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Composite Materials Research Progress

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280<br />

S.C. Tjong<br />

applications. Goujon et al. prepared the Al 5000/AlN (4-30 vol.%) nanocomposites though<br />

cryomilling of 5000 Al powder (380 nm) and AlN particle (150 nm) followed by hot pressing<br />

[12, 13]. Cryomilling for 6 h is required to obtain a good homogeneity of powder mixtures.<br />

The crystallite sizes of Al and AlN in the powders are reduced to about 49 and 30 nm,<br />

respectively. Hot pressing leads to homogeneous dispersion of the AlN phase in the Al alloy<br />

matrix and to an increase of the crystallite size of Al to submicrometer regime but not of AlN<br />

(Fig. 6). The microstructure of this composite consists of UFG aluminum grains free of AlN<br />

particles and regions dispersed with AlN nanoparticles.<br />

Figure 4. SEM micrograph showing the microstructure of as-cast A356/2%SiC nanocomposite [10].<br />

Figure 5. TEM micrograph showing agglomeration of particulates at the grain boundary of Al/5 vol.%<br />

Al2O 3 nanocomposite. The mean size of alumina nanoparticles is ~ 50 nm [36].

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