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Properties of hemp fibre polymer composites -An optimisation of ...

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2000) and their orientation gave thereby an indication <strong>of</strong> the micr<strong>of</strong>ibril orientation.<br />

SEM observations <strong>of</strong> P. radiata Cel 26 defibrated and delignified <strong>hemp</strong> fibers showed<br />

slightly darker intermediate lines on the fiber surface parallel with the cellulose<br />

micr<strong>of</strong>ibrils.<br />

Gravimetric plant fiber analysis<br />

The fibers were milled to pass a 1 mm sieve. From the milled fibers, wax was extracted<br />

in chlor<strong>of</strong>orm, water-soluble components in water, pectin in EDTA solution, lignin in<br />

solution <strong>of</strong> chlorite and acetic acid and hemicellulose in boric acid and 12 % NaOH<br />

solution. The residual part was cellulose with less than 1 % <strong>of</strong> minerals (Browning,<br />

1967).<br />

RESULTS AND DISCUSSION<br />

The original <strong>hemp</strong> stems were 1.5-2.5 m tall and 5-15 mm in diameter near the soil<br />

surface. The stems contained 35-40 % w/w bast fibers and were organized in layers from<br />

the stem pith towards the surface by 1-5 mm xylem, 10-50 μm cambium, 100-300 μm<br />

cortex, 20-100 μm epidermis and 2-5 μm cuticle. The definition <strong>of</strong> stem components are<br />

in accordance with Garcia-Jaldon et al. (1998) and aspects <strong>of</strong> the stems are shown in<br />

SEM micrographs (Figure 1) and modeled in Figure 2A.<br />

Figure 1. Hemp stem shown at increasing magnification using different transverse<br />

sections in SEM: A: Xylem + cambium + cortex + epidermis; B: Primary and secondary<br />

single fibers; C: Major layers in primary single fiber; D: Thin lamellae within the S2<br />

layer.<br />

Risø-PhD-11 95

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