Register your product now - Radiometer Analytical

More documents

Recommendations

Info

3. To set another electrode rotating speed at the end of the method, select “D/AOUT final” and enter, in mV, a DC constant potential between 0 and +5000 mV tobe output at the PGZ or PST050 “D/A OUT” socket at the end of the method. Thesame principle as for the “D/A OUT initial” is applied. Note that the rotation speedis set to zero by default at the end of the method (“D/A OUT final = 0”).4. Run the experiment (command “Run” - “Start”, or icon or F5 function key).The EDI101 or EDI10000 starts rotating at the selected speed when the methodrun is initiated then stops rotating at the end of this method.152VoltaLab 21/06/10/40/50/80Section 6, Chapter 1: Rotating Disc Electrode (EDI)
6.2 BipotentiostatThe bipotentiostat described hereafter is an association of two PGZ potentiostats.The following associations are also possible: PGZ100/PGZ100, PGZ100/PGZ301,PGZ100/PGZ402, PGZ301/PGZ402, PGZ402/PGZ402. The first PGZ (PGZ One)monitors a voltammetry on the disc electrode and the Vg potential is applied versusthe same reference electrode. The second PGZ (PGZ Two) polarizes the ringelectrode versus a reference electrode. The reference and auxiliary electrodes areconnected to PGZ One. The “I OUT” output of PGZ no. 1 is connected to the “A/DIN” socket of PGZ One so that the ring and disc currents can be followed versusthe disc potential applied.6.2.1 Physical connectionsFront panelPGZ Two(exampleof a PGZ402)ONE(X) INI OUTI (Y) INE OUTVg INVg OUTA/D IND/A OUTREF5AUXSENSEWORKCELL64PGZ One(exampleof a PGZ402)ONE(X) INI OUTI (Y) INE OUTVg INVg OUTA/D IND/A OUTREFAUXSENSEWORKCELLFX (blue head)AuxiliaryelectrodeBlack banana plugsWorkingelectrode (disc)12 3ReferenceelectrodeWorkingelectrode(ring)12 3 4BNC plugPL259 plugsCK112 kit of 6 connecting cablesCK112 kit of 6 connecting cablesVoltaLab 21/06/10/40/50/80 153Section 6, Chapter 2: Bipotentiostat
Page 1 and 2:
Register your product nowTo keep up
Page 3 and 4:
ContentsRegister your product now 1
Page 5 and 6:
1. General presentationDear Custome
Page 7 and 8:
Precautionary LabelsRead all labels
Page 9:
1.3 VoltaLab 21 Economical Electroc
Page 12 and 13:
1.6 VoltaLab 40 Dynamic Electrochem
Page 14:
1.8 VoltaLab 80 Universal Electroch
Page 20:
Edit the Other settings parameters.
Page 23 and 24:
2.5 Uninstalling VoltaMaster 4Volta
Page 25 and 26:
3. Getting startedFor a VoltaLab 10
Page 28:
For a VoltaLab 06RS232 cable9-pin f
Page 31 and 32:
3.3 User identificationIf you selec
Page 33 and 34:
3.5 Set up your instrumentIf you se
Page 35 and 36:
3.7 Set up the Other settings param
Page 37 and 38:
4. VoltaMaster 44.1 The VoltaMaster
Page 39 and 40:
Curve type bar - XX is the abscissa
Page 41:
4.2 Using the VoltaMaster 4 Help fi
Page 45 and 46:
4.3.1 Open Circuit PotentialThe Ope
Page 47 and 48:
Visual IFVA virtual front panel is
Page 49 and 50:
4.3.13 Pot. Dynamic EIS (Impedance)
Page 51 and 52:
4.3.17 Gal. Expert EIS (Impedance)T
Page 53 and 54:
4.3.22 Pot. Step by step CVStep by
Page 55 and 56:
4.3.28 Gal. Universal DPThe Gal. Un
Page 57 and 58:
4.3.34 Pot. Low Current CAA potenti
Page 59 and 60:
4.3.40 Auto. TrajectThe Auto. Traje
Page 61 and 62:
4.3.46 Standard calibrationThis met
Page 63 and 64:
4.3.47 Calibration by additionThis
Page 65 and 66:
4.3.53 Print ReportThe Print Report
Page 67 and 68:
The following guidances are given i
Page 69 and 70:
8. Save the sequenceThe initial dat
Page 71 and 72:
4.5.1 Before starting a sequenceChe
Page 73 and 74:
4.6 Processing curves to obtain res
Page 75 and 76:
4.6.1 Post run processing functions
Page 77 and 78:
InformationDisplay information on a
Page 79 and 80:
Evans plotDisplay the Evans diagram
Page 81 and 82:
4.7 PrintoutsThe Printpreview iconV
Page 83 and 84:
4.7.3 Preparing a printoutThe “Fi
Page 85 and 86:
4.7.5 Printing the parameters of an
Page 87:
4.7.6 Printing CurvesA curve or an
Page 90 and 91:
1. 20 curves maximun in a graphYou
Page 92 and 93:
6. Current disjunctionEffectsThe po
Page 94 and 95:
11. Out of range: -15 V to 15 VWhil
Page 96 and 97:
17. Vg overloadThis error message i
Page 98 and 99:
4.9 Troubleshooting list4.9.1 Chara
Page 100 and 101:
4.10 The ohmic drop compensation4.1
Page 102 and 103: 4.10.4 Running an experiment with a
Page 104 and 105: CGgIPpQRSTZCalibration CV STGal. Un
Page 106 and 107: Menu “File” (Routine setup mode
Page 108 and 109: Menu “Settings” (Full and Super
Page 110 and 111: Menu “File” (Routine setup mode
Page 112 and 113: Menu “Settings” (Full and Super
Page 114 and 115: 5.1.1 The front panelsPGZ100 and PG
Page 116 and 117: The “D/A OUT” socket (4)A DC vo
Page 118 and 119: 5.1.2 The rear panelsLINE FUSE T2A
Page 120 and 121: 4 connecting cords are used (see th
Page 122 and 123: 5.1.4 UseThe PGZ and PST potentiost
Page 124 and 125: 5. Background noise on measurements
Page 126 and 127: 5.1.7 Technical specificationsPGZ10
Page 128 and 129: PGZ301 PotentiostatRegulationCompli
Page 130 and 131: PGZ402 Universal PotentiostatRegula
Page 132 and 133: PST006 Educational PotentiostatRegu
Page 134 and 135: 5.1.8 CE MarkingThe PGZ100, PGZ301,
Page 136 and 137: the PGP201 internal signal generato
Page 138 and 139: 5.2.2 The rear panelLI-BATTERY3.6 V
Page 140 and 141: 5.2.3 InstallationElectrical safety
Page 142 and 143: 2. Connecting the computerSee Secti
Page 144 and 145: 3. User data lost - Press any keyTh
Page 146 and 147: 5.2.6 MaintenanceWarning!All cables
Page 148 and 149: 5.2.8 CE MarkingThe PGP201 complies
Page 150 and 151: If the EDI10000 is used:ONE(X) INI
Page 154 and 155: Cables 1 to 4 are supplied in the C
Page 156 and 157: 6.3 Rotating Ring and Disc Electrod
Page 158 and 159: PGZ TwoWORKAUXREFCell ringCell AUXC
Page 160 and 161: 6.3.5 ConclusionIt is convenient an
Page 162 and 163: 1 PGZ/PST050 “REF.” socket to t
Page 164 and 165: 6.5.2 SettingsEstablish the serial
Page 166 and 167: 166VoltaLab 21/06/10/40/50/80Sectio
Page 168 and 169: Determine the peak and integrate th
Page 170 and 171: Determine the peak and integrate th
Page 172 and 173: 6.6 ABU901 AutoburetteThe ABU901 is
Page 174 and 175: RS232 cable9-pin female / 9-pin fem
Page 176 and 177: 6.7.4 Set up your cellIf you run a
Page 178 and 179: 6.7.8 Technical specifications - HV
Page 180 and 181: 6.8 HCB005 - HCB010 - HCB020 High C
Page 182 and 183: RS232CLINE FUSE T2A L250V120/230 Va
Page 184 and 185: If it is not the case (communicatio
Page 186 and 187: 6.8.5 Set up the other settingsSet
Page 188 and 189: Environmental conditionsInterior us
Page 190 and 191: 6.9 Additional units - PGZ402 E(X)
Page 192 and 193: Check that the electrical zero and
Page 194 and 195: Click the “Settings” button and
Page 196 and 197: 6.11 External signal generator - Vg
Page 198 and 199: 6.12 Measuring an A/D IN signalUsin
show all

Register your product now - Radiometer Analytical

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?