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Physical Principles of Electron Microscopy: An Introduction to TEM ...

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134 Chapter 5<br />

Figure 5-7. (a) Secondary-electron image <strong>of</strong> a small crystal; the side-mounted Everhart-<br />

Thornley detec<strong>to</strong>r is located <strong>to</strong>ward the <strong>to</strong>p <strong>of</strong> the image. (b) Backscattered-electron image<br />

recorded by the same side-mounted detec<strong>to</strong>r, which also shows <strong>to</strong>pographical contrast and<br />

shadowing effects. Such contrast is much weaker for a BSE detec<strong>to</strong>r mounted directly above<br />

the specimen. From Reimer (1998), courtesy <strong>of</strong> Springer-Verlag.<br />

Taking advantage <strong>of</strong> the orientation dependence <strong>of</strong> �, the whole sample is<br />

<strong>of</strong>ten tilted away from a horizontal plane and <strong>to</strong>ward the detec<strong>to</strong>r, as shown<br />

in Fig. 5-1. This increases the overall SE signal, averaged over all regions <strong>of</strong><br />

the sample, while preserving the <strong>to</strong>pographic contrast due <strong>to</strong> differences in<br />

surface orientation.<br />

To further increase the SE signal, a positively-biased electrode is used <strong>to</strong><br />

attract the secondary electrons away from the specimen. This electrode could<br />

be a simple metal plate that absorbs the electrons, generating a small current<br />

that could be amplified and used <strong>to</strong> generate a SE image. However, the<br />

resulting SE signal would be weak and noisy. The amount <strong>of</strong> electronic noise<br />

could be reduced by limiting the frequency response (bandwidth) <strong>of</strong> the<br />

amplifier, but the amplified signal might not follow the fast changes in input<br />

signal that occur when the electron probe is scanned rapidly over a nonuniform<br />

specimen.<br />

A stronger signal is obtained from an Everhart-Thornley detec<strong>to</strong>r, named<br />

after the scientists who first applied this design <strong>to</strong> the SEM. The secondaries<br />

are first attracted <strong>to</strong>ward a wire-mesh electrode biased positively by a few<br />

hundred volts; see Fig. 5-8. Most <strong>of</strong> the electrons pass through the grid and<br />

are accelerated further <strong>to</strong>ward a scintilla<strong>to</strong>r that is biased positive Vs by<br />

several thousand volts. The scintilla<strong>to</strong>r can be a layer <strong>of</strong> phosphor (similar <strong>to</strong><br />

the coating on a <strong>TEM</strong> screen) on the end <strong>of</strong> a glass rod, or a light-emitting<br />

plastic or a garnet (oxide) material, each made conducting by a thin metallic<br />

surface coating. The scintilla<strong>to</strong>r has the property (cathodoluminescence) <strong>of</strong>

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