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Hall marks on gold & silver plate

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ASSAY. : WASTE AND SWEEP. 137<br />

ASSAY BY MEANS OF THE SPECTROSCOPE.<br />

Before c<strong>on</strong>cluding our account of the Assay Offices of the<br />

United Kingdom, we may here briefly notice the new system of<br />

assay of the precious metals by means of the spectroscope, recently<br />

proposed by Mr. J. Norman Lockyer, F.R.S. Experiments have<br />

been c<strong>on</strong>ducted at the Mint to ascertain the practicability of the<br />

scheme and determine whether it would be possible to it. adopt Mr.<br />

the aid<br />

Roberts, Chemist of the Mint, expresses an opini<strong>on</strong> that by<br />

of the spectroscope differences of compositi<strong>on</strong> more minute than the<br />

Tooou^h part might be readily distinguished.<br />

The Deputy Master of the Mint (Mr. C. W. Fremantle), in his<br />

Mr. Roberts<br />

report for the year 1873, states that he had requested<br />

to render every assistance to Mr. Lockyer in developing a process<br />

of quantitative spectrum analysis, which might with advantage re-<br />

place the methods of assay, or at any rate of verificati<strong>on</strong>, in use at<br />

the Mint. Experiments c<strong>on</strong>ducted by Mr. Lockyer and Mr. Roberts<br />

were c<strong>on</strong>tinued throughout the early part of the year, and the results<br />

were communicated in a paper to the Royal Society, who have directed<br />

their publicati<strong>on</strong> in the "<br />

Philosophical Transacti<strong>on</strong>s." As,<br />

however, these researches were of the nature of laboratory experiments<br />

merely, it became necessary to c<strong>on</strong>duct a series under c<strong>on</strong>diti<strong>on</strong>s<br />

more nearly approaching those which would occur in actual<br />

practice, and instructi<strong>on</strong>s were given that such experiments should<br />

be c<strong>on</strong>ducted in the Mint itself. Instruments have been obtained,<br />

and arrangements have now been completed for this branch of the<br />

work.<br />

WASTE AND SWEEP.<br />

The sweep is composed of cinders or dust from the forge, the<br />

sweepings of the workshop, broken crucibles, the dross which adheres<br />

to the ingots of metal after fusi<strong>on</strong>, and of every waste which<br />

can possibly c<strong>on</strong>tain minute particles of <strong>gold</strong> and <strong>silver</strong>, which had<br />

escaped the notice of the workman, or had become dispersed and<br />

lost in the manipulati<strong>on</strong> of the metals.<br />

This sweep is washed over a fine hair sieve, and the more per-<br />

ceptible porti<strong>on</strong>s of metal separated and refined ;<br />

but the remainder<br />

is called by the French les regrets, yet c<strong>on</strong>tain impalpable particles,<br />

and is usually sold to pers<strong>on</strong>s who have the necessary utensils and<br />

appliances, and who, by means of mercury mills, about the size of a<br />

coffee mill, burning it in the crucible, and by the employment of<br />

fluxes of saltpetre, etc., are able to extract whatever metal may remain.<br />

It is then cupelled to determine the proporti<strong>on</strong>s of <strong>gold</strong> and<br />

<strong>silver</strong> eliminated in the process.<br />

In large establishments the waste and sweep form a c<strong>on</strong>siderable<br />

item. We may especially notice the coinage operati<strong>on</strong>s at the<br />

L<strong>on</strong>d<strong>on</strong> Mint. The large <strong>gold</strong> coinage which commenced in 1871,<br />

and was finished in June, 1873, amounted to ,^24,500,000 sterling.<br />

The value of the metal actually deficient during the operati<strong>on</strong> was

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