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128 KKU Science Journal Volume 39 Number 1 Research √ÿª·≈–«‘®“√≥å ®“°‡∑§π‘§ ‡ª§‚µ√‚ø‚µ‡¡µ√’∑’Ëæ—≤π“¢÷Èπ „π°“√«‘‡§√“–ÀåÀ“ “√°≈ÿà¡´—≈‚øπ“‰¡¥å„πµ—«Õ¬à“ß ¬“∑“ß‡¿ —°√√¡ ´÷ËßÕ“»—¬À≈—°°“√‡°‘¥ªØ‘°‘√‘¬“¢Õß “√Õπÿæ—π∏å°≈ÿà¡´—≈‚øπ“‰¡¥å°—∫ 8-‰Œ¥√Õ°´’§«‘‚π≈’π ‚¥¬∑”ªØ‘°‘√‘¬“√à«¡°—∫´—≈ø“‡¡∑Õ°´“‚´≈ (SFMx) ´—≈ø“‰¥Õ–´’π (SFD) ·≈–´—≈ø“‡¡∑“´’π (SFM) „π ¿“«–∑’Ë‡ªìπ‡∫ À≈—ß®“°∑”„Àâ‡°‘¥ªØ‘°‘√‘¬“‰¥Õ–‚´- ‰∑´å‡´—π ‰¥âº≈‘µ¿—≥±å‡ªìπ “√ª√–°Õ∫ ’ â¡·¥ß´÷Ëß ¡’§à“°“√¥Ÿ¥°≈◊π· ß Ÿß ÿ¥∑’Ë§«“¡¬“«§≈◊Ëπ 500 π“‚π ‡¡µ√ æ∫«à“§à“¢’¥®”°—¥µË” ÿ¥„π°“√«‘‡§√“–Àå¢Õß SFMx SFD ·≈– SFM ¡’§à“‡∑à“°—∫ 0.0283 0.0292 ·≈– 0.0298 ¡‘≈≈‘°√—¡/≈‘µ√ µ“¡≈”¥—∫ §à“¢’¥®”°—¥„π°“√ «‘‡§√“–ÀåÀ“ª√‘¡“≥¢Õß SFMx SFD ·≈– SFM §◊Õ 0.0944 0.0973 ·≈– 0.0992 ¡‘≈≈‘°√—¡/≈‘µ√ µ“¡≈”¥—∫ §«“¡‡∑’Ë¬ß„π°“√«‘‡§√“–ÀåÕ¬Ÿà„πà«ß√âÕ¬≈– 0.41 - 5.17 §«“¡·¡àπ„π°“√«‘‡§√“–Àå· ¥ß„π√Ÿª√âÕ¬≈–°“√°≈—∫ §◊πÕ¬Ÿà„πà«ß√âÕ¬≈– 92.24 - 123.45 «‘∏’°“√∑’Ëæ—≤π“ ¢÷Èππ’È„â√’‡Õ‡®πµå„π°“√∑”ªØ‘°‘√‘¬“πâÕ¬‡¡◊ËÕ‡ª√’¬∫ ‡∑’¬∫°—∫ß“π«‘®—¬∑’Ëºà“π¡“ (Nagaraja et al., 2007) ·≈–¬—ß “¡“√∂π”‰ªª√–¬ÿ°µå„â„π°“√À“ª√‘¡“≥ “√°≈ÿà¡ ´—≈‚øπ“‰¡¥å∑’Ë¡’„πµ—«Õ¬à“ß¬“∑“ß‡¿ —°√√¡π‘¥µà“ßÊ ‡æ◊ËÕ‡ªìπ°“√§«∫§ÿ¡§ÿ≥¿“æ¢Õß¬“∑’Ë¡’®”Àπà“¬¿“¬„π ª√–‡∑» ‚¥¬¡’§«“¡·¡àπ·≈–§«“¡‡∑’Ë¬ß¥’°«à“«‘∏’ ‰π‰µ√∑å‰∑‡∑√—π ´÷Ëß‡ªìπ«‘∏’¡“µ√∞“π„π°“√«‘‡§√“–Àå ¬“°≈ÿà¡´—≈‚øπ“‰¡¥å πÕ°®“°π’È¬—ß “¡“√∂π”‡∑§π‘§ ∑’Ëæ—≤π“¢÷Èπ‰ªª√–¬ÿ°µå„â‡æ◊ËÕÀ“ª√‘¡“≥¬“°≈ÿà¡ ´—≈‚øπ“‰¡¥å∑’Ëµ°§â“ßÕ¬Ÿà„πµ—«Õ¬à“ßπ‘¥Õ◊ËπÊ ‡àπ πÈ”º÷Èß ‡π◊ÈÕ —µ«å ª≈“ ‰¢à ‡ªìπµâπ ´÷Ëß‡ªìπß“π«‘®—¬µàÕ ¬Õ¥„πÕπ“§µ ‚¥¬‡∑§π‘§∑’Ëæ—≤π“¢÷Èππ’È¡’¢âÕ¥’ §◊Õ ‡ªìπ‡∑§π‘§∑’Ë¡’§«“¡√«¥‡√Á«·≈–¡’¢—ÈπµÕπ„π°“√ «‘‡§√“–Àå‰¡à´—∫´âÕπ Õ’°∑—Èß¬—ß¡’§«“¡®”‡æ“–‡®“–®ß Ÿß µàÕ “√°≈ÿà¡´—≈‚øπ“‰¡¥å·≈–‰¡à®”‡ªìπµâÕß„âÕÿ≥À¿Ÿ¡‘ Ÿß¡“°„π¢—ÈπµÕπ°“√∑”ªØ‘°‘√‘¬“√à«¡°àÕπ°“√ «‘‡§√“–Àå °‘µµ‘°√√¡ª√–°“» ¢Õ¢Õ∫§ÿ≥ ¥√.¬ÿ∑∏æß…å Õÿ¥·πàπ ∑’Ë„Àâ§” ª√÷°…“µ≈Õ¥°“√«‘®—¬ ¿“§«‘“‡§¡’ §≥–«‘∑¬“»“ µ√å ¡À“«‘∑¬“≈—¬π‡√»«√∑’Ë„Àâ§«“¡Õπÿ‡§√“–Àå∑“ß¥â“π ‡§√◊ËÕß¡◊Õ·≈–Õÿª°√≥å„π°“√«‘®—¬ ∂“∫—π àß‡ √‘¡°“√ Õπ«‘∑¬“»“ µ√å·≈–‡∑§‚π‚≈¬’ (‚§√ß°“√ àß‡ √‘¡ °“√º≈‘µ§√Ÿ∑’Ë¡’§«“¡ “¡“√∂æ‘‡»…∑“ß«‘∑¬“»“ µ√å ·≈–§≥‘µ»“ µ√å) ∑’Ë„Àâ‡ß‘π∑ÿπ π—∫ πÿπ„π°“√»÷°…“ µàÕ√–¥—∫∫—≥±‘µ»÷°…“ ‡Õ° “√Õâ“ßÕ‘ß °¡≈—¬ µ√ß«“π‘π“¡. (2544). °“√„â¬“µâ“π®ÿ≈’æ „π —µ«å. (æ‘¡æå§√—Èß∑’Ë 3). ¿“§«‘“‡¿ —«‘∑¬“ §≥– —µ«·æ∑¬å»“ µ√å ¡À“«‘∑¬“≈—¬‡°…µ√- »“ µ√å: ”π—°æ‘¡æå¡À“«‘∑¬“≈—¬‡°…µ√»“ µ√å. 33 - 54. ‚Õ¿“ «—√–§ÿªµå. (2551). ‡§¡’¢Õß¬“ ©∫—∫ 1. ππ∑∫ÿ√’ : ”π—°æ‘¡æå æ’.‡Õ .æ√‘Èπ∑å. 218-232. Antonio Hernandez - Cardoso, B. S., Scientist, Latin American Specialist. (2553). Nitrite titration. ◊∫§âπ‡¡◊ËÕ«—π∑’Ë 7 ¡’π“§¡ 2553 ®“° http:// www.pharmacopeia.cn/v29240/usp29nf 24s0_c451.html Mohamed, A. M. (1989). Spectrophotometric Determination of some benzene sulfonamides with 7,7,8,8-tetracyanoquinodimethane. Assoc. Off. Anal. Chem. 72(6): 885 - 889. Nagaraja, P., Naik, S. D., Shrestha, A. K. and Shivakumar, A. (2007). A sensitive spectrophotometric method for the determination of sulfonamides in pharmaceutical preparations. Acta. Pharm. 57: 333 - 342. Nagaraja, P., Sunitha, K., Vasantha, R. A. and Yathirajan, H. S. (2002). Iminodibenzyl as a novel coupling agent for the
ß“π«‘®—¬ «“√ “√«‘∑¬“»“ µ√å ¡¢. ªï∑’Ë 39 ©∫—∫∑’Ë 1 129 spectrophotometric determination of sulfonamide derivatives. Eur. J. Pharm. Biopharm. 53(2): 187 - 192. Nagaraja, P., Yathirajan, H. S. Raju, C. R. Vasantha, R. A. Nagendra, P. and Hemantha Kumar, M. S. (2003). 3-Aminophenol as a novel coupling agent for the spectrophotometric determination of sulfonamide derivatives. Il Farmaco. 58(12): 1295 - 1300. Preuss, H. G., Razavi, M. H., Slemmer, D. and Zein, M. (1988). Colorimetry of p-aminohippurate in the presence of sulfomethoxazole. Clin. Chem. 34: 422 - 423. ❏❏❏❏❏
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