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FIFTH CANADIAN CONFERENCE ON NONDESTRUCTIVE ... - IAEA

FIFTH CANADIAN CONFERENCE ON NONDESTRUCTIVE ... - IAEA

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- 310 -<br />

frequency of about 50 MHz is optimum for the detection of surface cracks as small<br />

as 20 um in silicon nitride. This frequency is equivalent to an acoustic<br />

wavelength of 112 um in silicon nitride. Beyond 50 MHz, the detectability tends<br />

to level off due to the increase of attenuation losses. Thus, the crack<br />

measurements in this investigation were carried out at 50 MHz.<br />

The leaky Rayleigh waves propogating along the water-solid interface, lose their<br />

energy rapidly and particularily at high frequencies. Thus, only those flaws<br />

which are located near the point of incidence of the impinging beam are detected.<br />

As a result, the resolution of this method is very good since reflections from<br />

neighbouring flaws or specimen edges do not overlap with the signal from the flaw<br />

of interest. The resolution is particularily good when a narrow Rayleigh beam is<br />

employed by focusing the incident beam on the surface of the test piece using a<br />

focused transducer.<br />

Overall, the scanning simplicity, the high resolution and high sensitivity of<br />

leaky Rayleigh waves make this technique a practical and reliable method of<br />

detecting small surface flaws in ceramic materials.<br />

2.4 Measurement techniques<br />

The normal procedure for flaw size measurement by any ultrasonic technique<br />

utilizes the acoustic reflection coefficient, S, of the flaw for size estimation.<br />

S is defined as the ratio of the peak amplitudes of the flaw signal to input<br />

signal at the transducer terminal. In the case of cracks, however, the acoustic<br />

reflection is very much dependent on orientation of the crack with respect to the<br />

incident beam. This is demonstrated in the experimental results of Fig. 5<br />

obtained for a 100 ym Knoop indentation. Analytical solutions are given by<br />

Auld^ ' for calculation of the reflection coefficient at oblique angles. Both<br />

the analytical and experimental results indicate that as the direction of the<br />

crack relative to the Rayleigh beam deviates from normal, a smaller portion of<br />

the crack face reflections are received by the transducer. Thus, for complete<br />

characterization of cracks from the reflection coefficient, it is necessary to<br />

scan the test material in more than one direction.<br />

Another important factor affecting the acoustic signal amplitude from a flaw is<br />

the wavelength compared to the flaw size. Since at 50 MHz the Rayleigh<br />

wavelength in silicon nitride is about 112 pm and this is in the flaw size range<br />

of our interest (i.e. 10-200 um), therefore both the long wavelength (X^>a) and<br />

the short wavelength (A^

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