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IGCAR : Annual Report - Indira Gandhi Centre for Atomic Research

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IGC<br />

<strong>Annual</strong> <strong>Report</strong> 2007<br />

experimental analysis of<br />

detection and quantification of<br />

corrosion in mild steel by<br />

gamma ray scattering the<br />

Monte Carlo simulations have<br />

been done by using the Monte<br />

Carlo N- Particle (MCNP) code,<br />

which takes into account the<br />

detailed characteristics of the<br />

source, detector and the<br />

scatterer in calculating the<br />

gamma scattered intensity from<br />

the MS plates. The result of<br />

MCNP PHS simulations and<br />

their comparison with the<br />

experimental ones are shown in<br />

Fig. 6 <strong>for</strong> the normal MS plate<br />

and in Fig. 7 <strong>for</strong> the corroded<br />

one. A good agreement in the<br />

shape of the PHS is seen<br />

between the experimental<br />

spectra and MC simulated<br />

ones.<br />

Fig.6 The scattered PHS and its<br />

comparison with MCNP simulated<br />

one <strong>for</strong> normal MS plate<br />

Fig.7 The scattered PHS and its<br />

comparison with MCNP simulated<br />

one <strong>for</strong> corroded MS plate<br />

Table1. Density of MS corroded plate (kg/ m3) reconstructed from the<br />

experimental and MCNP simulated gamma scattered intensities and the average<br />

density value obtained by weight and volume measurements<br />

A methodology to reconstruct<br />

the densities of the corroded<br />

regions of the MS plate directly<br />

from the scattered intensities is<br />

developed and implemented. In<br />

this method the density, ρ of the<br />

specimen need not be known<br />

and only the knowledge of the<br />

target material's mass<br />

attenuation coefficients, µ/ ρ<br />

and µ'/ ρ is sufficient to correct<br />

<strong>for</strong> absorption of incident and<br />

scattered radiation. These mass<br />

attenuation coefficients are<br />

independent of the physical<br />

state of the matter (independent<br />

of density) and the knowledge<br />

of composition of the material<br />

is sufficient <strong>for</strong> reconstruction.<br />

The experimental and MCNP<br />

reconstructed densities from a<br />

typical voxel of the corroded<br />

MS plate are given in Table 1<br />

along with the average density<br />

value obtained by weighing the<br />

MS plate in a weighing balance<br />

and estimating its volume by<br />

fluid displacement method.<br />

From the Table 1 it can be seen<br />

that a good agreement is seen<br />

between the experimental<br />

values, MCNP calculations and<br />

average density value within<br />

estimated errors.<br />

The measured gamma<br />

scattered photo peak intensity<br />

from corroded MS plate<br />

decreases up to 6.46%<br />

compared to a normal MS plate<br />

and this corresponds to an<br />

average density loss of 0.416 x<br />

10 3 kg/ m 3 (5.24%) due to<br />

corrosion in a MS plate of size<br />

235 x 155 x 10 mm. This<br />

amount of metal loss due to<br />

corrosion has been detected<br />

and quantified in the present<br />

study. The experimental and<br />

MC results show that the<br />

scattering method is highly<br />

sensitive to changes in<br />

electronic and physical<br />

densities of the voxel under<br />

study and the magnitude of<br />

corrosion can be clearly<br />

identified and quantified by<br />

monitoring single scattered<br />

events.<br />

96 FUEL CYCLE

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