Clw@terizclon of tL*Mi. ,1cid in Di&tu',t Pho@dicd Dotuge Fw.d tn ...

T!. chrcdatosm obrliftd toB slandad $lurid w idori@l eirh rhx oblliEt tm
spik d solution cont jninS m .quivalot co.centnlion. Th€ cprcmradv. chematogms
(ngw 3.22) show.d no olhd pe.Is on fi€ Fteniion rihe of..tirizin€ dd cQhrlospotiB ih.
eidtion tih6 did m| clang.. A@.dinely, rb. proFsd tulhod @ b. @ili&Ed
sl€ctiv€. Th€ coGlarion c@fficimls (!blc 3,126)
detcmined Ior ell the degs denoNtr4r.d .xcell@r
lintuig in th. tugc of 2-50 ,rghl r.
y=@856x 66123
y=11909x+59194
y=l7l22x+19A92
y=l392Jr+65711
kge$im stdinix @1d tNitirit!
LOa t,oD
0.211
00t6
0.012
Th. cnsirivity of rh. meinod w.s.valnated (rablc Ll26) by ddmining the LOD md LOQ
fot dl lhe druSs asyed. The LOD eslisaied s ihe mowi ofdtugs fdjrhing a siglal thra
r rbe $c noi$ (s^=3/l) and LOQ 6 @cidd.d s tbe low*r @m!iri@
lin6 sFt
a!.lyad widr @.piahL @ufuy md
pFction (20olo) for all th. ealyes.
Psision M n4ued in tcm of
GF.ralility of appliedon {d
n.!ll@@1. A.cur&t dd pEcision \m
dct mined six iines per concarra,liod
(r.blc 3.127). within- ard b.r*qiay
pEcisior rElre! e giv6 in r.bl€ 3.128.
%R.cov€nes ed %RSD valEs weE used
10 .xpB @l@y &d P@ision. stad:rd
addition and @ovat €xFircnrs wG
al$.ond@ted !o dehine the accuacy of
lh. pFst medod for the q@rific*ion of
cairiziE, cephalqin, efotaxitr dd etoidorc.
aewet @d paniu of tlf tulod
0.23
l2@/, 100.1
968
t2tt%
0.61
0.ll
0.21
LI5 100.!
0.34
0.73 100.21
Mcthod mbwlls! md ruggedncls w@ deremincd by dat,zirS sm€ smple ar mmal
op€Btitrg @ndilio6 &d also by ch&ging son opd.liDg analtlical conditioff s*h Es
qv.laglh, oobil. ptas @npositiol! llow '!1e, i.srul@r .nd a!.tr!r IlE Ehrire
staftiad devi.riotr ir @h ce es foud mr norc rhd 42yo. IrE n.rhod @ fttthd
0.001
t23