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Click the “Settings” button and enter the following settings:The potential input at the PGZ402 E(X) IN socket is measured with no gain (“Gain”= 1) and no offset (“Offset” = 0 V).The 200 pA (2e-10 A) current range is selected on the AMU130. It means that200 pA output at the AMU130 “I OUT” socket corresponds to ±1 V measured at thePGZ402 “I(Y) IN” socket. The current is measured with no gain (“Gain” = 1) and nooffset (“Offset” = 0 V).The Vg potential generated at the PGZ402 “Vg OUT” socket is imposed to theWORK electrode versus the REF with no polarity inversion (“Gain” = +1) and nooffset (“Offset” = 0 V).6.10.4 Set up your cellIf you run a sequence with the AMU130 built-in dummy cell, there is no need toedit the “Cell setup” parameters. If you run a sequence on a real cell, perform thefollowing operations:. Select the “Settings” menu then the “Cell setup” command.. Specify the reference electrode you are using (select a predefined type orselect “User defined”). Enter the area of the working electrode (WORK (WE)– Area). No auxiliary electrode is used with an AMU130 so the “AUX (CE) –Area” parameter is not significant. The other settings are to be entered if youintend to calculate a corrosion rate. In all other cases, you do not need to makeany changes to the other “Cell setup” settings.For more information, consult the Help file, keyword index:Cell setup.194VoltaLab 21/06/10/40/50/80Section 6, Chapter 10: AMU130 - PGZ402 E(X) IN and I(Y) IN sockets
6.10.5 Set up the other settingsSelect the “Settings” menu then the “Other settings” command.Select the frequency (50 Hz or 60 Hz) of your power supply. This selection is usedby VoltaMaster 4 to minimize the background noise ratio on the measurements.Check that the “Anti-oscillation filter” is cleared. The other settings are notsignificant when using a PGZ402 with an AMU130.For more information, consult the Help file, keyword index:Other settings.You are now ready to start your first experiment using a PGZ402 with an AMU130.The methods available are: Open Circuit Potential, Chrono Amperometry, Pot.Interactive CV, Pot. Tutorial CA and all Tool methods that can be used with aPGZ402.VoltaLab 21/06/10/40/50/80 195Section 6, Chapter 10: AMU130 - PGZ402 E(X) IN and I(Y) IN sockets
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Register your product nowTo keep up
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ContentsRegister your product now 1
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1. General presentationDear Custome
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Precautionary LabelsRead all labels
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1.3 VoltaLab 21 Economical Electroc
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1.6 VoltaLab 40 Dynamic Electrochem
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1.8 VoltaLab 80 Universal Electroch
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Edit the Other settings parameters.
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2.5 Uninstalling VoltaMaster 4Volta
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3. Getting startedFor a VoltaLab 10
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For a VoltaLab 06RS232 cable9-pin f
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3.3 User identificationIf you selec
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3.5 Set up your instrumentIf you se
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3.7 Set up the Other settings param
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4. VoltaMaster 44.1 The VoltaMaster
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Curve type bar - XX is the abscissa
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4.2 Using the VoltaMaster 4 Help fi
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4.3.1 Open Circuit PotentialThe Ope
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Visual IFVA virtual front panel is
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4.3.13 Pot. Dynamic EIS (Impedance)
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4.3.17 Gal. Expert EIS (Impedance)T
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4.3.22 Pot. Step by step CVStep by
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4.3.28 Gal. Universal DPThe Gal. Un
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4.3.34 Pot. Low Current CAA potenti
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4.3.40 Auto. TrajectThe Auto. Traje
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4.3.46 Standard calibrationThis met
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4.3.47 Calibration by additionThis
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4.3.53 Print ReportThe Print Report
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The following guidances are given i
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8. Save the sequenceThe initial dat
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4.5.1 Before starting a sequenceChe
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4.6 Processing curves to obtain res
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4.6.1 Post run processing functions
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InformationDisplay information on a
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Evans plotDisplay the Evans diagram
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4.7 PrintoutsThe Printpreview iconV
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4.7.3 Preparing a printoutThe “Fi
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4.7.5 Printing the parameters of an
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4.7.6 Printing CurvesA curve or an
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1. 20 curves maximun in a graphYou
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6. Current disjunctionEffectsThe po
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11. Out of range: -15 V to 15 VWhil
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17. Vg overloadThis error message i
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4.9 Troubleshooting list4.9.1 Chara
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4.10 The ohmic drop compensation4.1
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4.10.4 Running an experiment with a
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CGgIPpQRSTZCalibration CV STGal. Un
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Menu “File” (Routine setup mode
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Menu “Settings” (Full and Super
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Menu “File” (Routine setup mode
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Menu “Settings” (Full and Super
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5.1.1 The front panelsPGZ100 and PG
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The “D/A OUT” socket (4)A DC vo
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5.1.2 The rear panelsLINE FUSE T2A
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4 connecting cords are used (see th
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5.1.4 UseThe PGZ and PST potentiost
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5. Background noise on measurements
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5.1.7 Technical specificationsPGZ10
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PGZ301 PotentiostatRegulationCompli
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PGZ402 Universal PotentiostatRegula
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PST006 Educational PotentiostatRegu
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5.1.8 CE MarkingThe PGZ100, PGZ301,
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the PGP201 internal signal generato
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5.2.2 The rear panelLI-BATTERY3.6 V
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5.2.3 InstallationElectrical safety
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2. Connecting the computerSee Secti
Page 144 and 145: 3. User data lost - Press any keyTh
Page 146 and 147: 5.2.6 MaintenanceWarning!All cables
Page 148 and 149: 5.2.8 CE MarkingThe PGP201 complies
Page 150 and 151: If the EDI10000 is used:ONE(X) INI
Page 152 and 153: 3. To set another electrode rotatin
Page 154 and 155: Cables 1 to 4 are supplied in the C
Page 156 and 157: 6.3 Rotating Ring and Disc Electrod
Page 158 and 159: PGZ TwoWORKAUXREFCell ringCell AUXC
Page 160 and 161: 6.3.5 ConclusionIt is convenient an
Page 162 and 163: 1 PGZ/PST050 “REF.” socket to t
Page 164 and 165: 6.5.2 SettingsEstablish the serial
Page 166 and 167: 166VoltaLab 21/06/10/40/50/80Sectio
Page 168 and 169: Determine the peak and integrate th
Page 170 and 171: Determine the peak and integrate th
Page 172 and 173: 6.6 ABU901 AutoburetteThe ABU901 is
Page 174 and 175: RS232 cable9-pin female / 9-pin fem
Page 176 and 177: 6.7.4 Set up your cellIf you run a
Page 178 and 179: 6.7.8 Technical specifications - HV
Page 180 and 181: 6.8 HCB005 - HCB010 - HCB020 High C
Page 182 and 183: RS232CLINE FUSE T2A L250V120/230 Va
Page 184 and 185: If it is not the case (communicatio
Page 186 and 187: 6.8.5 Set up the other settingsSet
Page 188 and 189: Environmental conditionsInterior us
Page 190 and 191: 6.9 Additional units - PGZ402 E(X)
Page 192 and 193: Check that the electrical zero and
Page 196 and 197: 6.11 External signal generator - Vg
Page 198 and 199: 6.12 Measuring an A/D IN signalUsin
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