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Check that the electrical zero and the casing of the AMU130 are connectedtogether by a jumper (the non-floating mode is used). The casing socket is itselfconnected to the functional ground socket which is connected to the functionalground socket of the PGZ402 (via cable 4) and to the earth via the PGZ402 3-leadline cord.Cell (electrodes) connectionA 2-electrode (WE and REF) setting is used. The electrodes are connected to theAMU130. It means that the PGZ402 “Cell” button must not be pressed (“Cell” lampmust be off).POTENTIALCELLEXT. +0-1V WORKEXT.Working electrodeAMU130POWERONOFFSETCURRENTFILTERINT.RANGE REF.2nA200pAReference electrodeOFF±1V 20nA1ms 10Operation principleThe Vg potential scan defined in VoltaMaster 4 is output at the Vg OUT socket ofthe PGZ402. The AMU130 imposes Vg to the WE electrode versus the REF andmeasures the current (measurement range = 200 pA, 2 nA, 20 nA). The directpotential and I measured current are input at the E(X) IN and I(Y) IN sockets of thePGZ402.6.10.2 Configure Windows and VoltaMaster 4Configure Windows and VoltaMaster 4 as explained in section 3 “Getting started”.6.10.3 Set up <strong>your</strong> instrumentsSwitch on the PGZ402.Click the icon in the General bar or select the “File” menu then the “Newsequence” command. The Laboratory logbook window of a new sequence isopened.Select the “Settings” menu then the “Instrument setup” command.192VoltaLab 21/06/10/40/50/80Section 6, Chapter 10: AMU130 - PGZ402 E(X) IN and I(Y) IN sockets
Declare the AMU130 as a “Potentiostat (X/Y/Vg)” in the “Additional unit”.Click the “Test” button. The instrument type (PGZ402) and version are displayed.If it is not the case (communication failure (1) message), select “VoltaLab PGZ402”for “Potentiostat”, select the communication port (1 to 8) of the PC used for theconnection to the PGZ402 for “Serial port” then click again the “Test” button.On the AMU130 perform the following settings:. Power switch to “On”.. Potential switch to “Ext.”.. “Cell Ext./Int.” switch to “Int.” to use the AMU130 built in dummy cell or “Ext.” touse a real cell with 2 electrodes (REF and WORK) connected to the AMU130.. Range switch to “200 pA” as an example. This switch sets the AMU130 currentmeasurement range.Use with a real cell (electrodes)POTENTIALCELLEXT. +0-1V WORK WEEXT.POWERONOFFOFFSETCURRENTFILTERAMU130INT.RANGE2nA±1V 20nA1ms 10200pAREF.electrodeREFelectrodeUse with the AMU130 dummy cellPOTENTIALEXT. +0-1VPOWERCURRENTON OFFSETFILTERAMU130CELLWORKEXT.INT.RANGE REF.2nA200pAOFF±1V 20nA1ms 10VoltaLab 21/06/10/40/50/80 193Section 6, Chapter 10: AMU130 - PGZ402 E(X) IN and I(Y) IN sockets
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Register your product nowTo keep up
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ContentsRegister your product now 1
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1. General presentationDear Custome
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Precautionary LabelsRead all labels
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1.3 VoltaLab 21 Economical Electroc
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1.6 VoltaLab 40 Dynamic Electrochem
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1.8 VoltaLab 80 Universal Electroch
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Edit the Other settings parameters.
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2.5 Uninstalling VoltaMaster 4Volta
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3. Getting startedFor a VoltaLab 10
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For a VoltaLab 06RS232 cable9-pin f
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3.3 User identificationIf you selec
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3.5 Set up your instrumentIf you se
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3.7 Set up the Other settings param
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4. VoltaMaster 44.1 The VoltaMaster
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Curve type bar - XX is the abscissa
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4.2 Using the VoltaMaster 4 Help fi
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4.3.1 Open Circuit PotentialThe Ope
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Visual IFVA virtual front panel is
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4.3.13 Pot. Dynamic EIS (Impedance)
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4.3.17 Gal. Expert EIS (Impedance)T
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4.3.22 Pot. Step by step CVStep by
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4.3.28 Gal. Universal DPThe Gal. Un
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4.3.34 Pot. Low Current CAA potenti
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4.3.40 Auto. TrajectThe Auto. Traje
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4.3.46 Standard calibrationThis met
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4.3.47 Calibration by additionThis
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4.3.53 Print ReportThe Print Report
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The following guidances are given i
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8. Save the sequenceThe initial dat
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4.5.1 Before starting a sequenceChe
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4.6 Processing curves to obtain res
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4.6.1 Post run processing functions
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InformationDisplay information on a
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Evans plotDisplay the Evans diagram
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4.7 PrintoutsThe Printpreview iconV
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4.7.3 Preparing a printoutThe “Fi
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4.7.5 Printing the parameters of an
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4.7.6 Printing CurvesA curve or an
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1. 20 curves maximun in a graphYou
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6. Current disjunctionEffectsThe po
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11. Out of range: -15 V to 15 VWhil
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17. Vg overloadThis error message i
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4.9 Troubleshooting list4.9.1 Chara
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4.10 The ohmic drop compensation4.1
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4.10.4 Running an experiment with a
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CGgIPpQRSTZCalibration CV STGal. Un
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Menu “File” (Routine setup mode
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Menu “Settings” (Full and Super
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Menu “File” (Routine setup mode
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Menu “Settings” (Full and Super
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5.1.1 The front panelsPGZ100 and PG
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The “D/A OUT” socket (4)A DC vo
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5.1.2 The rear panelsLINE FUSE T2A
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4 connecting cords are used (see th
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5.1.4 UseThe PGZ and PST potentiost
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5. Background noise on measurements
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5.1.7 Technical specificationsPGZ10
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PGZ301 PotentiostatRegulationCompli
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PGZ402 Universal PotentiostatRegula
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PST006 Educational PotentiostatRegu
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5.1.8 CE MarkingThe PGZ100, PGZ301,
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the PGP201 internal signal generato
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5.2.2 The rear panelLI-BATTERY3.6 V
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5.2.3 InstallationElectrical safety
Page 142 and 143: 2. Connecting the computerSee Secti
Page 144 and 145: 3. User data lost - Press any keyTh
Page 146 and 147: 5.2.6 MaintenanceWarning!All cables
Page 148 and 149: 5.2.8 CE MarkingThe PGP201 complies
Page 150 and 151: If the EDI10000 is used:ONE(X) INI
Page 152 and 153: 3. To set another electrode rotatin
Page 154 and 155: Cables 1 to 4 are supplied in the C
Page 156 and 157: 6.3 Rotating Ring and Disc Electrod
Page 158 and 159: PGZ TwoWORKAUXREFCell ringCell AUXC
Page 160 and 161: 6.3.5 ConclusionIt is convenient an
Page 162 and 163: 1 PGZ/PST050 “REF.” socket to t
Page 164 and 165: 6.5.2 SettingsEstablish the serial
Page 166 and 167: 166VoltaLab 21/06/10/40/50/80Sectio
Page 168 and 169: Determine the peak and integrate th
Page 170 and 171: Determine the peak and integrate th
Page 172 and 173: 6.6 ABU901 AutoburetteThe ABU901 is
Page 174 and 175: RS232 cable9-pin female / 9-pin fem
Page 176 and 177: 6.7.4 Set up your cellIf you run a
Page 178 and 179: 6.7.8 Technical specifications - HV
Page 180 and 181: 6.8 HCB005 - HCB010 - HCB020 High C
Page 182 and 183: RS232CLINE FUSE T2A L250V120/230 Va
Page 184 and 185: If it is not the case (communicatio
Page 186 and 187: 6.8.5 Set up the other settingsSet
Page 188 and 189: Environmental conditionsInterior us
Page 190 and 191: 6.9 Additional units - PGZ402 E(X)
Page 194 and 195: Click the “Settings” button and
Page 196 and 197: 6.11 External signal generator - Vg
Page 198 and 199: 6.12 Measuring an A/D IN signalUsin
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