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PNNL-13501 - Pacific Northwest National Laboratory

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Approach<br />

Two flow loops, one that operates in the laminar flow<br />

regime, and one that operates over a higher flow rate<br />

range, were developed to provide a flexible system for<br />

sensor evaluation. The laminar flow loop, shown in<br />

Figure 1 was designed especially for evaluating<br />

applications for ultrasonic doppler velocimetry and<br />

pressure drop, a technique to provide rheological profiles<br />

across the pipe. Based on conservation of linear<br />

momentum for steady pressure-driven flow, the pressure<br />

drop in the pipe provides the local shear rate distribution.<br />

Figure 1. Laminar flow loop instrumented with an<br />

ultrasonic doppler velocimetry sensing system for in-line<br />

velocity and viscosity profile measurements<br />

Evaluating the shear rate and the shear stress at points<br />

along the pipe yields the shear stress shear rate relation,<br />

which is equivalent to the shear viscosity shear rate<br />

relationship. This information and attenuation profiles<br />

can provide both rheological and concentration profiles of<br />

the fluid flowing in the 5-cm- (2-in.-) diameter loop. A<br />

Moyno pump provides flow rates of up to 40 L/min. The<br />

flow rate range and piping configuration were designed to<br />

provide fully developed laminar pipe flow and pressure<br />

drop measurements (the theory and operation of the<br />

sensing system are described in Powell et al. [2000]).<br />

Laminar flow loop support instrumentation includes<br />

measurement of temperature, flow rate, and pressure drop.<br />

The second loop, shown in Figure 2, is powered by a<br />

centrifugal pump that provides a flow rate from 114 to<br />

568 L/min (30 to 150 gal/min). This flexible<br />

configuration includes two pipelines, a 2.5-cm- (1-in.-)<br />

diameter and 5-cm- (2-in.-) diameter. These lines can be<br />

operated either singly or in parallel. The lines include<br />

penetrations to permit integration of spool pieces housing<br />

several existing ultrasonic sensors, shown in Figure 3.<br />

These ultrasonic densimeters measure the density at the<br />

sensor-fluid interface based on the amount of reflected<br />

ultrasonic signal (Greenwood et al. 1999). In addition to<br />

density, by making measurements at multiple orientations,<br />

the sensors can be used to characterize sedimentation, the<br />

presence of bubble layers, and detect density gradients.<br />

Figure 2. Variable-flow rate, low-volume flow loop for<br />

slurry process evaluation using multiple ultrasonic sensing<br />

systems<br />

Figure 3. a) Prototype ultrasonic densimeter spool piece,<br />

b) Ultrasonic densimeter spool piece for deployment at<br />

Hanford to support radioactive waste transfers<br />

Instrumentation in each line to support loop operation<br />

includes temperature measurement; Micromotion coriolus<br />

mass flow meters to measure mass flow rate, density, and<br />

temperature; and Controlotron clamp on ultrasonic flow<br />

meters to measure volumetric flow and velocity. The<br />

process sensors are integrated into a data acquisition<br />

computer.<br />

In addition to fluid evaluation during pipeline transport,<br />

sensors such as the immersion densimeter (shown in<br />

Figure 4a) and the concentration and particle sizing sensor<br />

(shown in Figure 4b) can be installed into the fluid<br />

a<br />

b<br />

Separations and Conversions 425

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