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Nondestructive testing of defects in adhesive joints

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selected as matrix material due to the reason <strong>of</strong> easy removal <strong>of</strong> trapped air and wett<strong>in</strong>g <strong>of</strong> the<br />

powder and further maximiz<strong>in</strong>g the filler load<strong>in</strong>g . Composites are manufactured <strong>in</strong> an alum<strong>in</strong>um<br />

mold fabricated with a cavity <strong>of</strong> 8mm dia and 28 mm length. Appropriate volume fractions <strong>of</strong><br />

Terfenol-D particles are mixed with epoxy res<strong>in</strong> <strong>in</strong> a beaker. The mixed slurry is placed <strong>in</strong> a vacuum<br />

for degass<strong>in</strong>g. The degassed slurry is further poured <strong>in</strong>to the mould just before the gelation time. The<br />

mold is then sealed and placed between two permanent magnets (field strength ~ 1000 gauss). The<br />

mould is further kept on rotation at room temperature dur<strong>in</strong>g cur<strong>in</strong>g process to prevent the settl<strong>in</strong>g <strong>of</strong><br />

dense Terfenol-D particles.<br />

The magnets placed at the two ends <strong>of</strong> the mould, produce uniform horizontal magnetic field through<br />

the length <strong>of</strong> the cavity. This aligns the particulate <strong>in</strong>to cha<strong>in</strong>s or pseudo fibers fashion, which when<br />

cured get locked <strong>in</strong> the epoxy matrix results <strong>in</strong> a 1–3 composite. A 1–3 composite produces a higher<br />

stra<strong>in</strong> output than the particles are randomly aligned [3]. In addition to align<strong>in</strong>g the particles the<br />

magnetic field also further aligns the doma<strong>in</strong>s <strong>in</strong>side the particles, however, s<strong>in</strong>ce Terfenol-D is a s<strong>of</strong>t<br />

magnetic material the doma<strong>in</strong>s redistribute once the magnetic field is removed.<br />

2.2. Magneto mechanical Characterisation<br />

2.2 (a) compressive modulus.A universal <strong>test<strong>in</strong>g</strong> mach<strong>in</strong>e (Zwick 1476) is employed to determ<strong>in</strong>e<br />

the compressive modulus <strong>of</strong> the composite.<br />

2.2 (b ) Magnetostriction The stra<strong>in</strong> developed <strong>in</strong> the material is determ<strong>in</strong>ed us<strong>in</strong>g a stra<strong>in</strong> gauge<br />

and whetstone bridge setup.<br />

2.2 (c ) Magnetisation The saturation magnetization, remnant magnetic field and magnetic coercivity<br />

are determ<strong>in</strong>ed us<strong>in</strong>g walker scientific magnetometer<br />

2.3. Transducer Fabrication<br />

2.3 (a) Approach: NPOL has designed and developed Flextensional Transducers (FT) us<strong>in</strong>g<br />

peizoceramic transduction material. The effort was to fabricate flextensional transducer us<strong>in</strong>g the<br />

fabricated magnetostricitve composite material. FT consists <strong>of</strong> an elliptical alum<strong>in</strong>ium shell,<br />

encapsulated with neoprene rubber.<br />

The ma<strong>in</strong> consideration for design<strong>in</strong>g the driver us<strong>in</strong>g the GM material was the the space available <strong>in</strong><br />

the shell. Composite rods <strong>of</strong> 8 mm diameter and 28 mm length were fabricated as described above.<br />

The conceptual sketch <strong>of</strong> the arrangement <strong>of</strong> the rods is shown <strong>in</strong> Fig. 1. The numbered items are (1)<br />

magentostricitve composite rods 8 mm dia, 28 mm long [6 Nos.] (2) Tablet-type 20 mm dia, 10 mm<br />

thick Samarium-Cobalt permanent magnets [12 Nos.] (3) 375 turns <strong>of</strong> 22 SWG Solenoids [6 Nos.]<br />

(4) 30 mm dia, 27.5 mm long alum<strong>in</strong>um bobb<strong>in</strong>s [6 Nos.] (5) 8 mm thick brass magnetic de-coupler<br />

(6) I mm MS outer frame for magnetic flex return path (7) Alum<strong>in</strong>um shell [Elliptical cyl<strong>in</strong>der]. The<br />

solenoids are connected <strong>in</strong> parallel and designed to be powered by AC current with a current<br />

limitation <strong>of</strong> 5 amp.). A compressive mechanical pre-stress<strong>in</strong>g is given to the drive by elastic spr<strong>in</strong>g<br />

<strong>of</strong> the flextensional shell. For this the total length <strong>of</strong> the drive module taken is 0.5 mm more than the<br />

major axis <strong>of</strong> the shell. The drive module is <strong>in</strong>serted <strong>in</strong> the shell by mechanically press<strong>in</strong>g the shell <strong>in</strong><br />

the m<strong>in</strong>or axis. Once the drive module is <strong>in</strong>serted the press<strong>in</strong>g is removed and the shell is loaded<br />

aga<strong>in</strong>st the drive and this will give sufficient pre-stress.<br />

2.3(b) Design <strong>of</strong> magnetic circuit<br />

Magnetic circuit was designed and analysed us<strong>in</strong>g a FE model<strong>in</strong>g s<strong>of</strong>tware Vizimag R . The <strong>in</strong>put<br />

parameters are enlisted <strong>in</strong> table 1.On the basis <strong>of</strong> model<strong>in</strong>g a most suitable schemes is arrived at,<br />

and the plots <strong>of</strong> which is shown <strong>in</strong> Fig. 2 (a) and (b). Magnetostricitive composite material drive is<br />

shown <strong>in</strong> Fig. 3 and that <strong>of</strong> fabricated FT with is shown <strong>in</strong> Fig. 4.<br />

2.3 (c) Transducer measurements<br />

Measurements are made <strong>in</strong> the open water tank, keep<strong>in</strong>g the transducer at a depth <strong>of</strong> 10 m. The sound<br />

projected by the transducer is picked up by a standard B& K hydrophone. A similar FT, with<br />

monolithic Terfenol-d rod drive was also subjected to measurements us<strong>in</strong>g the same set-up and the

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