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Composite Materials Research Progress

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Conclusion<br />

An Experimental and Analytical Study of Unidirectional Carbon Fiber… 161<br />

(a) (b)<br />

Figure 28. Simulated micro damage patterns. (a) Weak interface, (b) Strong interface.<br />

Using the solution impregnation and filament winding techniques, an innovative<br />

manufacturing method was introduced to manufacture nano-phased carbon/epoxy prepreg<br />

tapes/tows from a nanoparticle modified epoxy resin system.<br />

It was seen from TGA that the as-prepared nanocomposites were thermally more stable<br />

than their neat counterparts. An improvement of about 7 0 C was noticed. The improvement in<br />

thermal stability was believed to have been caused by increased cross-linking and better<br />

interactions between the epoxy and SiC nanoparticles.<br />

As seen with DSC and DMA, an improvement in glass transition temperature (Tg) of the<br />

nano-phased system was about 5 0 C. The improvement is due to the restricted mobility of the<br />

chain segments in the presence of SiC nanoparticles, as a result of a greater number of crosslinked<br />

polymer chains.<br />

Response of nano SiC infused composites under flexure loading showed significant<br />

improvements in strength as well as stiffness over the neat ones. On an average the increment<br />

in strength and stiffness was 32% and 20% respectively over the neat systems. It is believed<br />

that the higher strength of the SiC systems is attributed to better interfacial bonding and the<br />

resistance offered by the nanoparticles to crack propagation.<br />

In respect of tensile strength and stiffness, the nanocomposite systems offered<br />

improvements between 7 and 10%. It was seen that all the test coupons (neat and nanophased)<br />

failed in the gage length and failure modes were as described in the ASTM standard.<br />

This nominal improvement in the tensile properties was believed to have occurred because in<br />

tension, stresses in fibers were more dominant than in the nano-phased matrix and the<br />

property improvement is merely due to the improved properties of the resin.<br />

Monte Carlo simulation technique has been established to simulate unidirectional layered<br />

neat and nano-phased composites. The simulation results are in agreement with the<br />

experimental results. Tensile failure process was simulated and the damage zone and micro-

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