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IGCAR : Annual Report - Indira Gandhi Centre for Atomic Research

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IGC<br />

<strong>Annual</strong> <strong>Report</strong> 2007<br />

Fig.2 Shear punch testing of irradiated SS316 specimens (a) test setup (b) load-displacement<br />

plots showing increase in the maximum load with increasing dpa<br />

studies. Prior to preparation of<br />

irradiated specimens, extensive<br />

trials were carried out with<br />

unirradiated specimens to<br />

optimize the pre-thinning and<br />

electrolytic<br />

thinning<br />

parameters. TEM specimens<br />

were prepared using special<br />

fixtures developed <strong>for</strong> handling<br />

irradiated specimens.<br />

Irradiated specimens which had<br />

undergone displacement<br />

damage from 2 dpa to 56 dpa<br />

have been examined using 200<br />

keV Analytical TEM.<br />

A considerable increase in<br />

the strength and decrease in<br />

the ductility of the wrapper with<br />

increasing displacement per<br />

atom (dpa) have been observed<br />

from the small specimen<br />

mechanical tests. The<br />

transmission electron<br />

microscopic studies revealed<br />

the presence of voids and<br />

precipitates in the matrix (Fig<br />

3). Precipitates were identified<br />

to be of M23C6 type and<br />

precipitation of second phases<br />

corroborates the hardening<br />

observed on the wrapper.<br />

Precipitates<br />

Voids<br />

Fig.3 TEM image of the irradiated SS316 at a displacement damage of 40 dpa<br />

52 R&D FOR FBRs

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