 ton/gün) alüminyum cürufu, geri dönüşüm işlemine tabi tutularak çelik endüstrisi için flaks üretimi yapılacaktır. Laboratuvar deney sonucunda; 50 gr tuzlu kara alüminyum cürufunun, 25 o C ve 60 o C sıcaklığındaki su ile yıkanmasına bağlı olarak sırasıyla 23 mL ve 24 mL toplam gaz çıkışı olduğu görülmüştür. Dolayısıyla, yıkanmamış bir ton tuzlu kara alüminyum cürufunun oda sıcaklığında (25 o C) yıkanması sonucunda yaklaşık 0,46 m 3 /gün gaz çıkacaktır. Tesisin günlük cüruf yıkama kapasitesinin yaklaşık 135 ton olduğu göz önüne alındığında da, günlük toplam gaz hacminin 62,1 m 3 /gün olacağı, günde yaklaşık 16 saat (iki vardiya) çalışıldığında da saatlik gaz hacminin yaklaşık 3.89 m 3 /h olacağı tespit edilebilmektedir. İlgili tesise ait alüminyum cürufun SEM ve XRD analizleri Şekil 2 ve Şekil 3’ de görülmektedir. Analizler içerisinde karbon, fosfür ve sülfürlü bileşiklerin bulunmadığı görülmektedir. Bu analizler incelendiğinde cüruf içerisinde AlN (alüminyum nitrür) fazla miktarda olduğu ve sırası ile Al2MgO4 (Magnesium aluminate), NaCl (sodyum klorür ) ve Al2O3 (alüminyum oksit) bileşiklerinin olduğu görülmektir. Dolayısıyla tuzlu kara alüminyum cürufunun yıkama prosesi sonucunda içerdiği elelment ve bileşiklerden dolayı sadece amonyak (NH3), eser miktarda hidrojen (H₂) ve eser miktarda metan (CH4) gazları çıkışı olacaktır. 860
N. SOZBIR et al./ ISEM2016 Alanya – Turkey Element Atomik ağırlık (%) Conc. ağırlık (%) O 23.167 14.057 Na 21.004 18.312 Mg 1.103 1.017 Al 22.243 22.759 Si 0.422 0.450 Cl 30.425 40.906 K 0.760 1.127 Ca 0.740 1.124 Ti 0.136 0.247 Toplam 100 100 Şekil 2. Alüminyum Cürufun içerisinde SEM Analizi sonucu görülen elementler Yıkama sonucunda çıkan gazın debisi yaklaşık 1.1x10 -3 m 3 /sn olup, yanma için lel hacmi oluşturmamaktadır. Bu yüzden ortamda yanma riski oluşturmaz. Yanma gerçekleşse bile çabuk söner. Yıkama sonucu örnek tesisten çıkacak günlük gaz miktarının 62,1 m 3 /gün, saatlik gaz miktarının 3.89 m 3 /h olduğu esas alındığında ve ortalama gaz yoğunluğu da yaklaşık 0,66 kg/m 3 kabul edildiğin de, çıkan gazın saatlik kütlesel debisinin de 2,6 kg/h olacağı hesaplanabilmektedir. Bu değerin, Tablo 1 ’ de belirtilen değerlerin altında olduğu görülmektedir (günde iki vardiya ve 16 saat çalışıldığı esas alınmıştır). 861
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