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On the Formation of Nitrogen Oxides During the Combustion of ...

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3.1 Droplet <strong>Combustion</strong> Facility<br />

• High surface quality – by applying surface coating<br />

• High temperature resistance – by using special sealing<br />

• High vacuum level and low leakage rate<br />

As illustrated in Figure 3.2, <strong>the</strong> EGS system is installed on <strong>the</strong> fifth experiment<br />

platform, in close proximity to <strong>the</strong> combustion chamber. It is shown in greater<br />

detail in Figure 3.9. The installation directly above <strong>the</strong> combustion chamber<br />

is chosen to keep <strong>the</strong> dead volume <strong>of</strong> <strong>the</strong> piping low, which results in low contamination<br />

<strong>of</strong> <strong>the</strong> samples and an optimized performance <strong>of</strong> <strong>the</strong> EGS system.<br />

The design meets <strong>the</strong> strict relation <strong>of</strong> V piping /V sample ≤ 1%, and <strong>the</strong> piping itself<br />

has a surface to volume ratio <strong>of</strong> 1.85 with an inner diameter <strong>of</strong> D i = 2.16mm.<br />

Since four combustion runs were scheduled on <strong>the</strong> TEXUS-46 sounding rocket<br />

campaign, <strong>the</strong> layout is based on four sample cylinders. Each <strong>of</strong> <strong>the</strong>m has a<br />

volume <strong>of</strong> 200 ml, which is optimized towards <strong>the</strong> minimum volume required<br />

for gas analysis. All metal surfaces <strong>of</strong> <strong>the</strong> EGS system being directly exposed to<br />

<strong>the</strong> combustion products are coated with amorphous silicon 1 to prevent negative<br />

surface effects on <strong>the</strong> gas composition and a distorting gas adsorption.<br />

B<br />

C<br />

A<br />

D<br />

Figure 3.9: Exhaust Gas Sampling Platform. Left: top view, right: bottom view [196, 197, 293,<br />

294, 296]. A: sample cylinders, B: solenoid vacuum valve for connection to combustion<br />

chamber, C: solenoid vacuum valve for connection to evacuation line, D:<br />

vacuum gauge.<br />

1 Sulfinert ® coating was used instead <strong>of</strong> <strong>the</strong> Silcosteel ® coating mentioned above. Both are very similar from <strong>the</strong><br />

chemical point <strong>of</strong> view but have different product names.<br />

73

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