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Clw@terizclon of tL*Mi. ,1cid in Di&tu',t Pho@dicd Dotuge Fw.d tn ...

Clw@terizclon of tL*Mi. ,1cid in Di&tu',t Pho@dicd Dotuge Fw.d tn ...

Clw@terizclon of tL*Mi. ,1cid in Di&tu',t Pho@dicd Dotuge Fw.d tn ...

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k meh Fon<strong>in</strong> !t at 3145.9? di , dipbdic chl<strong>in</strong> is obedcd at 2913 @r .nd C=O bond<br />

ot6.(!d ar 159?-28 mn. Th. €k ab$btion fo. es obs€d al2030 d'' v6 drc ro<br />

h.aw weidt <strong>of</strong> sulphu grup. C=O stdch<strong>in</strong>g w obeped at loM fr€quency a conpcd<br />

to p.Mt &!g i... ar 1597,28 m''.<br />

S<strong>in</strong>elct <strong>of</strong>^'tl, apFared .t 2,49 ppm, etile signrl for s@nddy dircs sppened !t 6.3ppm.<br />

Th. ptoton <strong>of</strong> pipeE<strong>in</strong>. nng app€.red d 3-83 and at 467 ppn. A t ipld obs.d€d at 3.84l.9t<br />

ppo for t$o preront ir dE Cft M dt O i! cH2CtUO. Th. Foron <strong>of</strong> cH thc<br />

nc<strong>in</strong>yldilh.nyl grup is shoM by ! broad bul *$l s<strong>in</strong>gl.t *<strong>tn</strong>ch app.!r.d al5 4lPpn. Th€<br />

ehad. Dift protos appqlld at 7.147.32 ppi while O.F is m s<strong>in</strong>elci at 6l0jppm for<br />

th. cdboxylic eid eroup llrl c@68.d th! sa <strong>of</strong> @dio!<br />

Ma ttugtuntation spectw <strong>of</strong>TU<br />

G^CT<br />

TrbL 3JlE<br />

P|r*tcal and spectscopic daa olconPound n4<br />

l.(2{2{+b.n2hrdrrlpiFE<strong>in</strong>- | -yl/.lhoxyF@tyllhio@<br />

412.5t<br />

lTfc<br />

l9?.r 3(1.36, 133.2(6.32), 2tr.r5(16.21).<br />

148

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