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RS232CLINE FUSE T2A L250V120/230 Vac 47.5-63 Hz 170 VAPGZ402 rear panel115230MADE IN FRANCE RADIOMETER ANALYTICAL SASLINE FUSE T10A L250V120/230 Vac 47.5-63 Hz 800 VAHigh Current Boosterrear panelRS232CTo a mains socketLine cord 230 V(Part no. A95S001)MADE IN FRANCERADIOMETER ANALYTICAL SASPC serial port COM1(or COM2 to COM8)Caution: Connect the PC tothis socket (the 2 "RS232C"sockets are not equivalent)RS232 cable9-pin female / 9-pin femaletype: C501XPart no. A95X5016.8.2 Configure Windows and VoltaMaster 4Configure Windows and VoltaMaster 4 as explained in section 3 “Getting started”.6.8.3 Set up <strong>your</strong> instrumentsSelect the “Settings” menu then the “Instrument setup” command.182VoltaLab 21/06/10/40/50/80Section 6, Chapter 8: HCB005 - HCB010 - HCB020 High Current Boosters
Click the “Test” button. The instrument type (PGZ402) and version are displayed. Ifit is not the case (communication failure (1) message), select “VoltaLab PGZ402”for “Potentiostat”, select the communication port (1 to 8) of the PC used for theconnection to the potentiostat for “Serial port” then click again the “Test” button.Select “Booster HCB005”, “Booster HCB010” or “Booster HCB020” for “Additionalunit”.Click the “Settings” button and enter the following settings and check that the Antioscillationfilter is cleared:With this settings, a 4-electrode cell is used with the connections performed asshown on page 181. The High Current Booster is an HCB010.The Vg potential applied by the PGZ402 is directly applied to REF2 versus REF1electrode by the HCB010 (Vg IN ----Vg OUT * (Gain = +1) + (Offset = 0)).The potential of REF2 versus the REF1 is measured and saved directly(E OUT ----- E(X) IN * (Gain = +1) + (Offset = 0)).The current flowing through the WORK electrode circuit is measured on a 2.5 Arange of the HCB010. That is to say ±2.5 A corresponds to ±1 V measured at thePGZ402 I(Y) IN socket. The current is saved with no amplification and no offset(I OUT ----- I(Y) IN * (Gain = +1) + (Offset = 0)).Click the “Test” button. The instrument types (PGZ402 and High Current Booster)and versions are displayed.VoltaLab 21/06/10/40/50/80 183Section 6, Chapter 8: HCB005 - HCB010 - HCB020 High Current Boosters
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Register your product nowTo keep up
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ContentsRegister your product now 1
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1. General presentationDear Custome
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Precautionary LabelsRead all labels
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1.3 VoltaLab 21 Economical Electroc
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1.6 VoltaLab 40 Dynamic Electrochem
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1.8 VoltaLab 80 Universal Electroch
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Edit the Other settings parameters.
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2.5 Uninstalling VoltaMaster 4Volta
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3. Getting startedFor a VoltaLab 10
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For a VoltaLab 06RS232 cable9-pin f
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3.3 User identificationIf you selec
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3.5 Set up your instrumentIf you se
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3.7 Set up the Other settings param
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4. VoltaMaster 44.1 The VoltaMaster
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Curve type bar - XX is the abscissa
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4.2 Using the VoltaMaster 4 Help fi
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4.3.1 Open Circuit PotentialThe Ope
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Visual IFVA virtual front panel is
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4.3.13 Pot. Dynamic EIS (Impedance)
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4.3.17 Gal. Expert EIS (Impedance)T
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4.3.22 Pot. Step by step CVStep by
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4.3.28 Gal. Universal DPThe Gal. Un
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4.3.34 Pot. Low Current CAA potenti
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4.3.40 Auto. TrajectThe Auto. Traje
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4.3.46 Standard calibrationThis met
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4.3.47 Calibration by additionThis
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4.3.53 Print ReportThe Print Report
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The following guidances are given i
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8. Save the sequenceThe initial dat
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4.5.1 Before starting a sequenceChe
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4.6 Processing curves to obtain res
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4.6.1 Post run processing functions
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InformationDisplay information on a
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Evans plotDisplay the Evans diagram
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4.7 PrintoutsThe Printpreview iconV
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4.7.3 Preparing a printoutThe “Fi
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4.7.5 Printing the parameters of an
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4.7.6 Printing CurvesA curve or an
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1. 20 curves maximun in a graphYou
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6. Current disjunctionEffectsThe po
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11. Out of range: -15 V to 15 VWhil
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17. Vg overloadThis error message i
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4.9 Troubleshooting list4.9.1 Chara
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4.10 The ohmic drop compensation4.1
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4.10.4 Running an experiment with a
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CGgIPpQRSTZCalibration CV STGal. Un
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Menu “File” (Routine setup mode
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Menu “Settings” (Full and Super
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Menu “File” (Routine setup mode
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Menu “Settings” (Full and Super
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5.1.1 The front panelsPGZ100 and PG
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The “D/A OUT” socket (4)A DC vo
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5.1.2 The rear panelsLINE FUSE T2A
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4 connecting cords are used (see th
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5.1.4 UseThe PGZ and PST potentiost
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5. Background noise on measurements
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5.1.7 Technical specificationsPGZ10
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PGZ301 PotentiostatRegulationCompli
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PGZ402 Universal PotentiostatRegula
Page 132 and 133: PST006 Educational PotentiostatRegu
Page 134 and 135: 5.1.8 CE MarkingThe PGZ100, PGZ301,
Page 136 and 137: the PGP201 internal signal generato
Page 138 and 139: 5.2.2 The rear panelLI-BATTERY3.6 V
Page 140 and 141: 5.2.3 InstallationElectrical safety
Page 142 and 143: 2. Connecting the computerSee Secti
Page 144 and 145: 3. User data lost - Press any keyTh
Page 146 and 147: 5.2.6 MaintenanceWarning!All cables
Page 148 and 149: 5.2.8 CE MarkingThe PGP201 complies
Page 150 and 151: If the EDI10000 is used:ONE(X) INI
Page 152 and 153: 3. To set another electrode rotatin
Page 154 and 155: Cables 1 to 4 are supplied in the C
Page 156 and 157: 6.3 Rotating Ring and Disc Electrod
Page 158 and 159: PGZ TwoWORKAUXREFCell ringCell AUXC
Page 160 and 161: 6.3.5 ConclusionIt is convenient an
Page 162 and 163: 1 PGZ/PST050 “REF.” socket to t
Page 164 and 165: 6.5.2 SettingsEstablish the serial
Page 166 and 167: 166VoltaLab 21/06/10/40/50/80Sectio
Page 168 and 169: Determine the peak and integrate th
Page 170 and 171: Determine the peak and integrate th
Page 172 and 173: 6.6 ABU901 AutoburetteThe ABU901 is
Page 174 and 175: RS232 cable9-pin female / 9-pin fem
Page 176 and 177: 6.7.4 Set up your cellIf you run a
Page 178 and 179: 6.7.8 Technical specifications - HV
Page 180 and 181: 6.8 HCB005 - HCB010 - HCB020 High C
Page 184 and 185: If it is not the case (communicatio
Page 186 and 187: 6.8.5 Set up the other settingsSet
Page 188 and 189: Environmental conditionsInterior us
Page 190 and 191: 6.9 Additional units - PGZ402 E(X)
Page 192 and 193: Check that the electrical zero and
Page 194 and 195: Click the “Settings” button and
Page 196 and 197: 6.11 External signal generator - Vg
Page 198 and 199: 6.12 Measuring an A/D IN signalUsin
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