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Advances in Fingerprint Technology.pdf

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Procedure<br />

1. Fill the spray unit with the work<strong>in</strong>g n<strong>in</strong>hydr<strong>in</strong> solution and spray the<br />

surface conta<strong>in</strong><strong>in</strong>g the latent pr<strong>in</strong>t from a distance of about 6 <strong>in</strong>.<br />

2. Allow the solvent to evaporate and then repeat the spray<strong>in</strong>g process.<br />

3. After spray<strong>in</strong>g, the surface can be heated with an <strong>in</strong>frared lamp or<br />

steam iron for a short period. Be careful not to overheat the surface<br />

and do not allow the heat source to come <strong>in</strong>to direct contact with the<br />

surface.<br />

4. Alternatively, leave the specimen at room temperature until the latent<br />

pr<strong>in</strong>t fully develops. It may take quite a bit longer to develop pr<strong>in</strong>ts<br />

at room temperature than it would if the development is heat<br />

enhanced. However, it often yields more satisfactory results.<br />

As just noted <strong>in</strong> connection with the n<strong>in</strong>hydr<strong>in</strong> solution formulation, a<br />

number of latent pr<strong>in</strong>t <strong>in</strong>vestigators have recently focused attention on reformulat<strong>in</strong>g<br />

n<strong>in</strong>hydr<strong>in</strong>, its analogues, and other chemicals that are commonly<br />

sprayed (such as DFO) <strong>in</strong> solvents/vehicles other than Freon 113. Freon 113<br />

(CFC 113, 1,1,2-trichlorotrifluoroethane) was <strong>in</strong>cluded <strong>in</strong> the “Montreal Protocol”<br />

signed <strong>in</strong> 1987 which banned CFCs <strong>in</strong> most of the <strong>in</strong>dustrialized<br />

countries because of concerns about the ozone layer. It appears likely that<br />

CFCs will not be available for this purpose. It should be noted that Watl<strong>in</strong>g<br />

and Smith 116 and Hewlett, Sears, and Suzuki 117 used heptane as the solvent<br />

because of the result<strong>in</strong>g reagent’s performance; heptane is extremely flammable.<br />

Margot and Lennard 9 noted that they have substituted ma<strong>in</strong>ly petroleum<br />

ether, even though care and attention are necessary because of the<br />

potential fire hazard. Jungbluth 118 explored an <strong>in</strong>dustrial solvent called Genesolv<br />

2000 for both n<strong>in</strong>hydr<strong>in</strong> and DFO and found it to be satisfactory, and<br />

Hewlett et al. 117,119 found the hydrofluorocarbons (HFCs) HFC4310mee and<br />

HFE7100 to be promis<strong>in</strong>g n<strong>in</strong>hydr<strong>in</strong> solvents, but not as good overall as the<br />

heptane based formulation.<br />

Marquez described a modified n<strong>in</strong>hydr<strong>in</strong> development procedure applicable<br />

to carbonless form documents. 120 Here, the n<strong>in</strong>hydr<strong>in</strong> solution was<br />

prepared <strong>in</strong> ethanol and heptane. Filter paper pieces the size of the document<br />

were saturated with the n<strong>in</strong>hydr<strong>in</strong> solution and then allowed to dry. The<br />

document was then sandwiched between the filter papers and heat applied<br />

for 30 m<strong>in</strong>, after which the document was placed <strong>in</strong> a humid chamber. This<br />

method was said to prevent the n<strong>in</strong>hydr<strong>in</strong> solvent from caus<strong>in</strong>g runn<strong>in</strong>g of<br />

the writ<strong>in</strong>g on the carbonless document. Pressly described the successful<br />

process<strong>in</strong>g of latent pr<strong>in</strong>ts on latex gloves us<strong>in</strong>g a n<strong>in</strong>hydr<strong>in</strong> dipp<strong>in</strong>g procedure,<br />

but with no heat<strong>in</strong>g. 121 Margot and Lennard said that heat acceleration

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