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Composite Materials Research Progress

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Recent Advances in Discontinuously Reinforced Aluminum… 293<br />

room temperature for only four passes (Fig. 19(b)). Moreover, the grain boundaries of<br />

submicron grains of the composite are diffused comparing to a well defined structure of Al<br />

grains. The selected area electron diffraction (SAD) patterns of pure Al and the composite<br />

reveal numerous spot features indicating the presence of an array of many ultarfine grains<br />

having random distribution of orientations (insets of Figs. 1(9a)-(b)). The tensile strength of<br />

the composite increases from 97 to 249 MPa after four ECAP passes.<br />

Figure 20. TEM micrograph of Al/5 vol.% Al 2O 3 nanocomposite fabricated by HPT consolidation of<br />

raw material powders under 1.5 GPa [21].<br />

Figure 21. Tensile stress-strain curves of Al samples (1,2) and Al/5 vol.% Al 2O 3 samples (3, 4, 5)<br />

fabricated by HPT consolidation under the pressure of 1.5 GPa and tested at 300 ºC at strain rates of 10 -<br />

4 s -1 (1,3) and 10 -3 s -1 (2, 4) and at 400 ºC at a strain rate of 10 -4 s -1 (5) [21].

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