ICMCTF 2012! - CD-Lab Application Oriented Coating Development

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ICMCTF 2012 Focused Topic Sessions Monday, April 23, 2012, 12:15 – 1:15 pm Pacific Salon 1-2 Coating Quality Control Solutions Nicholas Randall, Gregory Favato, and Bo Shou For more than 30 years, CSM Instruments has been developing dedicated instruments for measuring the mechanical properties of PVD and CVD coatings. The Revetest scratch tester has become the industry standard for measuring the adhesion and scratch resistance of hard coatings. With our extensive experience gained over the years, we have recently developed a new line of instruments which are intended for routine Quality Control (QC) inspection of hard coatings. Such machines are affordable, robust, and simple to operate, therefore allowing even the smallest coating manufacturer to be able to quantify coating mechanical properties to standard methods (ISO, ASTM, JIS, etc.). CSM Instruments has also worked tirelessly to increase the sensitivity and resolution of our already industry leading instrumentation. This can best be seen by looking at the development of the new Nanoindentation Tester 2 (NHT2) and the Nanotribometer 2 (NTR2). These instruments allow for more accurate measurement of hardness and frictional properties respectively by not only increasing the resolution of measurement but also by becoming a more user-friendly measurement platform. This tutorial will focus on our most recent innovations in the indentation, scratch, and tribology testing of thin films and coatings. Specific focus will be placed on recent research into the optimization of the progressive load scratch test for investigating the mechanical integrity of hard coatings. Based on nanoindentation measurements obtained from a coating-substrate system, the scratch test can be dimensioned with respect to load range and indenter geometry. The measured data from this scratch test is used to simulate spatial stress profiles and to calculate the von Mises stress characteristics and the maximum tensile stresses in the scratch direction. This can increase sensitivity of the test for specific depth regions in the coating and allow improved analysis of critical interfaces, transition layers and surface-near substrate regions. FOOD & REFRESHMENTS WILL BE PROVIDED VISIT BOOTH #203 Monday, April 23, 2012, 5:30 – 6:30 pm Royal Palm 1-3 VAMAS TWA22 Annual General Meeting Mechanical Property Measurements of Thin Films and Coatings Nigel Jennett 1 , Nicholas Randall 2 , Junhee Hahn 3 1National Physical Laboratory, UK 2 3 CSM Instruments Inc., Korea Research Institute of Standards and Science This is an open meeting that will report on the projects undertaken by VAMAS Technical Working Area 22 in (continued) x
2011/12, discuss ideas and priorities for future work, and generate new co-operative action. Current projects include evaluation of the performance of scratch testing and indentation testing and results will be reported that are being fed into International Standards (ISO) for those tests. All are warmly welcomed, especially those interested in co-operative action to generate data that would support new methods and standards in this field. VAMAS Technical Working Area 22 addresses pre-standardization needs in the general area of test method development and evaluation for the measurement of the mechanical properties of small volumes of materials, in particular thin films and coatings on substrates. Activities cover nano-mechanical measurement methods to determine the mechanical properties of surfaces, and the films or coatings themselves, as well as larger scale test methods to evaluate the performance of coating/substrate systems as a whole. Membership is open to all and the adopted activities are those that attract sufficient international partners willing to work together for the common goal. Wednesday, April 25, 2012, 4:30 – 5:30 pm Pacific Salon 1-2 Advanced 3-D Nano and Micro Scratch Testing of Thin Films with In-line Imaging Dr. Norm Gitis STLE Fellow and Chair of STLE Committee on Tribotesting Vice President of Bruker Nano Inc. Advanced 3-D scratch-adhesion tests are proposed, based on synchronization of X and Y stages and implementation of 3-D sensors that monitor simultaneously the normal load and lateral forces in all directions, while the software automatically calculates the actual friction coefficient in real time. The scratch depth is continuously monitored with an integrated capacitance sensor. The in-line imaging is performed via optical microscope with a digital camera, producing panoramic photos in the same file with friction, load, and acoustic data. Optionally, it is done with an advanced optical profiler (for micro-scratches) or AFM (for nano-scratches), all fully integrated in the CETR-APEX world-leading testing platform. All the motions of the test specimen between the microscope, profiler, and AFM are done automatically, based on the precision factory calibration of distances. Examples of impressive test results are presented and discussed for ultra-thin and relatively-thick films of various hard and soft materials. This session is intended to deepen the audience’s knowledge of the thin-film and coatings high-end metrology. Please visit Bruker Nano Inc. Booth #212 in the Exhibit Hall. xi
Page 1 and 2: I C M C T F 2 0 1 2 INTERNATIONAL C
Page 3 and 4: TABLE OF CONTENTS Welcoming Remarks
Page 5 and 6: 2012 ICMCTF SCHEDULE OF EVENTS DAY
Page 7 and 8: SYMPOSIUM A Coatings for Use at Hig
Page 9 and 10: Marco Cremona Pontificia Universida
Page 11: Exhibitor Keynote Lecture Tuesday,
Page 15 and 16: At the focus topic, from the experi
Page 17 and 18: 2012 R.F. Bunshah Annual Award & IC
Page 19 and 20: ICMCTF 2012 Graduate Student Awards
Page 21 and 22: ICMCTF 2012 thanks Plansee for thei
Page 23 and 24: ICMCTF 2012 thanks AJA Internationa
Page 25 and 26: ICMCTF 2012 thanks CemeCon for thei
Page 27 and 28: ICMCTF 2012 Short Courses April 22
Page 29 and 30: ICMCTF 2012 Planning Grid We provid
Page 31 and 32: Key to Session/Paper Numbers A Coat
Page 33 and 34: Monday Morning, April 23, 2012 Fund
Page 35 and 36: New Horizons in Coatings and Thin F
Page 37 and 38: Fundamentals and Technology of Mult
Page 39 and 40: Advanced Characterization of Coatin
Page 41 and 42: Hard Coatings and Vapor Deposition
Page 43 and 44: Tribology & Mechanical Behavior of
Page 45 and 46: Hard Coatings and Vapor Deposition
Page 47 and 48: Coatings for Use at High Temperatur
Page 49 and 50: Applications, Manufacturing, and Eq
Page 51 and 52: Wednesday Afternoon, April 25, 2012
Page 61 and 62: Thursday Afternoon Poster Sessions
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Thursday Afternoon Poster Sessions
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Page 67 and 68:
Page 69 and 70:
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Tribology & Mechanical Behavior of
Page 73 and 74:
Free Caricatures & Massages!! E-1 V
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ICMCTF 2012 EXHIBIT HALL Internatio
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I C M C T F 2012 S P O N S O R S Bo
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All in Good Measure A 24 µm scan o
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Call For Abstracts Deadline: MAY 2,
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CC800 ® /9 HIPIMS true integration
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Exhibit Hall Reception - Atlas Ball
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Kaufman & Robinson announces their
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Miba Coating Group is the specialis
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PLANSEE SE, 6600 Reutte, Austria, T
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� ��
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Plenary Talk Room: Golden Ballroom
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content. Analyses of the oxidised c
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- The control on the gradient in re
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μ = 0.4 to μ = 0.9). On the other
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Hard Coatings and Vapor Deposition
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application tests the ta-C coated d
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4:10pm C2-2/F4-2-10 Investigation o
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process with surfactant on WO3/ITO
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is already reported. To further com
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conditions. The details of the comp
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esidual stress and to the Poisson
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Coatings for Use at High Temperatur
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eactive gases with the target mater
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emerging fields. State-of-the-art t
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transparent conducting layers. Howe
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methods provide similar carrier den
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of AISI 52100 steels by developing
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deposition based on high power puls
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coatings removed from the aluminum
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spectroscopy varies from 25 at% to
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This article describes how to use s
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een demonstrated both theoretically
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Furthermore, the silane coupling ag
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10:40am A1-1-9 High temperature oxi
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10:40am B4-2-10 Understanding the d
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11:00am B5-1-10 Hard nanocrystallin
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* Sandia National Laboratories is a
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fluidized bed of tin, zinc and alum
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mechanical and chemical properties.
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duration for super-low friction see
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stainless steel DIN X42Cr13 surface
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2:30pm TS1-1-3 Surface engineering
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X-ray diffraction patterns of the Z
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11:20am B6-1-11 Direct current magn
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loading situations could help to ob
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Energetic Materials and Micro-Struc
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The present work was supported by t
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silica-based hydrophilic coatings i
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extent depending on the actual grow
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[1] F. Tasnádi, B. Alling, C. Hög
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eproducibility of the preparation o
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showed by the uncoated 4140 steel s
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polarization resistance and corrosi
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thin films in which a multiscale mo
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centers, ascribed to conduction ele
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BP-26 Characterization of laser abl
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BP-38 Stress signature of an amorph
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simultaneously optimize materials p
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CP-17 Effects of UV Light Treatment
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amorphous structure with a smooth s
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addition, it was observed that the
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EP-5 The effective Indenter concept
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the substrates directly or after ra
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as-grown films using textured Si as
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proposed memory device exhibits exc
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FP-24 Effect of hydrogen addition o
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oxide obtained was correlated to th
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Post Deadline Discoveries and Innov
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chemical bonds have also been achie
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9:40am B3-1-6 Compressive stress ge
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10:20am D2-1-8 Corrosion Resistance
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property combination is attractive
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PVD is a challenging task. The pres
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Chang, G.W.: C2-3/F4-3-3, 29; GP-3,
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Huang, K.H.: BP-33, 102 Huang, P.H.
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Moody, N.R.: F6-1-1, 7 Moon, S.: D1
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Szeremley, D.: G3-1-7, 68 Szesz, E.
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NOTES 145
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Description of Research Highlights:
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their presentations in order to eva
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NOTES 151
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153
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MARK YOUR CALENDAR FOR ICMCTF 2013!
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ICMCTF 2012! - CD-Lab Application Oriented Coating Development

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