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Properties of hemp fibre polymer composites -An optimisation of ...

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a: Raw <strong>hemp</strong> bast<br />

c: P. rad. treated <strong>hemp</strong><br />

b: Water retted <strong>hemp</strong><br />

d: Hemp yarn<br />

Figure 4. SEM microscopy photos <strong>of</strong> transverse composite sections recorded at low and<br />

high magnification with the defibrated <strong>hemp</strong> <strong>fibre</strong>s. The small inset pictures have a scale<br />

bar length <strong>of</strong> 200 μm and the background pictures 20 μm.<br />

Composite mechanical properties<br />

The tensile strength and stiffness <strong>of</strong> the fabricated <strong>composites</strong>, corrected for porosity are<br />

presented in Figure 6 and 7, respectively. The terms σcup and Ecp are calculated from the<br />

measured strength and stiffness (σcu and Ec) using nσ=2.1 and nE=1 in Equation 9.<br />

Finally, the <strong>fibre</strong> strength and stiffness determined from σcup and Ecp are calculated from<br />

Equation 9 and presented in Table 4.<br />

Filament winding and hand lay-up were used for preparation <strong>of</strong> <strong>fibre</strong> sheets for<br />

impregnation in epoxy leading to the procedures for composite fabrication. These two<br />

fabrication techniques were compared using <strong>hemp</strong> yarn. The curve for composite tensile<br />

strength versus <strong>fibre</strong> volume fraction showed a slightly higher slope with the wound<br />

<strong>fibre</strong>s than with the lay-up <strong>of</strong> <strong>fibre</strong>s (Figure 6a). The calculated <strong>fibre</strong> tensile strength with<br />

the wound <strong>hemp</strong> yarn was therefore higher (728 MPa) and also with lower standard<br />

deviation (44 MPa) than with the hand lay-up <strong>of</strong> <strong>hemp</strong> yarn (677 ± 92 MPa, Table 4).<br />

The failure strain <strong>of</strong> these <strong>composites</strong> were 1.6 – 1.8% and based on this the failure stress<br />

<strong>of</strong> the epoxy matrix was 39 – 43 MPa (Table 4). For composite stiffness versus the <strong>fibre</strong><br />

content, the curves for the wound <strong>fibre</strong>s and the lay-up <strong>of</strong> <strong>fibre</strong>s showed similar slopes<br />

(Figure a). The determined <strong>fibre</strong> stiffness did not therefore appear to be much affected by<br />

the preparation method, and the determined <strong>fibre</strong> stiffness was 60 – 61 GPa (Table 4).<br />

For both <strong>fibre</strong> tensile strength and stiffness, the standard deviation obtained with hand<br />

lay-up was twice the standard deviation obtained with filament winding.<br />

132 Risø-PhD-11

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