Homoleptische Methylverbindungen von Elementen der 4. und 5 ...

Praktischer Teil
Tab. 74 Atomic coordinates (10 4 ) and equivalent isotropic displacement parameters (10 -1 pm 2 ) for
[Li{O(C H ) } ][Ti (CH ) ]. U(eq) is defined as one third of the trace of the orthogonalized Uij tensor.
2 5 2 3 2 3 9
x y z U(eq)
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Ti(1) 954(1) 1346(1) 9448(1) 34(1)
Ti(2) 4093(1) 1286(1) 10428(1) 35(1)
Ti(3) -6015(1) 1106(1) 5567(1) 30(1)
Ti(4) -9149(1) 1169(1) 4546(1) 33(1)
C(8) -7488(2) 1098(2) 5038(2) 36(1)
C(1) 2611(2) 1330(2) 9924(2) 35(1)
C(2) 5496(3) 1271(2) 11024(2) 40(1)
C(13) -4581(3) 1190(2) 6072(2) 38(1)
C(9) -10566(2) 1272(2) 4169(2) 51(1)
C(12) -5960(2) 110(2) 5433(2) 40(1)
C(10) -9197(2) 186(2) 4346(2) 50(1)
C(6) 967(2) 2342(2) 9563(2) 48(1)
C(3) 4055(2) 2288(2) 10535(2) 52(1)
C(7) -474(3) 1318(2) 9093(2) 67(1)
C(4) 4420(2) 900(2) 9542(2) 48(1)
C(5) 1156(2) 962(2) 8519(2) 45(1)
C(11) -9274(2) 1505(2) 5521(2) 40(1)
C(14) -6357(2) 1443(2) 6478(2) 42(1)
C(15) -5785(2) 1741(2) 4793(2) 48(1)
C(16) 855(3) 738(2) 10276(2) 58(1)
C(17) -8882(3) 1777(2) 3770(2) 62(1)
C(18) 3746(3) 685(2) 11186(2) 63(1)
O(1) 6965(2) 639(1) 12505(1) 44(1)
O(2) 7789(1) 885(1) 11167(1) 41(1)
O(3) -2312(1) 1666(1) 6155(1) 39(1)
O(4) -3095(2) 1914(1) 7499(1) 47(1)
O(5) 7417(1) 2089(1) 12057(1) 35(1)
O(6) -2604(1) 466(1) 7071(1) 34(1)
C(71) 8007(3) -202(2) 13071(2) 65(1)
C(72) 7296(3) 0(2) 12451(2) 50(1)
C(73) 6398(5) 679(3) 12978(3) 141(3)
C(74) 5957(3) 1255(2) 13016(2) 70(1)
C(21) 7336(3) 966(2) 9915(2) 79(1)
C(22) 7437(3) 553(2) 10532(2) 52(1)
C(23) 8741(3) 1032(2) 11276(2) 68(1)
C(24) 9196(3) 989(2) 12010(2) 66(1)
C(31) -836(3) 1583(2) 6887(2) 68(1)
C(32) -1381(2) 1536(2) 6197(2) 68(1)
C(33) -2725(3) 2022(2) 5550(2) 54(1)
C(34) -2859(3) 1654(2) 4894(2) 65(1)
C(41) -2076(3) 2766(2) 8059(2) 76(1)
C(42) -2771(3) 2555(2) 7443(2) 56(1)
C(43) -3692(5) 1882(3) 7948(4) 188(4)
C(44) -4074(3) 1298(2) 8030(2) 84(2)
C(51) 6361(3) 2988(2) 11804(2) 63(1)
C(52) 7107(2) 2616(2) 11601(2) 45(1)
C(53) 7889(2) 2272(2) 12739(2) 45(1)
C(54) 8762(3) 2630(2) 12765(2) 64(1)
C(61) -1280(3) -60(2) 7806(2) 61(1)
C(62) -2149(2) 305(2) 7765(2) 41(1)
C(63) -2859(2) -65(2) 6615(2) 44(1)
C(64) -3543(3) -491(2) 6816(2) 64(1)
Li(2) -3048(4) 1309(2) 6753(3) 38(1)
Li(1) 7010(4) 1230(3) 11753(3) 39(1)
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100