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Scientific and Technical Aerospace Reports Volume 38 July 28, 2000

Scientific and Technical Aerospace Reports Volume 38 July 28, 2000

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pathways to precursors that produce high purity, two phase In2O3-SnO2. The precursors were formed by complexation of tin with<br />

any oxide lig<strong>and</strong>s to give the ammonium salt (NH4). Thermal studies of these precursors were carried out by thermal gravimetry<br />

(TG) <strong>and</strong> differential scanning calorimetry (DSC). Further studies by Fourier transform infrared spectroscopy (FTIR) <strong>and</strong> nuclear<br />

magnetic resonance spectroscopy (NMR) were also conducted.<br />

Author<br />

Thermodynamic Properties; Combustion Chemistry; Combustion Products; Ito (Semiconductors); Nitrogen Oxides; Metal<br />

Oxides<br />

<strong>2000</strong>0065664 Los Alamos National Lab., NM USA<br />

Quantification of damage evolution for a micromechanical model of ductile fracture in spallation of tantalum<br />

Zurek, A. K.; Thissell, W. R.; Tonks, D. L.; Hixon, R.; Addessio, F.; Dec. 31, 1997; 10p; In English; Mechanical <strong>and</strong> physical<br />

behavior of materials under dynamic loading (EURO/DYMAT)<br />

Report No.(s): DE97-005014; LA-UR-97-791; No Copyright; Avail: Department of Energy Information Bridge<br />

The authors present quantification of micromechanical features such as voids that comprise the ductile fracture obtained<br />

under uniaxial strain condition in a spall test of commercial purity tantalum. Two evolutionary parameters of ductile fracture void<br />

formation are quantified: (i) the void volume fraction (porosity) <strong>and</strong> its distribution with respect to the distance from the main<br />

spall fracture plane, <strong>and</strong> (ii) void diameter distribution.<br />

NTIS<br />

Damage; Ductility; Fracture Mechanics; Quantitative Analysis<br />

<strong>2000</strong>0067654 Florida Agricultural <strong>and</strong> Mechanical Univ., Tallahassee, FL USA<br />

Micromechanical Characterization <strong>and</strong> Texture Analysis of Direct Cast Titanium Alloys Strips Final Report<br />

Jun. 20, <strong>2000</strong>; 73p; In English; Original contains color illustrations<br />

Contract(s)/Grant(s): NAG1-1866; No Copyright; Avail: CASI; A04, Hardcopy; A01, Microfiche<br />

This research was conducted to determine a post-processing technique to optimize mechanical <strong>and</strong> material properties of a<br />

number of Titanium based alloys <strong>and</strong> aluminides processed via Melt Overflow Solidification Technique (MORST). This technique<br />

was developed by NASA for the development of thin sheet titanium <strong>and</strong> titanium aluminides used in high temperature<br />

applications. The materials investigated in this study included conventional titanium alloy strips <strong>and</strong> foils, Ti-1100, Ti-24Al-11Nb<br />

(Alpha-2), <strong>and</strong> Ti-48Al-2Ta (Gamma). The methodology used included micro-characterization, heat-treatment, mechanical processing<br />

<strong>and</strong> mechanical testing. Characterization techniques included optical, electron microscopy, <strong>and</strong> x-ray texture analysis. The<br />

processing included heat-treatment <strong>and</strong> mechanical deformation through cold rolling. The initial as-cast materials were evaluated<br />

for their microstructure <strong>and</strong> mechanical properties. Different heat-treatment <strong>and</strong> rolling steps were chosen to process these materials.<br />

The properties were evaluated further <strong>and</strong> a processing relationship was established in order to obtain an optimum processing<br />

condition. The results showed that the as-cast material exhibited a Widmanstatten (fine grain) microstructure that developed into<br />

a microstructure with larger grains through processing steps. The texture intensity showed little change for all processing performed<br />

in this investigation.<br />

Derived from text<br />

Characterization; Mechanical Properties; Micromechanics; Textures; Titanium Alloys; Titanium Aluminides; Metal Strips; Cast<br />

Alloys<br />

52<br />

27<br />

NONMETALLIC MATERIALS<br />

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<strong>2000</strong>0062452 Saclay Research Centre, Inst. National des Sciences et Techniques Nucleaires, Gif-sur-Yvette, France<br />

Conformation <strong>and</strong> arrangement of polyelectrolytes in semi-diluted solution: A study by small angle neutrons scattering<br />

Spiteri, M. N.; Mar. 25, 1997; 205p; In French; In English<br />

Report No.(s): DE98-732052; FRCEA-TH-608; No Copyright; Avail: Department of Energy Information Bridge<br />

Polyelectrolytes have particular physical <strong>and</strong> chemical properties <strong>and</strong> can thus be used for instance for petroleum production.<br />

Some of their microscopic properties have been studied in this work. With the particular zero average contrast technique, the small<br />

angle neutron scattering allows to directly know the form factors in semi-diluted solutions of polyelectrolytes where the chains<br />

are mixed. Another measure leads to the crystal structure. The electrostatic screen effects when salt is added in aqueous solutions

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