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On the Formation of Nitrogen Oxides During the Combustion of ...

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3 Experiments on Droplet Array <strong>Combustion</strong><br />

Measurement <strong>of</strong> Pressure<br />

The pressure inside <strong>the</strong> DCU vacuum protection is controlled in <strong>the</strong> range <strong>of</strong><br />

0 to 2bar at 5Hz. The responsible pressure control unit is activated just after<br />

lift-<strong>of</strong>f <strong>of</strong> <strong>the</strong> sounding rocket module. The most critical event is a pressure<br />

drop in <strong>the</strong> whole DCU during exhaust gas sampling and air displacement<br />

in <strong>the</strong> combustion chamber, caused by a leak <strong>of</strong> <strong>the</strong> combustion chamber<br />

shutter (cf. Chap. 3.1.3). Therefore, pressure control is disabled during this<br />

crucial event to avoid an excess consumption <strong>of</strong> air. Apart from that, compensation<br />

is regularly started when <strong>the</strong> pressure is out <strong>of</strong> its nominal range<br />

<strong>of</strong> (1.000±0.025)×10 5 Pa. Besides this direct control, three fur<strong>the</strong>r sensors are<br />

employed for monitoring purposes in <strong>the</strong> pressurized air supply system.<br />

A dynamic pressure sensor (manufacturer: PCB Piezotronics; type: M112A05)<br />

is installed in <strong>the</strong> combustion chamber in order to capture pressure fluctuations<br />

for scientific purposes at a sampling rate <strong>of</strong> 500 Hz. It has a sensitivity<br />

<strong>of</strong> 0.160 pC kPa −1 and its signal is amplified by an in-line charge converter<br />

and an ICP ® amplifier. Two different models <strong>of</strong> <strong>the</strong> in-line charge converter<br />

(both also manufactured by PCB Piezotronics) were used: <strong>the</strong> 422E36 and <strong>the</strong><br />

422E12 model in <strong>the</strong> drop tower and <strong>the</strong> sounding rocket setup, respectively.<br />

Both <strong>of</strong> <strong>the</strong>m have a charge conversion sensitivity <strong>of</strong> 10mV pC −1 [330–333].<br />

The exhaust gas sampling (EGS) system including its four sample cylinders is<br />

repeatedly evacuated during experiment preparation and countdown to keep<br />

contamination low and re-evacuation times short. The vacuum level is monitored<br />

directly at <strong>the</strong> central EGS backbone (cf. Fig. 3.9, D) by a compact Full-<br />

Range gauge (manufacturer: Pfeiffer Vacuum; type: PKR 251). It combines a<br />

cold cathode and Pirani gauge to cover a vacuum/pressure range from 5×10 −9<br />

to 1000 mbar. Thus, <strong>the</strong> associated leakage rates <strong>of</strong> <strong>the</strong> whole EGS system or<br />

single sample cylinders became calculable from <strong>the</strong> given volumes and <strong>the</strong><br />

pressure readings at fixed time intervals. The pressure readings <strong>the</strong>mselves<br />

were included in <strong>the</strong> data logging <strong>of</strong> <strong>the</strong> drop tower campaign but not in <strong>the</strong><br />

one <strong>of</strong> <strong>the</strong> sounding rocket campaign. In <strong>the</strong> case <strong>of</strong> <strong>the</strong> latter, monitoring<br />

by an external program was performed until −90 min before launch, using a<br />

separate control unit (manufacturer: Pfeiffer Vacuum; type: TPG 261) and access<br />

through <strong>the</strong> late access panel <strong>of</strong> <strong>the</strong> sounding rocket module. Afterwards,<br />

<strong>the</strong> remaining vacuum level <strong>of</strong> <strong>the</strong> sample cylinders was extrapolated for <strong>the</strong><br />

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